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식품의 기준 및 규격 · 제8편 일반시험법분석조건 4건7.1.2.2

다성분 시험법-제2법

식품의약품안전처 고시 제2026-55호 「식품의 기준 및 규격」 제8. 일반시험법

배포 전 적대적 검증 완료 (2026-09-04, Claude Fable 5)

이 페이지는 고시 원문의 크로마토그래프 분석조건만 뽑아 정리한 것입니다. 시험 전체 절차(검체 조제, 시스템적합성 기준, 계산식 등)는 담고 있지 않으니, 실제 시험 수행과 판정은 반드시 고시 원문을 확인하십시오.

이 시험법은 고시가 구판·신판을 병행 수록하는 개정 과도기에 있습니다. 같은 시험의 조건이 판별로 두 벌 실린 것은 원문 그대로이며, 아래에 판 단위로 나눠 실었습니다 — 어느 판을 적용할지는 각 판의 적용 기간을 확인하십시오.

구판— 2026.12.31.까지 적용

분석조건2건

분석조건 (1)

GC구판 · 2026.12.31.까지7.1.2.2FD-다성분-시험법-제2법-x1

원문 표제 단서: 기체크로마토그래프-질량분석기

칼럼
GC-5 · USP G27

DB-5MS

안지름 0.25 mm · 길이 30 m · 막두께 0.25 μm

칼럼온도
60℃에서 시험용액을 주입하여 20℃/분의 비율로 180℃까지 온도를 상승시키고 5℃/분의 비율로 300℃까지 상승시켜 5분간 유지한다.
유량
1.2 mL/분
운반기체
나) 이동상 가스 및 유량: 헬륨(He) 또는 이와 동등한 것, 1.2 mL/분
주입방법
라) 주입 방법: Splitless mode
질량분석(MS) 조건 보기 (3항목)
인터페이스 온도
마) 인터페이스 온도: 300℃
분석대상물질
바) 분석대상(272종) 물질의 조건 [표 1]
전이표
분석성분 (Compound)머무름 시간 (분)분자량 (MW)관측질량 (Exact mass)선구이온 (Precursor ion, m/z)생성이온 (Product ion, m/z)충돌 에너지 (Colllision energy, eV)
1노나클로르-시스*** (Nonachlor-cis)16.35444.2439.740730030
40930015
노나클로르-트랜스*** (Nonachlor-trans)14.45444.2439.740730015
40930025
2뉴아리몰 (Nuarimol)17.99314.7314.013911115
1075230
3니트로탈-아이소프로필 (Nitrothal-isopropyl)12.50295.3295.119412020
23619410
4다이아지논 (Diazinon)9.64304.3304.11999315
13510
5다이알레이트 (Diallate)8.63270.2269.023415020
19215
6다이알리포르 (Dialifor)21.84393.8393.03579725
2088925
7데스메트린 (Desmetryn)10.63213.3213.12135820
1985
8델타메트린 (Deltamethrin)27.20505.2502.92539315
17427
9디니코나졸 (Diniconazole)16.25326.2325.026813635
23215
10디니트라민 (Dinitramine)9.85322.2322.026124110
19520
11p,p’-디디디* (p,p’-DDD)16.40320.0317.923716525
23516525
p,p’-디디이* (p,p’-DDE)15.06318.0315.924617630
24817630
o,p’-디디티* (o,p’-DDT)16.47354.5351.923716525
23516525
p,p’-디디티* (p,p’-DDT)17.64354.5351.923716525
23516525
12디메타메트린 (Dimethametryn)13.19255.4255.12121225
9420
13디메타클로르 (Dimethachlor)10.66255.7255.113410515
19714810
14디메테나미드 (Dimethenamid)10.67275.8275.015411110
23015410
15디메토모르프(E)* (Dimethomorph E)27.99387.9387.130116512
38730112
디메토모르프(Z)* (Dimethomorph Z)28.58387.9387.138730112
30116512
16디메티핀* (Dimethipin)9.24210.3210.0124765
118585
17디메틸빈포스(E) (Dimethylvinphos E)11.73331.5329.929510920
29710920
디메틸빈포스(Z) (Dimethylvinphos Z)12.1.0331.5329.929510920
29710920
18디메피퍼레이트 (Dimepiperate)13.61263.4263.11451125
6915
192,6-디아이피엔* (2,6-DIPN, (2,6-Diisopropylnaphthalene)9.06212.3212.121219715
19715510
20디에타틸-에틸 (Diethatyl-ethyl)14.44311.8311.118816010
13040
21디에토펜카브 (Diethofencarb)12.10267.3267.12672255
22516810
22디옥사티온 (Dioxathion)9.42456.5456.02709730
125975
23디코폴 (Dicofol)12.49370.5367.91397535
11115
24디크로토포스 (Dicrotophos)8.28237.2237.01279515
1931275
25디클로란** (Dicloran)9.01207.0205.916012410
20617615
26디클로르미드 (Dichlormid)5.86208.1207.01721085
1665610
27디클로베닐 (Dichlobenil)5.80172.0170.917313610
17113630
28디클로뷰트라졸 (Diclobutrazol)15.37328.2327.027216110
27015915
29디클로펜티온** (Dichlofenthion)10.65315.1313.927922310
22320515
30디클로포프메틸 (Diclofop-methyl)18.21341.2340.034025310
25316240
31디클로플루아니드* (Dichlofluanid)8.27333.2331.9200455
4425
32디티오피르 (Dithiopyr)11.31401.4401.035428615
3065
33디페노코나졸 (Difenoconazole)26.90406.3405.032526715
32326515
34디페닐아민 (Diphenylamine)8.02169.2169.016816720
16916815
35디펜아미드 (Diphenamid)12.69239.3239.116716530
15220
36디플루페니칸 (Diflufenican)18.29394.3394.026621825
23815
37렙토포스 (Leptophos)20.46412.1409.837736225
1717725
38린단** (Lindane, γ-BHC)9.47290.8287.818114515
2171815
39마이클로뷰타닐 (Myclobutanil)15.18288.8288.117912515
1525
40메탈락실 (Metalaxyl)11.17279.3279.123414620
2491905
41메토프로트린 (Methoprotryn)15.47271.4271.125617025
21215
42메톡시클로르 (Methoxychlor)19.56345.6344.022714140
16925
43메톨라클로르 (Metolachlor)11.99283.8283.116213315
23816210
44메트리뷰진 (Metribuzin)10.79214.3214.01988220
5530
45메티다티온 (Methidathion)13.90302.3301.91455815
855
46메틸트리티온 (Methyl trithion)16.09314.8313.91254715
15712135
47메파니피림 (Mepanipyrim)14.42223.3223.122222120
22210
48메펜피르-디에틸 (Mefenpyr-diethyl)18.72373.3372.029925310
25319020
49메프로닐 (Mepronil)16.89269.3269.12699140
11915
50모노리누론 (Monolinuron)9.24214.6214.01269915
214615
51몰리네이트* (Molinate)7.30187.3187.11871265
126985
52베노다닐 (Benodanil)16.68323.1322.923120320
7625
53벤조일프로프-에틸 (Benzoylprop-ethyl)18.78366.2365.029210510
1057710
54벤퓨러세이트 (Benfuresate)10.62256.3256.02561635
1631215
55벤플루라린 (Benfluralin)8.31335.3335.129216020
26410
56보스칼리드 (Boscalid)24.34343.2342.01407625
11210
57부피리메이트 (Bupirimate)15.31316.4316.127319310
10810
58뷰타클로르 (Butachlor)14.22311.9311.123716010
17614710
59뷰타페나실 (Butafenacil)23.41474.8474.033118020
12440
60뷰트랄린 (Butralin)12.56295.3295.126617420
22015
61뷰틸레이트** (Butylate)6.36217.4217.3156575
1465710
62뷰프로페진 (Buprofezin)15.32305.4305.11725715
17513215
63브로모뷰타이드 (Bromobutide)10.81312.3311.011811710
23217610
64브로모포스-메틸 (Bromophos-methyl)12.67366.0363.833131620
32931415
65브로모포스-에틸 (Bromophos-ethyl)13.91394.0391.830321130
6330
66브로모프로필레이트 (Bromopropylate)19.37428.1425.934318515
33918315
67α-비에이치시 (α-BHC)8.77290.8287.818114515
2171815
β-비에이치시 (β-BHC)9.2518114515
2171815
δ-비에이치시 (δ-BHC)10.0718114515
2171815
68비페녹스* (Bifenox)19.89342.1341.034131110
18920
69비펜트린 (Bifenthrin)19.41422.9422.118116615
16530
70빈클로졸린 (Vinclozolin)10.89286.1284.919814515
18712420
71사이퍼메트린* (Cypermethrin)24.60416.3415.01659110
1631275
72사이프라진 (Cyprazine)10.71227.7227.017010915
21210930
73사이프로디닐 (Cyprodinil)13.03225.3225.122522410
22420825
74사이플루트린* (Cyfluthrin)23.99434.3433.022620610
1631275
75사이플루페나미드 (Cyflufenamid)15.67412.4412.122320312
1888840
76γ-사이할로트린* (γ-Cyhalothrin)20.93449.9449.12081815
19714110
λ-사이할로트린* (λ-Cyhalothrin)21.272081815
19714110
77사이할로포프뷰틸**** (Cyhalofop-butyl)20.98357.4357.125612020
22910915
78설포텝 (Sulfotep)8.39322.3322.020214610
32214625
79스피로메시펜 (Spiromesifen)18.75370.5370.227220910
25410
80스피록사민 (Spiroxamine)10.98297.5297.2100725
1981265
81시메코나졸 (Simeconazole)10.98293.4293.112110115
7535
82시메트린 (Simetryn)11.08213.3213.121317010
18510
83시아노포스 (Cyanophos)9.53243.2243.0125795
24310910
84신메틸린 (Cinmethylin)11.27274.4274.11541115
16910710
85실라플루오펜 (Silafluofen)25.31408.6408.11799110
28625810
86아닐로포스** (Anilofos)19.85367.8367.022615715
1845
87아라마이트 (Aramite)15.77334.9334.11876510
1856310
88아메트린 (Ametryn)11.18227.3227.12271855
17010
89아세토클로르* (Acetochlor)10.76269.8269.122314610
13220
에이치이엠에이* (HEMA(2-(1-hydroxyl-ethyl)-6-methyl-aniline))6.28151.2151.015111740
13220
이엠에이* (EMA(2-ethyl-6-methylaniline))5.14135.2135.11207720
13512010
90아스폰 (Aspon)11.93378.4378.021111510
9735
91아이소티아닐 (Isotianil)17.48298.1296.91809120
29718015
92아이소펜포스 (Isofenphos)13.28345.4345.121312120
1855
93아이소펜포스-메틸 (Isofenphos-methyl)12.85331.4331.11999330
12115
94아이소프로카브 (Isoprocarb)7.17193.2193.113612110
7730
95아이소프로티올레인 (Isoprothiolane)14.86290.4290.01898920
14510
96아이소프로파린 (Isopropalin)12.82309.4309.123816510
2802385
97아이소피라잠 (Isopyrazam)21.87359.4359.135915940
15913910
98아이속사디펜-에틸 (Isoxadifen-ethyl)17.19295.3295.12222055
20420
99아자코나졸 (Azaconazole)15.39300.1299.021917515
21717315
100아크리나트린* (Acrinathrin)21.70541.4541.12081815
2899310
101아트라진 (Atrazine)9.21216.7215.021520010
5815
102알드린** (Aldrin)12.18364.9361.826319340
19140
디엘드린** (Dieldrin)15.20380.9377.826319340
26519340
103알라클로르 (Alachlor)10.99269.8269.118816010
16013030
104알리도클로르 (Allidochlor)5.38173.6173.0134565
132565
105에디펜포스* (Edifenphos)17.36310.4310.017310910
20110915
106에타코나졸 (Etaconazole)16.35328.2327.017310925
24517320
107에탈플루랄린 (Ethalfluralin)8.12333.3333.027620215
3162765
108에토퓨메세이트 (Ethofumesate)11.67286.3286.016110510
20713710
109에토프로포스 (Ethoprophos)8.06242.3242.01581145
9720
110에톡사졸 (Etoxazole)19.65359.4359.130027025
20417610
111에트리디아졸 (Etridiazole)6.55247.5245.921114025
18310
112에티온 (Ethion)16.45384.5383.923112925
17510
113에티클로제이트 (Ethychlozate)13.29238.7238.016513810
10215
114에폭시코나졸 (Epoxiconazole)18.57329.8329.019211125
13815
115α-엔도설판 (α-Endosulfan)14.36406.9403.824120615
20517015
β-엔도설판 (β-Endosulfan)16.20406.9403.820517015
20717215
엔도설판 설페이트 (Endosulfan sulfate)17.43422.9419.827423725
27223720
116엔드린 (Endrin)15.85380.9377.826319340
19135
δ-케토-엔드린 (δ-keto-Endrin)18.80380.9377.831728110
24520
117엠지케이-264 (MGK-264)13.11275.4275.1164675
9810
118오쏘페닐페놀* (Ortho-phenyl phenol)7.10170.2170.016911530
14115
119옥사디아존 (Oxadiazon)15.12345.2344.01751125
25817515
120옥사딕실 (Oxadixyl)16.33278.3278.116311725
1325
121옥시플루오르펜 (Oxyfluorfen)15.29361.7361.030022320
36130020
122이사조포스 (Isazofos)9.93313.7313.02571625
20816610
123이프로디온* (Iprodione)19.03330.2329.03145620
24510
124이프로벤포스 (Iprobenfos)10.28288.3288.02049110
12135
125이프코나졸 (Ipconazole)21.28333.9333.11259920
8920
126이피엔 (EPN)19.29323.3323.01691415
1577730
127이피티씨 (EPTC)5.88189.3189.1132905
1891285
128인다노판 (Indanofan)19.78340.8340.01397535
15910315
129인독사카브** (Indoxacarb)27.34527.8527.020310625
13415
130족사마이드 (Zoxamide)18.62336.6335.018715920
12330
131카두사포스 (Cadusafos)8.56270.4270.01599720
1589720
132카보페노티온 (Carbophenothion)17.30342.9341.93441595
3421575
133카복신 (Carboxin)15.32235.3235.023514310
8720
134카펜트라존에틸* (Carfentrazone-ethyl)17.24412.2411.034031210
31215120
135코마포스 (Coumaphos)22.61362.8362.02101825
22616310
136퀴날포스 (Quinalphos)13.49298.3298.014611810
9130
137퀴녹시펜 (Quinoxyfen)17.43308.1306.923720830
30723720
138퀴잘로포프에틸* (Quizalofop-ethyl)24.68372.8372.037229910
29925515
139퀸토젠 (Quintozene)9.35295.3292.824921410
29523720
140크레속심메틸 (Kresoxim-methyl)15.37313.4313.11318935
1168915
141클로로넵 (Chloroneb)6.94207.1205.91935330
19111315
142클로로벤질레이트 (Chlorobenzilate)16.14325.2324.025113910
13911110
143클로로탈로닐* (Chlorothalonil)9.79265.9263.826623120
17030
144클로로프로필레이트 (Chloropropylate)16.14339.2338.025113910
13911110
145클로르니트로펜 (Chlornitrofen)17.19318.5316.931728715
2361735
146클로르단-시스 (Chlordane-cis)14.36409.8405.737526620
37326620
클로르단-트랜스 (Chlordane-trans)13.97409.8405.737526620
37326620
147클로르벤시드** (Chlorbenside)13.97269.2267.926812510
1258915
148클로르부팜 (Chlorbufam)9.21223.7223.02235315
12715
149클로르에톡시포스 (Chlorethoxyfos)7.88336.0333.81539715
974735
150클로르탈-디메틸 (Chlorthal-dimethyl)12.18332.0329.929922125
30122325
151클로르티오포스 (Chlorthiophos)16.52361.2359.932526910
26920510
152클로르티온 (Chlorthion)12.47297.6296.91254710
29710910
153클로르페나피르 (Chlorfenapyr)15.60407.6405.924722715
32824720
154클로르펜손 (Chlorfenson)14.72303.2301.917511110
1117515
155클로르프로팜 (Chlorpropham)8.25213.7213.017112715
1539025
156클로르플루레놀-메틸 (Chlorflurenol-methyl)13.79274.7274.021715225
21515220
157클로르피리포스 (Chlorpyrifos)12.05350.6348.931425820
19917115
158클로르피리포스-메틸 (Chlorpyrifos-methyl)10.80322.5320.828627120
9320
159클로마존 (Clomazone)9.32239.7239.01258915
20410725
160클로졸리네이트 (Chlozolinate)13.22332.1331.03312595
25918810
161키노메티오네이트* (Chinomethionat)13.99234.3233.92342065
20614815
162터바실 (Terbacil)9.89216.7216.01607615
1618820
163터부메톤 (Terbumeton)9.32225.3225.116915410
21010020
164터부트린 (Terbutryn)11.60241.4241.11851705
2411850
165테부코나졸 (Tebuconazole)18.09307.8307.125012530
25212730
166테부펜피라드 (Tebufenpyrad)19.89333.9333.127617110
33317120
167테부피림포스 (Tebupirimfos)10.21318.4318.12762345
26113715
168테크나젠 (Tecnazene)7.70260.9258.821314225
21517925
169테트라디폰 (Tetradifon)20.21356.0353.822920110
15911120
170테트라메트린* (Tetramethrin)19.18331.4331.11647725
10715
171테트라코나졸 (Tetraconazole)12.34372.1371.033620440
21820
172테트라클로르빈포스 (Tetrachlorvinphos)14.10366.0363.832910925
33110925
173테플루트린 (Tefluthrin)9.95418.7418.017713720
12720
174톨클로포스메틸 (Tolclofos-methyl)11.00301.1299.92659330
25015
175트랄로메트린 (Tralomethrin) (Deltamethrin으로 분석)27.20665.0660.02539315
17427
176트리디판** (Tridiphane)11.29320.4317.817310930
18715915
177트리아디메폰 (Triadimefon)12.36293.8293.020811135
18110
트리아디메놀 (Triadimenol)13.59295.8295.11306525
1286520
178트리아조포스 (Triazophos)16.94313.3313.01611345
10615
179트리알레이트 (Tri-allate)10.11304.7303.026818410
22620
180트리플록시스트로빈 (Trifloxystrobin)17.49408.4408.11168915
22213010
181트리플루랄린 (Trifluralin)8.26335.3335.12642065
30626410
182트리플루미졸 (Triflumizole)13.66345.8345.020617915
2784315
183티오나진 (Thionazin)7.76248.2248.01929615
24814010
184티오메톤 (Thiometon)8.89246.3245.91254725
93635
185티플루자마이드 (Thifluzamide)15.10528.1525.819412525
16610
186파라티온 (Parathion)12.27291.3291.02918140
10910
187파라티온메틸 (Parathion-methyl)10.96263.2263.02637935
10915
188파클로부트라졸 (Paclobutrazol)14.14293.8293.123612510
1675
189퍼메트린-시스*** (Permethrin-cis)22.72391.3390.018316820
15510
퍼메트린-트랜스*** (Permethrin-trans)22.9716820
15510
190퍼탄 (Perthane)15.92307.3306.022316520
19320
191페나리몰 (Fenarimol)21.40331.2330.025113915
21910710
192페나미돈 (Fenamidone)19.67311.4311.126818020
23823710
193페노뷰카브 (Fenobucarb)7.77207.3207.112110315
1501215
194페노티오카브 (Fenothiocarb)14.26253.4253.1725610
160728
195페녹사닐** (Fenoxanil)15.84329.2328.018912510
15410
196페니트로티온 (Fenitrothion)11.61277.2277.02772605
10920
197펜디메탈린 (Pendimethalin)12.99281.3281.125216210
2080
198펜발러레이트, 이성체 1* (Fenvalerate, Iso. 1)26.06419.9419.116712510
16912710
펜발러레이트, 이성체 2* (Fenvalerate, Iso. 2)26.47419.9419.116712510
16912710
199펜뷰코나졸 (Fenbuconazole)23.57336.8336.11981295
1297820
200펜손 (Fenson)12.64268.7267.91417710
2687720
201펜코나졸 (Penconazole)13.18284.2283.024815730
19220
202펜클로르포스 (Fenchlorphos)11.24321.5319.928527020
24030
203펜클로림** (Fenclorim)8.78225.1223.918910410
22418920
204펜타클로로벤조니트릴 (Pentachlorobenzonitrile)9.43275.3272.827517930
24020
205펜토에이트 (Phenthoate)13.47320.4320.027412515
12110
206펜톡사존 (Pentoxazone)20.47353.8353.02877010
2857015
207펜티오피라드 (Penthiopyrad)16.34359.4359.130217720
17710120
208펜티온 (Fenthion)12.17278.3278.027810920
16920
209펜퓨람 (Fenfuram)9.99201.2201.020110925
1095320
210펜프로파트린*** (Fenpropathrin)19.71349.4349.126521010
8940
211펜프로피모르프 (Fenpropimorph)12.28303.5303.21287015
11010
212펜플루펜 (Penflufen)16.80317.4317.11418415
27414115
213펜피라자민 (Fenpyrazamine)21.33331.4331.123018810
11730
214포노포스 (Fonofos)9.64246.3246.02461375
10915
215포모티온 (Formothion)10.40257.3256.9126935
1709315
216포사론 (Phosalone)20.43367.8366.91821385
10215
217포스멧 (Phosmet)19.15317.3316.916013310
7730
218포스파미돈(E) (Phosphamidon E)9.52299.7299.026412710
12710915
포스파미돈(Z) (Phosphamidon Z)10.42299.7299.026412710
12710915
219프레틸라클로르 (Pretilachlor)14.86311.9311.116213220
2622025
220프로디아민 (Prodiamine)11.59350.3350.127525510
32127910
221프로메톤 (Prometon)9.09225.3225.11831685
21016810
222프로메트린 (Prometryn)11.26241.4241.122618410
24119910
223프로사이미돈 (Procymidone)13.57284.1283.0283965
285965
224프로클로라즈* (Prochloraz)22.97376.7375.03087015
18013810
2,4,6-트리클로로페놀* (2,4,6-trichlorophenol)5.90376.7375.01329715
1969740
225프로티오포스 (Prothiofos)14.81345.2343.926722120
23910
226프로파닐 (Propanil)10.67218.1217.016112625
21716125
227프로파진 (Propazine)9.29229.7229.12295815
21417210
228프로파클로르 (Propachlor)7.82211.7211.01699310
1769220
229프로팜 (Propham)6.57179.2179.01799315
137938
230프로페노포스 (Profenofos)14.95373.6371.933726710
33926910
231프로페탐포스 (Propetamphos)9.47281.3281.01386420
1941665
232프로플루랄린 (Profluralin)9.39347.3347.131819920
5510
233프로피소클로르 (Propisochlor)11.10283.8283.116212020
14715
234프로피자마이드 (Propyzamide)9.59256.1255.017314520
10935
235프로피코나졸, 이성체 1 (Propiconazole, Iso. 1)17.42342.2341.02596910
1735
프로피코나졸, 이성체 2 (Propiconazole, Iso. 2)17.626910
1735
236프로하드로자스몬 (Prohydrojasmon)9.91254.4254.1153975
1848315
237프탈리드 (Phthalide, Fthalide)12.52271.9269.824121315
24321515
238플람프로프-아이소프로필 (Flamprop-isopropyl)16.19363.8363.11057715
5140
239플루메트랄린 (Flumetralin)14.20421.7421.014311720
10730
240플루미옥사진 (Flumioxazin)25.95354.3354.13543265
2872595
241플루발리네이트, 이성체 1* (Fluvalinate, Iso. 1)26.36502.9502.12505520
20020
플루발리네이트, 이성체 2* (Fluvalinate, Iso. 2)26.515520
20020
242플루시트리네이트, 이성체 1** (Flucythrinate, Iso. 1)24.74451.5451.115710715
19910725
플루시트리네이트, 이성체 2** (Flucythrinate, Iso. 2)25.1315710715
19910725
243플루실라졸 (Flusilazole)15.26315.4315.123316520
15220
244플루아지포프-뷰틸 (Fluazifop-butyl)15.96383.4383.1282915
23825
245플루아크리피림 (Fluacrypyrim)16.80426.4426.114510230
2041895
246플루엔설폰 Fluensulfone7.70291.7290.91195930
9210
247플루오로클로리돈 (Fluorochloridone)12.49312.1311.018710920
31117420
248플루오피람 (Fluopyram)13.35396.7396.01739535
14520
249플루퀸코나졸 (Fluquinconazole)22.84376.2375.034010840
28630
250플루클로랄린 (Fluchloralin)9.66355.7355.03062645
3266315
251플루티아닐 (Flutianil)25.19426.4426.02312165
20010
252플루펜피르-에틸 (Flufenpyr-ethyl)16.15408.7408.040834515
32128615
253플룩사피록사드 (Fluxapyroxad)19.27381.3380.01594330
13910
254피라조포스 (Pyrazophos)21.52373.4373.023220410
22119310
255피라카볼리드 (Pyracarbolid)12.70217.3217.1125975
5515
256피라클로포스** (Pyraclofos)22.04360.8360.019413820
13910
257피라플루펜에틸 (Pyraflufen-ethyl)17.71413.2412.041234910
34930715
258피리달릴*** (Pyridalyl)25.10491.1488.920417610
14820
259피리메타닐 (Pyrimethanil)9.77199.3199.119811835
15820
260피리미노박메틸(E) (Pyriminobac-methyl E)17.58361.4361.130223015
25620
피리미노박메틸(Z) (Pyriminobac-methyl Z)16.1423015
25620
261피리미카브 (Pirimicarb)10.22238.3238.11669612
23816610
262피리미포스메틸 (Pirimiphos-methyl)11.55305.3305.029012520
2331515
263피리미포스에틸 (Pirimiphos-ethyl)12.69333.4333.130416810
31816610
264피리페녹스 (Pyrifenox)14.06295.2294.018712420
17110025
265피리프탈리드 (Pyriftalid)21.50318.3318.031827320
2745
266피콕시스트로빈 (Picoxystrobin)14.41367.3367.114510230
33517310
267피페로닐부톡사이드 (Piperonyl butoxide)18.50338.4338.217613125
14510
268피프로닐 (Fipronil)13.10437.1435.936721330
25530
269할펜프록스*** (Halfenprox)24.51477.3476.026511710
26312940
270헥시티아족스 (Hexythiazox)13.96352.9352.11841495
1561555
271헵타클로르 (Heptachlor)11.22373.3369.827223720
27423720
헵타클로르 에폭사이드 (Heptachlor epoxide)13.26389.3385.835325330
21718220
272헵테노포스 (Heptenophos)7.46250.6250.01246340
8915

동일 규격 권장 · GC는 칼럼 규격을 원문 그대로 두는 것을 권합니다. 캐필러리는 고정상과 규격(길이·안지름·막두께)이 함께 시험법을 이루기 때문에, 치수를 바꾸면 머무름과 분리가 직접 달라집니다. 같은 고정상의 동등 제품을 원문과 같은 규격으로 고르십시오.

이 조건으로 GC 시뮬레이션 열기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다. 기울기 프로파일·압력·용매 소모량은 이 조건의 값이지만, 화합물 정보를 넘기지 않으므로 머무름 시간과 분리도는 예시값입니다.

고시 원문 보기 (축자)
가) 컬럼: DB-5MS(30 m × 0.25 mm, 0.25 μm) 또는 이와 동등한 것
나) 이동상 가스 및 유량: 헬륨(He) 또는 이와 동등한 것, 1.2 mL/분
다) 오븐 온도: 60℃에서 시험용액을 주입하여 20℃/분의 비율로 180℃까지 온도를 상승시키고 5℃/분의 비율로 300℃까지 상승시켜 5분간 유지한다.
라) 주입 방법: Splitless mode
마) 인터페이스 온도: 300℃
바) 분석대상(272종) 물질의 조건
[표 1]

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 GC-5USP G27 상당

5% 페닐-95% 메틸폴리실록산(USP G27). 범용 약비극성 상.

함께 보기

타사 컬럼 대체 솔루션컬럼 추천 도구

분석조건 (2)

LC기울기 용리구판 · 2026.12.31.까지7.1.2.2FD-다성분-시험법-제2법-x2

원문 표제 단서: 액체크로마토그래프-질량분석기

칼럼
C18 · USP L1

C18계 컬럼

안지름 2.1 mm · 길이 10 cm · 입자경 2.7 μm

칼럼온도
40℃
이동상
  • 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 수용액
  • 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 메탄올
유량
0.2 mL/분
주입량
2 μL
질량분석(MS) 조건 보기 (2항목)
분석대상물질
바) 분석대상(242종) 물질의 조건 [표 2]
전이표
분석성분 (Compound)이온화 (Ionization mode)머무름 시간 (분)분자량 (MW)관측질량 (Exact mass)선구이온 (Precursor ion, m/z)생성이온 (Product ion, m/z)충돌 에너지 (Collision energy, eV)
1나프로파마이드 (Napropamide)Positive9.20271.4271.127212921
17123
2네뷰론 (Neburon)Positive9.60275.2274.02758823
11421
3노레아(노루론) (Norea(Noruron))Positive8.17222.3222.12237239
6749
4노르플루라존 (Norflurazon)Positive7.48303.7303.030414049
14561
5노발루론* (Novaluron)Negative11.18492.7492.049147118
15622
6니텐피람 (Nitenpyram)Positive4.65270.7270.027122517
12639
7다이뮤론 (Daimuron)Positive8.60268.4268.126915117
11927
8도딘 (Dodine)Positive9.46287.4287.22284351
5737
9디노테퓨란 (Dinotefuran)Positive4.40202.2202.120312917
11317
10디메토에이트 (Dimethoate)Positive5.56229.2228.923012527
19913
11데메톤-S (Demeton-S)Positive7.92258.3258.02598917
6147
데메톤-S-설폰 (Demeton-S-sulfone)Positive5.71290.3290.029123521
9929
데메톤-S-설폭사이드 (Demeton-S-sulfoxide)Positive5.62274.3274.027514129
10933
디설포톤 (Disulfoton)Positive10.93274.4274.02758921
6145
디설포톤 설폰 (Disulfoton sulfone)Positive7.15306.4306.030712523
15317
디설포톤 설폭사이드 (Disulfoton sulfoxide)Positive7.04290.4290.029118519
12941
12데메톤-S-메틸 (Demeton-S-methyl)Positive6.65230.3230.02318919
6143
13데메톤-S-메틸-설폰 (Demeton-S-methyl-sulfone)Positive4.98262.3262.026316921
10937
14디우론 (Diuron)Positive7.45233.1232.02337237
4631
15디클로르보스 (Dichlorvos)Positive6.41221.0219.922110923
12721
16디클로슐람 (Diclosulam)Positive6.87406.2404.940616133
12583
17디플루벤주론 (Diflubenzuron)Positive9.41310.7310.031115819
14145
18레나실 (Lenacil)Positive7.30234.3234.123515323
13645
19레피멕틴 A3* (Lepimectin A3)Positive13.70705.8705.372854931
53139
레피멕틴 A4* (Lepimectin A4)Positive14.19719.9719.374256333
54539
20루페뉴론 (Lufenuron)Negative11.99511.1509.950933918
32628
21리뉴론 (Linuron)Positive8.13249.1248.024916023
18219
22만데스트로빈 (Mandestrobin)Positive9.98313.4313.131419215
13239
23만디프로파미드 (Mandipropamid)Positive9.82411.9411.141236625
38421
24말라티온 (Malathion)Positive8.57330.4330.033112717
12539
25말라옥손 (Malaoxon)Positive6.55314.3314.031512717
9935
26메빈포스 (Mevinphos)Positive5.85224.1224.022512723
19313
27메소트리온* (Mesotrione)Positive5.74339.3339.034022825
10441
28메카밤 (Mecarbam)Positive9.22329.4329.033022713
19919
29메타미도포스 (Methamidophos)Positive2.38141.1141.01429421
12519
30메타미트론 (Metamitron)Positive5.57202.2202.020310431
17523
31메타미포프 (Metamifop)Positive11.46440.9440.044128827
12341
32메타벤즈티아주론 (Methabenzthiazuron)Positive7.33221.3221.022216523
15045
33메타플루미존(E) (Metaflumizone E)Positive11.68506.4506.150717837
28735
메타플루미존(Z) (Metaflumizone Z)Positive10.89506.4506.117837
28735
34메토미노스트로빈 (Metominostrobin)Positive7.56284.3284.128519427
19619
35메토밀 (Methomyl)Positive4.90162.2162.01638813
10613
36메토브로뮤론 (Metobromuron)Positive7.24259.1258.025917023
14823
37메톡시페노자이드 (Methoxyfenozide)Positive8.52368.5368.236914923
31311
38메톨카브 (Metolcarb)Positive6.30165.2165.016610917
9441
39메트라페논 (Metrafenone)Positive10.70409.3408.040920923
22729
40메트코나졸 (Metconazole)Positive10.25319.8319.13207043
12561
41메티오카브 (Methiocarb)Positive8.16225.3225.022616913
12231
42메페나셋 (Mefenacet)Positive8.78298.4298.029914819
12035
43메펜트리플루코나졸 (Mefentrifluconazole)Positive10.04397.8397.03987051
18241
44메포스폴란 (Mephosfolan)Positive6.40269.3269.027016821
14021
45모노크로토포스 (Monocrotophos)Positive5.00223.2223.022419311
12721
46바미도티온 (Vamidothion)Positive5.47287.3287.028814617
11831
47바이오레스메트린* (Bioresmethrin)Positive14.02338.4338.133917121
14335
48발리페날레이트 (Valifenalate)Positive8.77398.9398.139915545
11635
49버놀레이트 (Vernolate)Positive10.82203.3203.120412815
8619
50베나락실 (Benalaxyl)Positive10.06325.4325.132614829
9151
51벤디오카브 (Bendiocarb)Positive6.54223.2223.022410925
16713
52벤설라이드 (Bensulide)Positive9.51397.5397.039831415
35611
53벤조비사이클론 (Benzobicyclon)Positive8.41467.0446.044725735
22951
54벤족시메이트 (Benzoximate)Positive10.70363.8363.036419911
10535
55벤티아발리카브아이소프로필(R) (Benthiavalicarb-isopropyl R)Positive8.59381.5381.138218043
19727
벤티아발리카브아이소프로필(S) (Benthiavalicarb-isopropyl S)Positive8.81381.5381.118043
19727
56뷰토카복심 (Butocarboxim)Positive6.03190.3190.02137519
15615
57브로마실 (Bromacil)Positive6.58261.1260.026120521
18841
58비스트리플루론 (Bistrifluron)Negative12.60446.7446.044526234
18680
59비터타놀* (Bitertanol)Positive10.27337.4337.133826913
9921
60빅사펜 (Bixafen)Positive9.53414.2413.041439421
26633
61사이목사닐 (Cymoxanil)Positive10.70198.2198.019918425
14137
62사이아조파미드 (Cyazofamid)Positive9.18324.8324.032510821
26113
63사이안트라닐리프롤 (Cyantraniliprole)Positive6.78473.7472.047528623
11281
64사이에노피라펜 (Cyenopyrafen)Positive12.87393.5393.239431035
25445
65사이클라닐리프롤 (Cyclaniliprole)Positive9.46602.1598.960028421
112113
66사이클로프로트린 (Cycloprothrin)Positive13.03482.4481.049918145
25719
67사이클로에이트 (Cycloate)Positive10.97215.4215.12168323
13419
68사이프로코나졸, 이성질체1 (Cyproconazole, Isomer1)Positive8.55291.8291.12927035
12539
사이프로코나졸, 이성질체2 (Cyproconazole, Isomer2)Positive8.82291.8291.12927035
12539
69사이플루메토펜 (Cyflumetofen)Positive11.38447.5447.146517333
24919
70사플루페나실 (Saflufenacil)Positive7.78500.9500.050119859
34935
71설펜트라존 (Sulfentrazone)Positive6.64387.2385.940438719
30735
72설폭사플로르 (Sulfoxaflor)Positive5.66277.3277.027817413
15439
73설프로포스 (Sulprofos)Positive12.64322.4322.032321921
13941
74세닥산-시스 (Sedaxane-cis)Positive8.68331.4331.133229226
15938
세닥산-트랜스 (Sedaxane-trans)Positive9.17331.4331.129226
15938
75세크뷰메톤 (Secbumeton)Positive7.21225.3225.122617027
10039
76세톡시딤 (Sethoxydim)Positive11.90327.5327.132817825
28217
77스피네토람-J (Spinetoram-J)Positive10.46748.0747.474814237
9899
스피네토람-L (Spinetoram-L)Positive11.09760.0759.476014235
9899
78스피노신 A (Spinosyn A)Positive9.62732.0731.473214237
9897
스피노신 D (Spinosyn D)Positive10.23746.0745.474614237
9897
79스피로디클로펜 (Spirodiclofen)Positive13.01411.3410.141131317
21347
80스피로테트라맷* (Spirotetramat)Positive8.93373.4373.137430223
21645
스피로테트라맷-엔올* (Spirotetramat-enol)Positive6.93301.4301.130221637
11747
81시마진 (Simazine)Positive6.62201.7201.020213225
12425
82시아나진 (Cyanazine)Positive6.27240.7240.024121425
10443
83아메톡트라딘 (Ametoctradin)Positive10.59275.4275.227617651
14949
84아미설브롬 (Amisulbrom)Positive11.27466.3464.946622727
14867
85아미트라즈* (Amitraz)Positive13.47293.4293.129416321
12241
86아바멕틴* (아바멕틴 B1a) (Abamectin B1a)Positive13.86873.1872.489130531
56819
87아세타미프리드 (Acetamiprid)Positive5.51222.7222.022312629
9953
88아세페이트 (Acephate)Positive3.60183.2183.018414311
9529
89아이소프로튜론 (Isoproturon)Positive7.36206.3206.12077231
13431
90아이속사벤 (Isoxaben)Positive8.33332.4332.133316523
10777
91아이속사티온 (Isoxathion)Positive10.58313.3313.031428613
17019
92아자메티포스 (Azamethiphos)Positive6.36324.7323.932511247
13935
93아족시스트로빈 (Azoxystrobin)Positive7.88403.4403.140437221
34435
94아진포스메틸 (Azinphos-methyl)Positive7.83317.3317.031813219
16019
95알디카브 (Aldicarb)Positive6.09190.3190.020811611
8923
96알레트린 (Allethrin)Positive11.97302.4302.130313515
9153
97에마멕틴 벤조에이트 (에마멕틴 B1a) (Emamectin B1a)Positive11.25886.1885.588682111
15843
98에스프로카브 (Esprocarb)Positive11.87265.4265.12669133
6579
99에타복삼 (Ethaboxam)Positive6.96320.4320.032118331
20035
100에토펜프록스 (Etofenprox)Positive14.84376.5376.239417721
13533
101에트림포스 (Etrimfos)Positive10.22292.3292.029312533
26521
102에티오펜카브 (Ethiofencarb)Positive6.96225.3225.02261699
10723
103엑스엠씨 (XMC)Positive6.99179.2179.018012315
7779
104오리사스트로빈 (Orysastrobin)Positive8.51391.4391.139220521
11631
105오리잘린 (Oryzalin)Negative9.06346.4346.034528132
14736
106오메토에이트 (Omethoate)Positive4.20213.2213.021412529
18315
107오퓨레이스 (Ofurace)Positive6.52281.7281.028216031
25417
108옥사디아길 (Oxadiargyl)Positive10.37341.2340.034115139
22237
109옥사밀 (Oxamyl)Positive4.67219.3219.02379011
7229
옥사밀 옥심 (Oxamyl oxime)Positive4.17162.0162.21637217
9023
110옥사지클로메폰 (Oxaziclomefone)Positive11.50376.3375.037619019
16139
111옥사티아피프롤린 (Oxathiapiprolin)Positive8.36539.5539.154050043
16343
112옥시데메톤메틸 (Oxydemeton-methyl)Positive4.80246.3246.024716921
10939
113옥시카복신 (Oxycarboxin)Positive5.75267.3267.026817521
14731
114유니코나졸 (Uniconazole)Positive9.19291.8291.12927041
12539
115육-비에이 (Benzyladenine, 6-Benzyl aminopurine)Negative6.04225.2225.122413330
10642
116이나벤파이드 (Inabenfide)Positive8.03338.8338.03398049
32123
117이마잘릴 (Imazalil)Positive6.65297.2296.029715933
6935
118이미다클로프리드 (Imidacloprid)Positive5.31255.7255.025620921
21217
119이미벤코나졸 (Imibenconazole)Positive11.80411.7409.941112550
17128
120이미시아포스 (Imicyafos)Positive6.17304.3304.130520131
23525
121이프로발리카브 (Iprovalicarb)Positive8.97320.4320.232111935
20315
122이프펜카바존 (Ipfencarbazone)Positive9.95427.2426.042719817
15631
123카바릴 (Carbaryl)Positive6.77201.2201.020214515
12739
124카베타마이드 (Carbetamide)Positive6.27236.3236.123719211
12023
125카벤다짐 (Carbendazim)Positive5.01191.2191.019216025
13241
126카보퓨란* (Carbofuran)Positive6.56221.3221.122216517
12329
3-하이드록시카보퓨란* (3-hydroxycarbofuran)Positive5.53237.3237.123818115
16323
127카펜스트롤 (Cafenstrole)Positive8.67350.4350.135110019
7241
128카프로파마이드 (Carpropamide)Positive9.97334.7333.033413931
19617
129크로톡시포스 (Crotoxyphos)Positive8.24314.3314.033221113
12735
130퀴노클라민 (Quinoclamine)Positive8.39207.6207.020815113
10923
131크로마페노자이드 (Chromafenozide)Positive8.90394.5394.239517521
33911
132크루포메이트 (Crufomate)Positive9.40291.7291.029223627
20437
133클로란트라닐리프롤 (Chlorantraniliprole)Positive7.65483.1480.948445327
28619
134클로로벤주론 (Chlorobenzuron)Positive9.81309.1308.030915621
13943
135클로로톨루론 (Chlorotoluron)Positive7.11212.7212.02137239
10443
136클로록수론 (Chloroxuron)Positive8.74290.7290.02917247
11163
137클로르펜빈포스(E) (Chlorfenvinphos E)Positive10.10359.6357.935915517
9945
클로르펜빈포스(Z) (Chlorfenvinphos Z)Positive10.50359.6357.915517
9945
138클로르플루아주론 (Chlorfluazuron)Positive13.14540.7538.954038331
15833
139클로리다존 (Chloridazone)Positive5.61221.6221.022210433
7753
140클로메프로프 (Clomeprop)Positive11.72324.2323.032412027
14821
141클로티아니딘 (Clothianidin)Positive7.34249.7249.02509347
13125
142클로펜테진 (Clofentezine)Positive10.94303302.030313821
10255
143터부틸라진 (Terbuthylazine)Positive8.33229.7229.123017421
10443
144터부포스 (Terbufos)Positive11.93288.4288.028910313
2339
터부포스 옥손 (Terbufos oxon)Positive8.98272.4272.027310313
11539
터부포스 옥손 설폰 (Terbufos oxon sulfone)Positive6.21304.4304.030523119
9545
터부포스 옥손 설폭사이드 (Terbufos oxon sulfoxide)Positive6.02288.4288.028917115
11541
터부포스 설폰 (Terbufos sulfone)Positive8.01320.4320.03219755
11539
터부포스 설폭사이드 (Terbufos sulfoxide)Positive7.97304.4304.030518715
13139
145테닐클로르 (Thenylchlor)Positive9.11323.8323.032412717
9757
146테부티우론 (Tebuthiuron)Positive6.64228.3228.122917225
11635
147테부페노자이드 (Tebufenozide)Positive9.47352.5352.235313325
29711
148테부플로퀸 (Tebufloquin)Positive9.92289.3289.129024823
23257
테부플로퀸 M1 (Tebufloquin M1)Positive7.97247.3247.124823247
19235
149테트라닐리프롤 (Tetraniliprole)Negative7.39554.9544.154313724
10978
150테프랄록시딤 (Tepraloxydim)Positive6.77341.8341.134225019
16629
151테플루벤주론 (Teflubenzuron)Negative11.89381.1379.937933916
35910
152톨펜피라드 (Tolfenpyrad)Positive11.93383.9383.138419737
15459
1532,3,5-트리메타카브 (2,3,5-Trimethacarb)Positive7.46193.2193.119413717
12235
3,4,5-트리메타카브 (3,4,5-Trimethacarb)Positive7.46193.2193.113717
12235
154트리뷰포스 (Tribufos)Positive13.50314.5314.031516921
5737
155트리사이클라졸 (Tricyclazole)Positive5.90189.2189.019013637
10947
156트리아자메이트 (Triazamate)Positive9.00314.4314.13157235
22617
157트리아파몬 (Triafamone)Positive6.60406.3406.040724533
16061
158트리클로르폰***** (Trichlorfon)Positive5.58257.4255.925710927
22117
159트리티코나졸 (Triticonazole)Positive9.01317.8317.13187053
12545
160트리포린* (Triforine)Positive7.45435431.943539037
21545
161트리플루뮤론 (Triflumuron)Positive10.35358.7358.035915623
13945
162티디아주론 (Thidiazuron)Positive6.45220.3220.022110219
12825
163티아디닐 (Tiadinil)Negative8.75267.7267.02667138
23816
164티아메톡삼 (Thiamethoxam)Positive4.98291.7291.029221117
13229
165티아벤다졸 (Thiabendazole)Positive5.36201.2201.020217535
13143
166티아조피르 (Thiazopyr)Positive9.93396.4396.039737727
33531
167티아클로프리드 (Thiacloprid)Positive5.71254.7252.025312629
9051
168티오디카브****** (Thiodicarb)Positive6.76354.5354.03558827
10821
169티오벤카브 (Thiobencarb)Positive10.72257.8257.025812525
8965
170티오파네이트메틸 (Thiophanate-methyl)Positive6.45342.4342.034315120
31110
171파목사돈 (Famoxadone)Positive10.13374.4374.139223823
23927
172페나미포스 (Fenamiphos)Positive9.41303.4303.130421731
20247
페나미포스설폰 (Fenamiphos sulfone)Positive6.53335.4335.033626627
30821
페나미포스설폭사이드 (Fenamiphos sulfoxide)Positive6.43319.4319.132023335
17133
173페나자퀸 (Fenazaquin)Positive13.52306.4306.130716119
14759
174페노트린-시스 (Phenothrin-cis)Positive14.39350.5350.135118331
12887
페노트린-트랜스 (Phenothrin-trans)Positive14.55350.5350.118331
12887
175페녹사프로프-에틸 (Fenoxaprop-ethyl)Positive11.50361.8361.036228825
11935
176페녹슐람 (Penoxsulam)Positive6.71483.4483.048419539
16449
177페녹시카브 (Fenoxycarb)Positive9.56301.3301.130211615
25617
178페림존(E) (Ferimzone E)Positive7.55254.3254.125513227
12429
페림존(Z) (Ferimzone Z)Positive8.02254.3254.125513227
12429
179페뷰레이트 (Pebulate)Positive10.83203.3203.120412817
7219
180펜메디팜 (Phenmedipham)Positive7.59300.3300.130113627
16813
181펜사이큐론 (Pencycuron)Positive10.61328.8328.132912535
21823
182펜설포티온 (Fensulfothion)Positive7.28308.4308.030915733
23531
183펜트라자마이드 (Fentrazamide)Positive9.92349.8349.135015415
7235
184펜피록시메이트 (Fenpyroximate)Positive13.02421.5421.242236623
13841
185펜헥사미드 (Fenhexamid)Positive8.92302.2301.03029731
14343
186포레이트 (Phorate)Positive10.71260.4260.02617523
19913
포레이트옥손 (Phorate oxon)Positive7.65244.3244.02457517
4741
포레이트옥손설폰 (Phorate oxon sulfone)Positive5.70276.3276.027711139
12721
포레이트설폰 (Phorate sulfone)Positive7.19292.3292.029317117
11533
포레이트옥손설폭사이드 (Phorate oxon sulfoxide)Positive5.54260.3260.026111129
9731
포레이트설폭사이드 (Phorate sulfoxide)Positive7.06276.4276.027719913
14329
187포메사펜 (Fomesafen)Negative8.05438.8437.943719550
22248
188포스티아제이트 (Fosthiazate)Positive6.99283.3283.028410429
22815
189포스폴란 (Phosfolan)Positive5.98255.3255.02562285
615
190포클로르페뉴론 (Forchlorfenuron)Positive7.34247.7247.024812925
9347
191폭심 (Phoxim)Positive10.54298.3298.029912917
7747
192퓨라티오카브* (Furathiocarb)Positive11.66382.5382.138319523
25217
193프로메카브 (Promecarb)Positive8.40207.3207.120815113
10923
194프로베나졸 (Probenazole)Positive5.61223.2223.022451113
63111
195프로설포카브 (Prosulfocarb)Positive11.43251.4251.12529137
12817
196프로퀴나지드 (Proquinazid)Positive13.35372.2372.037333121
28933
197프로파모카브 (Propamocarb)Positive4.10188.3188.118910223
7433
198프로파자이트* (Propargite)Positive12.69350.5350.136823121
17547
199프로파퀴자포프* (Propaquizafop)Positive11.83443.9443.144437123
29931
200프로폭서 (Propoxur)Positive6.52209.2209.121016811
15311
201플로니카미드 (Flonicamid)Positive4.96229.2229.023020327
9853
202플루디옥소닐 (Fludioxonil)Positive8.20248.2248.026622921
15847
203플루리돈 (Fluridone)Positive7.76329.3329.133031041
11589
204플루벤디아마이드 (Flubendiamide)Positive9.61682.4682.068340815
27447
205플루설파마이드 (Flusulfamide)Negative10.27415.2413.941317146
17950
206플루아지남 (Fluazinam)Negative11.96465.1463.946341628
39824
207플루오메투론 (Fluometuron)Positive6.96232.2232.023316035
14047
208플루오피콜라이드 (Fluopicolide)Positive8.53383.6381.938317331
10989
209플루톨라닐 (Flutolanil)Positive8.40323.3323.132426223
24223
210플루트리아폴 (Flutriafol)Positive7.17301.3301.13027045
12339
211플루티아셋-메틸 (Fluthiacet-methyl)Positive9.81403.9403.040427439
21553
212플루페나셋 (Flufenacet)Positive9.11363.3363.036415227
12447
213플루페녹수론 (Flufenoxuron)Negative12.58488.8488.048746712
30426
214플루폭삼 (Flupoxam)Positive9.48460.8460.046144437
12369
215플루피라디퓨론 (Flupyradifurone)Positive13.35288.7288.028927231
21647
216플룩사메타마이드 (Fluxametamide)Positive12.17474.3473.047440029
16051
217피디플루메토펜 (Pydiflumetofen)Positive10.63426.7425.042619351
16637
218피라족시펜 (Pyrazoxyfen)Positive10.02403.3402.04039161
10529
219피라졸레이트 (Pyrazolate)Positive10.60439.3438.043917325
14577
220피라지플루미드 (Pyraziflumid)Positive8.93379.3379.038014741
17527
221피라클로닐 (Pyraclonil)Positive6.94314.8314.131516937
27623
222피라클로스트로빈 (Pyraclostrobin)Positive10.36387.8387.038816333
19417
223피로퀼론 (Pyroquilon)Positive6.43173.2173.017413231
11743
224피리다벤 (Pyridaben)Positive13.33364.9364.136514731
30931
225피리다펜티온 (Pyridaphenthion)Positive8.67340.3340.034118933
20531
226피리데이트* (Pyridate)Positive14.08378.9378.137920725
35115
227피리미디펜 (Pyrimidifen)Positive11.82377.9377.137818431
15045
228피리미설판 (Pyrimisulfan)Positive7.52419.4419.042037023
38821
229피리벤족심 (Pyribenzoxim)Positive11.84609.6609.161041317
18047
230피리벤카브 (Pyribencarb)Positive7.98361.8361.136223925
20737
KIE-9749 (KIE-9749)Positive7.45361.8361.123927
20741
231피리뷰티카브 (Pyributicarb)Positive12.33330.4330.133110839
13335
232피리오페논 (Pyriofenone)Positive10.86365.8365.136618431
20933
233피리프록시펜* (Pyriproxyfen)Positive12.44321.4321.13229621
18531
234피리플루퀴나존 (Pyrifluquinazon)Positive8.68464.3464.146542327
10745
235피메트로진* (Pymetrozine)Positive4.25217.2217.021810527
7955
236피카뷰트라족스 (Picarbutrazox)Positive9.40409.4409.141031019
10735
TZ-1E (TZ-1E)Positive9.22409.4409.131019
10735
237피콜리나펜 (Picolinafen)Positive11.87376.3376.037723843
25631
238피페로포스 (Piperophos)Positive10.93353.5353.135417129
25519
239피플루뷰마이드 (Pyflubumide)Positive12.11535.5535.253615527
11175
피플루뷰마이드-NH (Pyflubumide-NH)Positive11.35465.4465.146613739
11137
240헥사지논 (Hexazinone)Positive6.57252.3252.125317123
7143
241헥사코나졸 (Hexaconazole)Positive10.20314.2313.03147039
15943
242헥사플루뮤론 (Hexaflumuron)Negative11.07461.1459.945943918
27626

기울기 조건표

시간(분)A(%)B(%)
0.0955
1.0955
3.04060
13.00100
18.00100
18.1955
25.0955
이 조건으로 Core-Shell 전환 계산하기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.

고시 원문 보기 (축자)
가) 컬럼: C18계 컬럼(2.1 mm × 100 mm, 2.7 μm) 또는 이와 등등한 것
나) 이동상
(1) 이동상 A: 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 수용액
(2) 이동상 B: 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 메탄올
[표 1]
다) 이동상 유량: 0.2 mL/분
라) 컬럼온도: 40℃
마) 주입량: 2 μL
바) 분석대상(242종) 물질의 조건
[표 2]
3) 정량한계

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 C18USP L1 상당

약전 일반명 '액체크로마토그래프용옥타데실실릴실리카겔'(USP 분류로는 L1 상당)에 해당. 약전은 브랜드를 지정하지 않으므로 각조가 기재한 물리 사양(치수·입자경 등)과 KP 통칙·일반시험법의 조정 허용범위 안에서 해당 상을 충족하는 C18을 선택할 수 있다 — 선택 기준은 시스템적합성(분리도·테일링·RSD) 통과 용이성과 재현성이다.

함께 보기

Core-Shell 전환 솔루션 (동등성 검증·계산기)타사 컬럼 대체 솔루션컬럼 추천 도구저분자 API 분석 솔루션컬럼 보호·수명 관리

신판— 2027.1.1.부터 적용

분석조건2건

분석조건 (3)

GC신판 · 2027.1.1.부터7.1.2.2FD-다성분-시험법-제2법-x3

원문 표제 단서: 기체크로마토그래프-질량분석기

칼럼
GC-5 · USP G27

DB-5MS

안지름 0.25 mm · 길이 30 m · 막두께 0.25 μm

칼럼온도
90℃에서 시험용액을 주입하여 20℃/분의 비율로 180℃까지 온도를 상승시키고 5℃/분의 비율로 300℃까지 상승시켜 5분간 유지한다.
이동상
  • 헬륨(He)
유량
1.2 mL/분
주입방법
라) 주입 방법: Splitless mode
질량분석(MS) 조건 보기 (2항목)
인터페이스 온도
마) 인터페이스 온도: 300℃
전이표
분석성분 (Compound)머무름 시간 (분)분자량 (MW)관측질량 (Exact mass)선구이온 (Precursor ion, m/z)생성이온 (Product ion, m/z)충돌 에너지 (Colllision energy, eV)
1노나클로르-시스 (Nonachlor-cis)15.59444.2439.740730030
40930015
노나클로르-트랜스 (Nonachlor-trans)13.65444.2439.740730015
40930025
2뉴아리몰 (Nuarimol)17.25314.7314.013911115
1075230
3니트로탈-아이소프로필 (Nitrothal-isopropyl)11.60295.3295.119412020
23619410
4다이아지논 (Diazinon)8.64304.3304.11999315
13510
5다이알레이트 (Diallate)7.78270.2269.023415020
19215
6다이알리포르 (Dialifor)21.08393.8393.03579725
2088925
7데스메트린 (Desmetryn)9.69213.3213.12135820
1985
8델타메트린 (Deltamethrin)26.58505.2502.92539315
17427
9디니코나졸 (Diniconazole)15.49326.2325.026813635
23215
10디니트라민 (Dinitramine)8.86322.2322.026124110
19520
11p,p’-디디디* (p,p’-DDD)15.62320.0317.923716525
23516525
p,p’-디디이* (p,p’-DDE)14.26318.0315.924617630
24817630
o,p’-디디티* (o,p’-DDT)15.70354.5351.923716525
23516525
p,p’-디디티* (p,p’-DDT)16.87354.5351.923716525
23516525
12디메타메트린 (Dimethametryn)12.35255.4255.12121225
9420
13디메타클로르 (Dimethachlor)9.71255.7255.113410515
19714810
14디메테나미드 (Dimethenamid)9.72275.8275.015411110
23015410
15디메토모르프(E)* (Dimethomorph E)27.26387.9387.130116512
38730112
디메토모르프(Z)* (Dimethomorph Z)27.85387.9387.138730112
30116512
16디메티핀* (Dimethipin)8.23210.3210.0124765
118585
17디메틸빈포스(E) (Dimethylvinphos E)10.83331.5329.929510920
29710920
디메틸빈포스(Z) (Dimethylvinphos Z)11.22331.5329.929510920
29710920
18디메피퍼레이트 (Dimepiperate)12.77263.4263.11451125
6915
192,6-디아이피엔* (2,6-DIPN, (2,6-Diisopropylnaphthalene)8.05212.3212.121219715
19715510
20디에타틸-에틸 (Diethatyl-ethyl)13.61311.8311.118816010
13040
21디에토펜카브 (Diethofencarb)11.20267.3267.12672255
22516810
22디옥사티온 (Dioxathion)8.42456.5456.02709730
125975
23디코폴 (Dicofol)11.63370.5367.91397535
11115
24디크로토포스 (Dicrotophos)7.22237.2237.01279515
1931275
25디클로란** (Dicloran)8.00207.0205.916012410
20617615
26디클로르미드 (Dichlormid)4.67208.1207.01721085
1665610
27디클로베닐 (Dichlobenil)4.63172.0170.917313610
17113630
28디클로뷰트라졸 (Diclobutrazol)14.60328.2327.027216110
27015915
29디클로펜티온** (Dichlofenthion)9.70315.1313.927922310
22320515
30디클로포프메틸 (Diclofop-methyl)17.42341.2340.034025310
25316240
31디클로플루아니드* (Dichlofluanid)10.92333.2331.9200455
4425
32디티오피르 (Dithiopyr)10.37401.4401.035428615
3065
33디페노코나졸 (Difenoconazole)26.25406.3405.032526715
32326515
34디페닐아민 (Diphenylamine)6.94169.2169.016816720
16916815
35디펜아미드 (Diphenamid)11.82239.3239.116716530
15220
36디플루페니칸 (Diflufenican)17.49394.3394.026621825
23815
37렙토포스 (Leptophos)19.71412.1409.837736225
1717725
38린단** (Lindane, γ-BHC)8.48290.8287.818114515
2171815
39마이클로뷰타닐 (Myclobutanil)14.41288.8288.117912515
1525
40메탈락실 (Metalaxyl)10.24279.3279.123414620
2491905
41메토프로트린 (Methoprotryn)14.68271.4271.125617025
21215
42메톡시클로르 (Methoxychlor)18.79345.6344.022714140
16925
43메톨라클로르 (Metolachlor)11.11283.8283.116213315
23816210
44메트리뷰진 (Metribuzin)9.86214.3214.01988220
5530
45메티다티온 (Methidathion)13.06302.3301.91455815
855
46메틸트리티온 (Methyl trithion)15.30314.8313.91254715
15712135
47메파니피림 (Mepanipyrim)13.61223.3223.122222120
22210
48메펜피르-디에틸 (Mefenpyr-diethyl)17.93373.3372.029925310
25319020
49메프로닐 (Mepronil)16.10269.3269.12699140
11915
50모노리누론 (Monolinuron)8.23214.6214.01269915
214615
51몰리네이트* (Molinate)6.18187.3187.11871265
126985
52베노다닐 (Benodanil)15.93323.1322.923120320
7625
53벤조일프로프-에틸 (Benzoylprop-ethyl)17.99366.2365.029210510
1057710
54벤퓨러세이트 (Benfuresate)9.66256.3256.02561635
1631215
55벤플루라린 (Benfluralin)7.23335.3335.129216020
26410
56보스칼리드 (Boscalid)23.62343.2342.01407625
11210
57부피리메이트 (Bupirimate)14.51316.4316.127319310
10810
58뷰타클로르 (Butachlor)13.37311.9311.123716010
17614710
59뷰타페나실 (Butafenacil)22.62474.8474.033118020
12440
60뷰트랄린 (Butralin)11.68295.3295.126617420
22015
61뷰틸레이트** (Butylate)5.18217.4217.3156575
1465710
62뷰프로페진 (Buprofezin)14.51305.4305.11725715
17513215
63브로모뷰타이드 (Bromobutide)9.87312.3311.011811710
23217610
64브로모포스-메틸 (Bromophos-methyl)11.80366.0363.833131620
32931415
65브로모포스-에틸 (Bromophos-ethyl)13.07394.0391.830321130
6330
66브로모프로필레이트 (Bromopropylate)18.61428.1425.934318515
33918315
67α-비에이치시 (α-BHC)7.75290.8287.818114515
2171815
β-비에이치시 (β-BHC)8.2718114515
2171815
δ-비에이치시 (δ-BHC)9.1318114515
2171815
68비페녹스* (Bifenox)19.13342.1341.034131110
18920
69비페닐 (Biphenyl)4.94154.2154.115415315
15315215
70비펜트린 (Bifenthrin)18.60422.9422.118116615
16530
71빈클로졸린 (Vinclozolin)9.95286.1284.919814515
18712420
72사이퍼메트린* (Cypermethrin)23.83416.3415.01659110
1631275
73사이프라진 (Cyprazine)9.77227.7227.017010915
21210930
74사이프로디닐 (Cyprodinil)12.18225.3225.122522410
22420825
75사이플루트린 (Cyfluthrin)23.23434.3433.022620610
1631275
76사이플루페나미드 (Cyflufenamid)14.84412.4412.122320312
1888840
77γ-사이할로트린* (γ-Cyhalothrin)20.48449.9449.12081815
19714110
λ-사이할로트린* (λ-Cyhalothrin)20.872081815
19714110
78사이할로포프뷰틸**** (Cyhalofop-butyl)20.19357.4357.125612020
22910915
79설포텝 (Sulfotep)7.31322.3322.020214610
32214625
80스피로메시펜 (Spiromesifen)17.97370.5370.227220910
25410
81스피록사민 (Spiroxamine)10.03297.5297.2100725
1981265
82시메코나졸 (Simeconazole)10.05293.4293.112110115
7535
83시메트린 (Simetryn)10.15213.3213.121317010
18510
84시아노포스 (Cyanophos)8.53243.2243.0125795
24310910
85신메틸린 (Cinmethylin)10.34274.4274.11541115
16910710
86실라플루오펜 (Silafluofen)24.54408.6408.11799110
28625810
87아닐로포스 (Anilofos)19.09367.8367.022615715
1845
88아라마이트 (Aramite)14.94334.9334.11876510
1856310
89아메트린 (Ametryn)10.25227.3227.12271855
17010
90아세토클로르* (Acetochlor)9.82269.8269.122314610
13220
에이치이엠에이* (HEMA(2-(1-hydroxyl-ethyl)-6-methyl-aniline))5.10151.2151.015111740
13220
이엠에이* (EMA(2-ethyl-6-methylaniline))3.99135.2135.11207720
13512010
91아스폰 (Aspon)11.01378.4378.021111510
9735
92아이소티아닐 (Isotianil)16.74298.1296.91809120
29718015
93아이소펜포스 (Isofenphos)12.41345.4345.121312120
1855
94아이소펜포스-메틸 (Isofenphos-methyl)11.98331.4331.11999330
12115
95아이소프로카브 (Isoprocarb)6.04193.2193.113612110
7730
96아이소프로티올레인 (Isoprothiolane)14.04290.4290.01898920
14510
97아이소프로파린 (Isopropalin)11.94309.4309.123816510
2802385
98아이소피라잠 (Isopyrazam)21.11359.4359.135915940
15913910
99아이속사디펜-에틸 (Isoxadifen-ethyl)16.38295.3295.12222055
20420
100아자코나졸 (Azaconazole)14.63300.1299.021917515
21717315
101아진포스-에틸 (Azinphos-ethyl)20.94345.4345.01601325
1327715
102아크리나트린* (Acrinathrin)20.48541.4541.12081815
2899310
103아트라진 (Atrazine)8.20216.7215.021520010
5815
104알드린** (Aldrin)11.31364.9361.826319340
19140
디엘드린** (Dieldrin)14.42380.9377.826319340
26519340
105알라클로르 (Alachlor)10.05269.8269.118816010
16013030
106알리도클로르 (Allidochlor)4.21173.6173.0134565
132565
107에디펜포스* (Edifenphos)16.60310.4310.017310910
20110915
108에타코나졸 (Etaconazole)15.58328.2327.017310925
24517320
109에탈플루랄린 (Ethalfluralin)7.02333.3333.027620215
3162765
110에토퓨메세이트 (Ethofumesate)10.76286.3286.016110510
20713710
111에토프로포스 (Ethoprophos)6.98242.3242.01581145
9720
112에톡사졸 (Etoxazole)18.86359.4359.130027025
20417610
113에트리디아졸 (Etridiazole)5.38247.5245.921114025
18310
114에티온 (Ethion)15.64384.5383.923112925
17510
115에티클로제이트 (Ethychlozate)12.45238.7238.016513810
10215
116에폭시코나졸 (Epoxiconazole)17.81329.8329.019211125
13815
117α-엔도설판 (α-Endosulfan)13.56406.9403.824120615
20517015
β-엔도설판 (β-Endosulfan)15.44406.9403.820517015
20717215
엔도설판 설페이트 (Endosulfan sulfate)16.67422.9419.827423725
27223720
118엔드린 (Endrin)14.42380.9377.826319340
19135
δ-케토-엔드린 (δ-keto-Endrin)18.26380.9377.831728110
24520
119엠지케이-264 (MGK-264)12.25275.4275.1164675
9810
120오쏘페닐페놀* (Ortho-phenyl phenol)5.98170.2170.016911530
14115
121옥사디아존 (Oxadiazon)14.29345.2344.01751125
25817515
122옥사딕실 (Oxadixyl)15.55278.3278.116311725
1325
123옥시플루오르펜 (Oxyfluorfen)14.46361.7361.030022320
36130020
124이사조포스 (Isazofos)8.95313.7313.02571625
20816610
125이프로디온* (Iprodione)18.25330.2329.03145620
24510
126이프로벤포스 (Iprobenfos)9.32288.3288.02049110
12135
127이프코나졸 (Ipconazole)20.54333.9333.11259920
8920
128이피엔 (EPN)18.53323.3323.01691415
1577730
129이피티씨 (EPTC)4.67189.3189.1132905
1891285
130인다노판 (Indanofan)19.03340.8340.01397535
15910315
131인독사카브** (Indoxacarb)26.55527.8527.020310625
13415
132족사마이드 (Zoxamide)17.86336.6335.018715920
12330
133카두사포스 (Cadusafos)7.50270.4270.01599720
1589720
134카보페노티온 (Carbophenothion)16.51342.9341.93441595
3421575
135카복신 (Carboxin)14.54235.3235.023514310
8720
136카펜트라존에틸* (Carfentrazone-ethyl)16.43412.2411.034031210
31215120
137코마포스 (Coumaphos)22.10362.8362.02101825
22616310
138퀴날포스 (Quinalphos)12.64298.3298.014611810
9130
139퀴녹시펜 (Quinoxyfen)16.67308.1306.923720830
30723720
140퀴잘로포프에틸* (Quizalofop-ethyl)23.93372.8372.037229910
29925515
141퀸토젠 (Quintozene)8.37295.3292.824921410
29523720
142크레속심메틸 (Kresoxim-methyl)14.54313.4313.11318935
1168915
143클로로넵 (Chloroneb)5.79207.1205.91935330
19111315
144클로로벤질레이트 (Chlorobenzilate)15.33325.2324.025113910
13911110
145클로로탈로닐* (Chlorothalonil)8.85265.9263.826623120
17030
146클로로프로필레이트 (Chloropropylate)15.33339.2338.025113910
13911110
147클로르니트로펜 (Chlornitrofen)16.43318.5316.931728715
2361735
148클로르단-시스 (Chlordane-cis)13.55409.8405.737526620
37326620
클로르단-트랜스 (Chlordane-trans)13.15409.8405.737526620
37326620
149클로르벤시드** (Chlorbenside)13.14269.2267.926812510
1258915
150클로르부팜 (Chlorbufam)8.19223.7223.02235315
12715
151클로르에톡시포스 (Chlorethoxyfos)6.79336.0333.81539715
974735
152클로르탈-디메틸 (Chlorthal-dimethyl)11.30332.0329.929922125
30122325
153클로르티오포스 (Chlorthiophos)15.71361.2359.932526910
26920510
154클로르티온 (Chlorthion)11.60297.6296.91254710
29710910
155클로르페나피르 (Chlorfenapyr)14.79407.6405.924722715
32824720
156클로르펜손 (Chlorfenson)13.90303.2301.917511110
1117515
157클로르프로팜 (Chlorpropham)7.18213.7213.017112715
1539025
158클로르플루레놀-메틸 (Chlorflurenol-methyl)12.95274.7274.021715225
21515220
159클로르피리포스 (Chlorpyrifos)11.16350.6348.931425820
19917115
160클로르피리포스-메틸 (Chlorpyrifos-methyl)9.87322.5320.828627120
9320
161클로마존 (Clomazone)8.31239.7239.01258915
20410725
162클로졸리네이트 (Chlozolinate)12.36332.1331.03312595
25918810
163키노메티오네이트* (Chinomethionat)13.20234.3233.92342065
20614815
164터바실 (Terbacil)8.94216.7216.01607615
1618820
165터부메톤 (Terbumeton)8.31225.3225.116915410
21010020
166터부트린 (Terbutryn)10.70241.4241.11851705
2411850
167테부코나졸 (Tebuconazole)17.34307.8307.125012530
25212730
168테부펜피라드 (Tebufenpyrad)19.10333.9333.127617110
33317120
169테부피림포스 (Tebupirimfos)9.23318.4318.12762345
26113715
170테크나젠 (Tecnazene)6.61260.9258.821314225
21517925
171테트라디폰 (Tetradifon)19.47356.0353.822920110
15911120
172테트라메트린 (Tetramethrin)18.69331.4331.11647725
10715
173테트라코나졸 (Tetraconazole)11.47372.1371.033620440
21820
174테트라클로르빈포스 (Tetrachlorvinphos)13.27366.0363.832910925
33110925
175테플루트린 (Tefluthrin)8.95418.7418.017713720
12720
176톨클로포스메틸 (Tolclofos-methyl)10.07301.1299.92659330
25015
177트랄로메트린 (Tralomethrin) (Deltamethrin으로 분석)26.58665.0660.02539315
17427
178트리디판** (Tridiphane)10.37320.4317.817310930
18715915
179트리아디메폰 (Triadimefon)11.48293.8293.020811135
18110
트리아디메놀 (Triadimenol)12.75295.8295.11306525
1286520
180트리아조포스 (Triazophos)16.14313.3313.01611345
10615
181트리알레이트 (Tri-allate)9.13304.7303.026818410
22620
182트리플록시스트로빈 (Trifloxystrobin)16.65408.4408.11168915
22213010
183트리플루랄린 (Trifluralin)7.17335.3335.12642065
30626410
184트리플루미졸 (Triflumizole)12.81345.8345.020617915
2784315
185티오나진 (Thionazin)6.65248.2248.01929615
24814010
186티오메톤 (Thiometon)7.87246.3245.91254725
93635
187티플루자마이드 (Thifluzamide)14.32528.1525.819412525
16610
188파라티온 (Parathion)11.39291.3291.02918140
10910
189파라티온메틸 (Parathion-methyl)10.03263.2263.02637935
10915
190파클로부트라졸 (Paclobutrazol)13.33293.8293.123612510
1675
191퍼메트린-시스*** (Permethrin-cis)21.95391.3390.018316820
15510
퍼메트린-트랜스*** (Permethrin-trans)22.2016820
15510
192퍼탄 (Perthane)15.11307.3306.022316520
19320
193페나리몰 (Fenarimol)20.67331.2330.025113915
21910710
194페나미돈 (Fenamidone)18.91311.4311.126818020
23823710
195페노뷰카브 (Fenobucarb)6.67207.3207.112110315
1501215
196페노티오카브 (Fenothiocarb)13.42253.4253.1725610
160728
197페녹사닐** (Fenoxanil)15.02329.2328.018912510
15410
198페니트로티온 (Fenitrothion)10.71277.2277.02772605
10920
199펜디메탈린 (Pendimethalin)12.13281.3281.125216210
2080
200펜발러레이트, 이성질체 1* (Fenvalerate, Isomer 1)25.32419.9419.116712510
16912710
펜발러레이트, 이성질체 2* (Fenvalerate, Isomer 2)25.71419.9419.116712510
16912710
201펜뷰코나졸 (Fenbuconazole)22.85336.8336.11981295
1297820
202펜손 (Fenson)11.77268.7267.91417710
2687720
203펜코나졸 (Penconazole)12.33284.2283.024815730
19220
204펜클로르포스 (Fenchlorphos)10.33321.5319.928527020
24030
205펜클로림** (Fenclorim)7.75225.1223.918910410
22418920
206펜타클로로벤조니트릴 (Pentachlorobenzonitrile)8.46275.3272.827517930
24020
207펜토에이트 (Phenthoate)12.61320.4320.027412515
12110
208펜톡사존 (Pentoxazone)19.71353.8353.02877010
2857015
209펜티오피라드 (Penthiopyrad)15.54359.4359.130217720
17710120
210펜티온 (Fenthion)11.28278.3278.027810920
16920
211펜퓨람 (Fenfuram)9.02201.2201.020110925
1095320
212펜프로파트린*** (Fenpropathrin)18.92349.4349.126521010
8940
213펜프로피모르프 (Fenpropimorph)11.38303.5303.21287015
11010
214펜플루펜 (Penflufen)16.00317.4317.11418415
27414115
215펜피라자민 (Fenpyrazamine)20.80331.4331.123018810
11730
216포노포스 (Fonofos)8.66246.3246.02461375
10915
217포모티온 (Formothion)9.45257.3256.9126935
1709315
218포사론 (Phosalone)19.69367.8366.91821385
10215
219포스멧 (Phosmet)18.41317.3316.916013310
7730
220포스파미돈(E) (Phosphamidon E)8.67299.7299.026412710
12710915
포스파미돈(Z) (Phosphamidon Z)9.61299.7299.026412710
12710915
221프레틸라클로르 (Pretilachlor)14.05311.9311.116213220
2622025
222프로디아민 (Prodiamine)10.66350.3350.127525510
32127910
223프로메톤 (Prometon)8.07225.3225.11831685
21016810
224프로메트린 (Prometryn)10.33241.4241.122618410
24119910
225프로사이미돈 (Procymidone)12.73284.1283.0283965
285965
226프로클로라즈* (Prochloraz)22.24376.7375.03087015
18013810
2,4,6-트리클로로페놀* (2,4,6-trichlorophenol)4.71376.7375.01329715
1969740
227프로티오포스 (Prothiofos)13.99345.2343.926722120
23910
228프로파닐 (Propanil)9.74218.1217.016112625
21716125
229프로파진 (Propazine)8.27229.7229.12295815
21417210
230프로파클로르 (Propachlor)6.72211.7211.01699310
1769220
231프로팜 (Propham)5.40179.2179.01799315
137938
232프로페노포스 (Profenofos)14.15373.6371.933726710
33926910
233프로페탐포스 (Propetamphos)8.45281.3281.01386420
1941665
234프로플루랄린 (Profluralin)8.36347.3347.131819920
5510
235프로피소클로르 (Propisochlor)10.17283.8283.116212020
14715
236프로피자마이드 (Propyzamide)8.60256.1255.017314520
10935
237프로피코나졸, 이성질체 1 (Propiconazole, Isomers 1)16.66342.2341.02596910
1735
프로피코나졸, 이성질체 2 (Propiconazole, Isomers 2)16.856910
1735
238프로하드로자스몬 (Prohydrojasmon)8.92254.4254.1153975
1848315
239프탈리드 (Phthalide, Fthalide)11.68271.9269.824121315
24321515
240플람프로프-아이소프로필 (Flamprop-isopropyl)14.51363.8363.11057715
5140
241플로메토퀸 (Flometoquin)20.08435.4435.140337420
43537630
242플루메트랄린 (Flumetralin)13.35421.7421.014311720
10730
243플루미옥사진 (Flumioxazin)25.21354.3354.13543265
2872595
244플루발리네이트, 이성질체 1* (Fluvalinate, Isomers 1)25.59502.9502.12505520
20020
플루발리네이트, 이성질체 2* (Fluvalinate, Isomers 2)25.735520
20020
245플루시트리네이트, 이성질체 1** (Flucythrinate, Isomers 1)23.97451.5451.115710715
19910725
플루시트리네이트, 이성질체 2** (Flucythrinate, Isomers 2)24.3615710715
19910725
246플루실라졸 (Flusilazole)14.48315.4315.123316520
15220
247플루아지포프-뷰틸 (Fluazifop-butyl)15.11383.4383.1282915
23825
248플루아크리피림 (Fluacrypyrim)15.95426.4426.114510230
2041895
249플루엔설폰 Fluensulfone6.60291.7290.91195930
9210
250플루오로클로리돈 (Fluorochloridone)11.61312.1311.018710920
31117420
251플루오피람 (Fluopyram)12.48396.7396.01739535
14520
252플루퀸코나졸 (Fluquinconazole)22.11376.2375.034010840
28630
253플루클로랄린 (Fluchloralin)8.65355.7355.03062645
3266315
254플루티아닐 (Flutianil)24.46426.4426.02312165
20010
255플루펜피르-에틸 (Flufenpyr-ethyl)15.32408.7408.040834515
32128615
256플룩사피록사드 (Fluxapyroxad)18.48381.3380.01594330
13910
257피라조포스 (Pyrazophos)20.75373.4373.023220410
22119310
258피라카볼리드 (Pyracarbolid)11.85217.3217.1125975
5515
259피라클로포스** (Pyraclofos)21.29360.8360.019413820
13910
260피라플루펜에틸 (Pyraflufen-ethyl)16.89413.2412.041234910
34930715
261피리달릴*** (Pyridalyl)24.34491.1488.920417610
14820
262피리메타닐 (Pyrimethanil)8.79199.3199.119811835
15820
263피리미노박메틸(E) (Pyriminobac-methyl E)16.77361.4361.130223015
25620
피리미노박메틸(Z) (Pyriminobac-methyl Z)15.3223015
25620
264피리미카브 (Pirimicarb)9.24238.3238.11669612
23816610
265피리미포스메틸 (Pirimiphos-methyl)10.62305.3305.029012520
2331515
266피리미포스에틸 (Pirimiphos-ethyl)11.78333.4333.130416810
31816610
267피리페녹스 (Pyrifenox)13.23295.2294.018712420
17110025
268피리프탈리드 (Pyriftalid)20.77318.3318.031827320
2745
269피콕시스트로빈 (Picoxystrobin)13.54367.3367.114510230
33517310
270피페로닐부톡사이드 (Piperonyl butoxide)17.69338.4338.217613125
14510
271피프로닐 (Fipronil)12.25437.1435.936721330
25530
272할펜프록스*** (Halfenprox)23.74477.3476.026511710
26312940
273헥사클로로벤젠******* (Hexachlorobenzene)7.84284.8283.828421440
24928
274헥시티아족스 (Hexythiazox)13.16352.9352.11841495
1561555
275헵타클로르 (Heptachlor)10.31373.3369.827223720
27423720
헵타클로르 에폭사이드 (Heptachlor epoxide)12.43389.3385.835325330
21718220
276헵테노포스 (Heptenophos)6.34250.6250.01246340
8915

동일 규격 권장 · GC는 칼럼 규격을 원문 그대로 두는 것을 권합니다. 캐필러리는 고정상과 규격(길이·안지름·막두께)이 함께 시험법을 이루기 때문에, 치수를 바꾸면 머무름과 분리가 직접 달라집니다. 같은 고정상의 동등 제품을 원문과 같은 규격으로 고르십시오.

이 조건으로 GC 시뮬레이션 열기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다. 기울기 프로파일·압력·용매 소모량은 이 조건의 값이지만, 화합물 정보를 넘기지 않으므로 머무름 시간과 분리도는 예시값입니다.

고시 원문 보기 (축자)
가) 컬럼: DB-5MS(30 m × 0.25 mm, 0.25 μm) 또는 이와 동등한 것
나) 이동상 가스 및 유량: 헬륨(He) 또는 이와 동등한 것, 1.2 mL/분
다) 오븐 온도: 90℃에서 시험용액을 주입하여 20℃/분의 비율로 180℃까지 온도를 상승시키고 5℃/분의 비율로 300℃까지 상승시켜 5분간 유지한다.
라) 주입 방법: Splitless mode
마) 인터페이스 온도: 300℃
바) 분석대상(276종) 물질의 조건
[표 1]

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 GC-5USP G27 상당

5% 페닐-95% 메틸폴리실록산(USP G27). 범용 약비극성 상.

함께 보기

타사 컬럼 대체 솔루션컬럼 추천 도구

분석조건 (4)

LC기울기 용리신판 · 2027.1.1.부터7.1.2.2FD-다성분-시험법-제2법-x4

원문 표제 단서: 액체크로마토그래프-질량분석기

칼럼
C18 · USP L1

C18계 컬럼

안지름 2.1 mm · 길이 10 cm · 입자경 2.7 μm

칼럼온도
40℃
이동상
  • 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 수용액
  • 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 메탄올
유량
0.2 mL/분
주입량
2 μL
질량분석(MS) 조건 보기 (1항목)
전이표
분석성분 (Compound)이온화 (Ionization mode)머무름 시간 (분)분자량 (MW)관측질량 (Exact mass)선구이온 (Precursor ion, m/z)생성이온 (Product ion, m/z)충돌 에너지 (Collision energy, eV)
1나프로파마이드 (Napropamide)Positive9.20271.4271.127212921
17123
2네뷰론 (Neburon)Positive9.60275.2274.02758823
11421
3노레아(노루론) (Norea(Noruron))Positive8.17222.3222.12237239
6749
4노르플루라존 (Norflurazon)Positive7.48303.7303.030414049
14561
5노발루론 (Novaluron)Negative11.18492.7492.049147118
15622
6니텐피람 (Nitenpyram)Positive4.65270.7270.027122517
12639
7다이뮤론 (Daimuron)Positive8.60268.4268.126915117
11927
8도딘 (Dodine)Positive9.46287.4287.22284351
5737
9디노테퓨란 (Dinotefuran)Positive4.40202.2202.120312917
11317
10디메설파젯 (Dimesulfazet)Positive7.53336.3336.133726717
23831
11디메토에이트 (Dimethoate)Positive5.56229.2228.923012527
19913
12데메톤-S (Demeton-S)Positive7.92258.3258.02598917
6147
데메톤-S-설폰 (Demeton-S-sulfone)Positive5.71290.3290.029123521
9929
데메톤-S-설폭사이드 (Demeton-S-sulfoxide)Positive5.62274.3274.027514129
10933
디설포톤 (Disulfoton)Positive10.93274.4274.02758921
6145
디설포톤 설폰 (Disulfoton sulfone)Positive7.15306.4306.030712523
15317
디설포톤 설폭사이드 (Disulfoton sulfoxide)Positive7.04290.4290.029118519
12941
13데메톤-S-메틸 (Demeton-S-methyl)Positive6.65230.3230.02318919
6143
14데메톤-S-메틸-설폰 (Demeton-S-methyl-sulfone)Positive4.98262.3262.026316921
10937
15데스메디팜 (Desmedipham)Positive7.45300.3300.130118213
13629
16디우론 (Diuron)Positive7.45233.1232.02337237
4631
17디클로르보스 (Dichlorvos)Positive6.41221.0219.922110923
12721
18디클로슐람 (Diclosulam)Positive6.87406.2404.940616133
12583
19디플루벤주론 (Diflubenzuron)Positive9.41310.7310.031115819
14145
20딤프로피리다즈 (Dimpropyridaz)Positive6.20301.4301.130210941
17923
21레나실 (Lenacil)Positive7.30234.3234.123515323
13645
22레피멕틴 A3* (Lepimectin A3)Positive13.70705.8705.372854931
53139
레피멕틴 A4* (Lepimectin A4)Positive14.19719.9719.374256333
54539
23루페뉴론 (Lufenuron)Negative11.99511.1509.950933918
32628
24리뉴론 (Linuron)Positive8.13249.1248.024916023
18219
25만데스트로빈 (Mandestrobin)Positive9.98313.4313.131419215
13239
26만디프로파미드 (Mandipropamid)Positive9.82411.9411.141236625
38421
27말라티온 (Malathion)Positive8.57330.4330.033112717
12539
28말라옥손 (Malaoxon)Positive6.55314.3314.031512717
9935
29메빈포스 (Mevinphos)Positive5.85224.1224.022512723
19313
30메소트리온* (Mesotrione)Positive5.74339.3339.034022825
10441
31메카밤 (Mecarbam)Positive9.22329.4329.033022713
19919
32메타미도포스 (Methamidophos)Positive2.38141.1141.01429421
12519
33메타미트론 (Metamitron)Positive5.57202.2202.020310431
17523
34메타미포프 (Metamifop)Positive11.46440.9440.044128827
12341
35메타벤즈티아주론 (Methabenzthiazuron)Positive7.33221.3221.022216523
15045
36메타플루미존(E) (Metaflumizone E)Positive11.68506.4506.150717837
28735
메타플루미존(Z) (Metaflumizone Z)Positive10.89506.4506.117837
28735
37메토미노스트로빈 (Metominostrobin)Positive7.56284.3284.128519427
19619
38메토밀 (Methomyl)Positive4.90162.2162.01638813
10613
39메토브로뮤론 (Metobromuron)Positive7.24259.1258.025917023
14823
40메톡시페노자이드 (Methoxyfenozide)Positive8.52368.5368.236914923
31311
41메톨카브 (Metolcarb)Positive6.30165.2165.016610917
9441
42메트라페논 (Metrafenone)Positive10.70409.3408.040920923
22729
43메트코나졸 (Metconazole)Positive10.25319.8319.13207043
12561
44메티오카브 (Methiocarb)Positive8.16225.3225.022616913
12231
45메페나셋 (Mefenacet)Positive8.78298.4298.029914819
12035
46메펜트리플루코나졸 (Mefentrifluconazole)Positive10.04397.8397.03987051
18241
47메포스폴란 (Mephosfolan)Positive6.40269.3269.027016821
14021
48모노크로토포스 (Monocrotophos)Positive5.00223.2223.022419311
12721
49바미도티온 (Vamidothion)Positive5.47287.3287.028814617
11831
50바이오레스메트린* (Bioresmethrin)Positive14.02338.4338.133917121
14335
51발리페날레이트 (Valifenalate)Positive8.77398.9398.139915545
11635
52버놀레이트 (Vernolate)Positive10.82203.3203.120412815
8619
53베나락실 (Benalaxyl)Positive10.06325.4325.132614829
9151
54베플루부타미드 (Beflubutamid)Positive9.66355.3355.13569157
17723
55벤디오카브 (Bendiocarb)Positive6.54223.2223.022410925
16713
56벤설라이드 (Bensulide)Positive9.51397.5397.039831415
35611
57벤조비사이클론 (Benzobicyclon)Positive8.41467.0446.044725735
22951
58벤족시메이트 (Benzoximate)Positive10.70363.8363.036419911
10535
59벤티아발리카브아이소프로필(R) (Benthiavalicarb-isopropyl R)Positive8.59381.5381.138218043
19727
벤티아발리카브아이소프로필(S) (Benthiavalicarb-isopropyl S)Positive8.81381.5381.118043
19727
60뷰토카복심 (Butocarboxim)Positive6.03190.3190.02137519
15615
61브로마실 (Bromacil)Positive6.58261.1260.026120521
18841
62브로플라닐라이드 (Broflanilide)Positive10.65663.3662.066564537
62557
63비스트리플루론 (Bistrifluron)Negative12.60446.7446.044526234
18680
64비터타놀 (Bitertanol)Positive10.27337.4337.133826913
9921
65빅사펜 (Bixafen)Positive9.53414.2413.041439421
26633
66사이목사닐 (Cymoxanil)Positive10.70198.2198.019918425
14137
67사이아조파미드 (Cyazofamid)Positive9.18324.8324.032510821
26113
68사이안트라닐리프롤 (Cyantraniliprole)Positive6.78473.7472.047528623
11281
69사이에노피라펜 (Cyenopyrafen)Positive12.87393.5393.239431035
25445
70사이클라닐리프롤 (Cyclaniliprole)Positive9.46602.1598.960028421
112113
71사이클로뷰트리플루람 (Cyclobutrifluram)Negative8.80389.2388.038721514
14642
72사이클로프로트린 (Cycloprothrin)Positive13.03482.4481.049918145
25719
73사이클로에이트 (Cycloate)Positive10.97215.4215.12168323
13419
74사이프로코나졸, 이성질체1 (Cyproconazole, Isomer1)Positive8.55291.8291.12927035
12539
사이프로코나졸, 이성질체2 (Cyproconazole, Isomer2)Positive8.82291.8291.12927035
12539
75사이플루메토펜 (Cyflumetofen)Positive11.38447.5447.146517333
24919
76사플루페나실 (Saflufenacil)Positive7.78500.9500.050119859
34935
77설펜트라존 (Sulfentrazone)Positive6.64387.2385.940438719
30735
78설폭사플로르 (Sulfoxaflor)Positive5.66277.3277.027817413
15439
79설프로포스 (Sulprofos)Positive12.64322.4322.032321921
13941
80세닥산-시스 (Sedaxane-cis)Positive8.68331.4331.133229226
15938
세닥산-트랜스 (Sedaxane-trans)Positive9.17331.4331.129226
15938
81세크뷰메톤 (Secbumeton)Positive7.21225.3225.122617027
10039
82세톡시딤 (Sethoxydim)Positive11.90327.5327.132817825
28217
83스피네토람-J (Spinetoram-J)Positive10.46748.0747.474814237
9899
스피네토람-L (Spinetoram-L)Positive11.09760.0759.476014235
9899
84스피노신 A (Spinosyn A)Positive9.62732.0731.473214237
9897
스피노신 D (Spinosyn D)Positive10.23746.0745.474614237
9897
85스피로디클로펜 (Spirodiclofen)Positive13.01411.3410.141131317
21347
86스피로테트라맷* (Spirotetramat)Positive8.93373.4373.137430223
21645
스피로테트라맷-엔올* (Spirotetramat-enol)Positive6.93301.4301.130221637
11747
87스피로피디온 (Spiropidion)Positive9.60422.9422.142328835
26449
스피로피디온-엔올 (Spiropidion-enol)Positive7.40350.9350.135128831
31923
88시마진 (Simazine)Positive6.62201.7201.020213225
12425
89시아나진 (Cyanazine)Positive6.27240.7240.024121425
10443
90아메톡트라딘 (Ametoctradin)Positive10.59275.4275.227617651
14949
91아미설브롬 (Amisulbrom)Positive11.27466.3464.946622727
14867
92아미트라즈* (Amitraz)Positive13.47293.4293.129416321
12241
93아바멕틴* (아바멕틴 B1a) (Abamectin B1a)Positive13.86873.1872.489130531
56819
94아세타미프리드 (Acetamiprid)Positive5.51222.7222.022312629
9953
95아세페이트 (Acephate)Positive3.60183.2183.018414311
9529
96아이소사이클로세람 (Isocycloseram)Positive11.47548.3547.154841835
16057
97아이소프로튜론 (Isoproturon)Positive7.36206.3206.12077231
13431
98아이속사벤 (Isoxaben)Positive8.33332.4332.133316523
10777
99아이속사티온 (Isoxathion)Positive10.58313.3313.031428613
17019
100아자메티포스 (Azamethiphos)Positive6.36324.7323.932511247
13935
101아족시스트로빈 (Azoxystrobin)Positive7.88403.4403.140437221
34435
102아진포스메틸 (Azinphos-methyl)Positive7.83317.3317.031813219
16019
103알디카브 (Aldicarb)Positive6.09190.3190.020811611
8923
104알레트린 (Allethrin)Positive11.97302.4302.130313515
9153
105에마멕틴 벤조에이트 (에마멕틴 B1a) (Emamectin B1a)Positive11.25886.1885.588682111
15843
106에스프로카브 (Esprocarb)Positive11.87265.4265.12669133
6579
107에타복삼 (Ethaboxam)Positive6.96320.4320.032118331
20035
108에토펜프록스 (Etofenprox)Positive14.84376.5376.239417721
13533
109에트림포스 (Etrimfos)Positive10.22292.3292.029312533
26521
110에티오펜카브 (Ethiofencarb)Positive6.96225.3225.02261699
10723
111에티프롤 (Ethiprole)Positive8.05397.2395.939735129
25551
112엑스엠씨 (XMC)Positive6.99179.2179.018012315
7779
113오리사스트로빈 (Orysastrobin)Positive8.51391.4391.139220521
11631
114오리잘린 (Oryzalin)Negative9.06346.4346.034528132
14736
115오메토에이트 (Omethoate)Positive4.20213.2213.021412529
18315
116오퓨레이스 (Ofurace)Positive6.52281.7281.028216031
25417
117옥사디아길 (Oxadiargyl)Positive10.37341.2340.034115139
22237
118옥사밀 (Oxamyl)Positive4.67219.3219.02379011
7229
옥사밀 옥심 (Oxamyl oxime)Positive4.17162.0162.21637217
9023
119옥사지클로메폰 (Oxaziclomefone)Positive11.50376.3375.037619019
16139
120옥사티아피프롤린 (Oxathiapiprolin)Positive8.36539.5539.154050043
16343
121옥시데메톤메틸 (Oxydemeton-methyl)Positive4.80246.3246.024716921
10939
122옥시카복신 (Oxycarboxin)Positive5.75267.3267.026817521
14731
123유니코나졸 (Uniconazole)Positive9.19291.8291.12927041
12539
124육-비에이 (Benzyladenine, 6-Benzyl aminopurine)Negative6.04225.2225.122413330
10642
125이나벤파이드 (Inabenfide)Positive8.03338.8338.03398049
32123
126이마잘릴 (Imazalil)Positive6.65297.2296.029715933
6935
127이미다클로프리드 (Imidacloprid)Positive5.31255.7255.025620921
21217
128이미벤코나졸 (Imibenconazole)Positive11.80411.7409.941112550
17128
129이미시아포스 (Imicyafos)Positive6.17304.3304.130520131
23525
130이프로발리카브 (Iprovalicarb)Positive8.97320.4320.232111935
20315
131이프펜카바존 (Ipfencarbazone)Positive9.95427.2426.042719817
15631
132이프플루페노퀸 (Ipflufenoquin)Positive9.37347.3347.134833031
18037
133인피르플룩삼 (Inpyrfluxam)Positive9.10333.4333.233423839
25827
134카바릴 (Carbaryl)Positive6.77201.2201.03142115
12739
135카베타마이드 (Carbetamide)Positive6.27236.3236.123719211
12023
136카벤다짐 (Carbendazim)Positive5.01191.2191.019216025
13241
137카보퓨란* (Carbofuran)Positive6.56221.3221.122216517
12329
3-하이드록시카보퓨란* (3-hydroxycarbofuran)Positive5.53237.3237.123818115
16323
138카펜스트롤 (Cafenstrole)Positive8.67350.4350.135110019
7241
139카프로파마이드 (Carpropamide)Positive9.97334.7333.033413931
19617
140크로톡시포스 (Crotoxyphos)Positive8.24314.3314.033221113
12735
141퀴노클라민 (Quinoclamine)Positive8.39207.6207.020815113
10923
142크로마페노자이드 (Chromafenozide)Positive8.90394.5394.239517521
33911
143크루포메이트 (Crufomate)Positive9.40291.7291.029223627
20437
144클로란트라닐리프롤 (Chlorantraniliprole)Positive7.65483.1480.948445327
28619
145클로로벤주론 (Chlorobenzuron)Positive9.81309.1308.030915621
13943
146클로로톨루론 (Chlorotoluron)Positive7.11212.7212.02137239
10443
147클로록수론 (Chloroxuron)Positive8.74290.7290.02917247
11163
148클로르펜빈포스(E) (Chlorfenvinphos E)Positive10.10359.6357.935915517
9945
클로르펜빈포스(Z) (Chlorfenvinphos Z)Positive10.50359.6357.915517
9945
149클로르플루아주론 (Chlorfluazuron)Positive13.14540.7538.954038331
15833
150클로리다존 (Chloridazone)Positive5.61221.6221.022210433
7753
151클로메프로프 (Clomeprop)Positive11.72324.2323.032412027
14821
152클로퀸토셋멕실 (Cloquintocet-mexyl)Positive11.76335.8335.133623823
19243
153클로티아니딘 (Clothianidin)Positive7.34249.7249.02509347
13125
154클로펜테진 (Clofentezine)Positive10.94303302.030313821
10255
155터부틸라진 (Terbuthylazine)Positive8.33229.7229.123017421
10443
156터부포스 (Terbufos)Positive11.93288.4288.028910313
2339
터부포스 옥손 (Terbufos oxon)Positive8.98272.4272.027310313
11539
터부포스 옥손 설폰 (Terbufos oxon sulfone)Positive6.21304.4304.030523119
9545
터부포스 옥손 설폭사이드 (Terbufos oxon sulfoxide)Positive6.02288.4288.028917115
11541
터부포스 설폰 (Terbufos sulfone)Positive8.01320.4320.03219755
11539
터부포스 설폭사이드 (Terbufos sulfoxide)Positive7.97304.4304.030518715
13139
157테닐클로르 (Thenylchlor)Positive9.11323.8323.032412717
9757
158테부티우론 (Tebuthiuron)Positive6.64228.3228.122917225
11635
159테부페노자이드 (Tebufenozide)Positive9.47352.5352.235313325
29711
160테부플로퀸 (Tebufloquin)Positive9.92289.3289.129024823
23257
테부플로퀸 M1 (Tebufloquin M1)Positive7.97247.3247.124823247
19235
161테트라닐리프롤 (Tetraniliprole)Negative7.39554.9544.154313724
10978
162테프랄록시딤 (Tepraloxydim)Positive6.77341.8341.134225019
16629
163테플루벤주론 (Teflubenzuron)Negative11.89381.1379.937933916
35910
164톨펜피라드 (Tolfenpyrad)Positive11.93383.9383.138419737
15459
165톨피라레이트 (Tolpyralate)Positive7.66484.5484.148538315
32531
1662,3,5-트리메타카브 (2,3,5-Trimethacarb)Positive7.46193.2193.119413717
12235
3,4,5-트리메타카브 (3,4,5-Trimethacarb)Positive7.46193.2193.113717
12235
167트리뷰포스 (Tribufos)Positive13.50314.5314.031516921
5737
168트리사이클라졸 (Tricyclazole)Positive5.90189.2189.019013637
10947
169트리아자메이트 (Triazamate)Positive9.00314.4314.13157235
22617
170트리아파몬 (Triafamone)Positive6.60406.3406.040724533
16061
171트리클로르폰***** (Trichlorfon)Positive5.58257.4255.925710927
22117
172트리티코나졸 (Triticonazole)Positive9.01317.8317.13187053
12545
173트리포린 1 (Triforine 1)Positive7.50435.0431.943539019
21537
트리포린 2 (Triforine 2)Positive7.70435.0431.939019
21537
174트리플루뮤론 (Triflumuron)Positive10.35358.7358.035915623
13945
175티디아주론 (Thidiazuron)Positive6.45220.3220.022110219
12825
176티아디닐 (Tiadinil)Negative8.75267.7267.02667138
23816
177티아메톡삼 (Thiamethoxam)Positive4.98291.7291.029221117
13229
178티아벤다졸 (Thiabendazole)Positive5.36201.2201.020217535
13143
179티아조피르 (Thiazopyr)Positive9.93396.4396.039737727
33531
180티아클로프리드 (Thiacloprid)Positive5.71254.7252.025312629
9051
181티오디카브****** (Thiodicarb)Positive6.76354.5354.03558827
10821
182티오벤카브 (Thiobencarb)Positive10.72257.8257.025812525
8965
183티오파네이트메틸 (Thiophanate-methyl)Positive6.45342.4342.034315120
31110
184파목사돈 (Famoxadone)Positive10.13374.4374.139223823
23927
185페나미포스 (Fenamiphos)Positive9.41303.4303.130421731
20247
페나미포스설폰 (Fenamiphos sulfone)Positive6.53335.4335.033626627
30821
페나미포스설폭사이드 (Fenamiphos sulfoxide)Positive6.43319.4319.132023335
17133
186페나자퀸 (Fenazaquin)Positive13.52306.4306.130716119
14759
187페노트린-시스 (Phenothrin-cis)Positive14.39350.5350.135118331
12887
페노트린-트랜스 (Phenothrin-trans)Positive14.55350.5350.118331
12887
188페녹사설폰 (Fenoxasulfone)Positive8.74366.3365.038320321
17551
189페녹사프로프-에틸 (Fenoxaprop-ethyl)Positive11.50361.8361.01117725
11935
190페녹슐람 (Penoxsulam)Positive6.71483.4483.048419539
16449
191페녹시카브 (Fenoxycarb)Positive9.56301.3301.130211615
25617
192페림존(E) (Ferimzone E)Positive7.55254.3254.125513227
12429
페림존(Z) (Ferimzone Z)Positive8.02254.3254.125513227
12429
193페뷰레이트 (Pebulate)Positive10.83203.3203.120412817
7219
194펜메디팜 (Phenmedipham)Positive7.59300.3300.130113627
16813
195펜사이큐론 (Pencycuron)Positive10.61328.8328.132912535
21823
196펜설포티온 (Fensulfothion)Positive7.28308.4308.030915733
23531
197펜트라자마이드 (Fentrazamide)Positive9.92349.8349.135015415
7235
198펜피록시메이트 (Fenpyroximate)Positive13.02421.5421.242236623
13841
199펜헥사미드 (Fenhexamid)Positive8.92302.2301.03029731
14343
200포레이트 (Phorate)Positive10.71260.4260.02617523
19913
포레이트옥손 (Phorate oxon)Positive7.65244.3244.02457517
4741
포레이트옥손설폰 (Phorate oxon sulfone)Positive5.70276.3276.027711139
12721
포레이트설폰 (Phorate sulfone)Positive7.19292.3292.029317117
11533
포레이트옥손설폭사이드 (Phorate oxon sulfoxide)Positive5.54260.3260.026111129
9731
포레이트설폭사이드 (Phorate sulfoxide)Positive7.06276.4276.027719913
14329
201포메타네이트 (Formetanate)Positive4.16221.3221.122216521
4647
202포메사펜 (Fomesafen)Negative8.05438.8437.91203750
22248
203포스티아제이트 (Fosthiazate)Positive6.99283.3283.028410429
22815
204포스폴란 (Phosfolan)Positive5.98255.3255.02562285
615
205포클로르페뉴론 (Forchlorfenuron)Positive7.34247.7247.024812925
9347
206폭심 (Phoxim)Positive10.54298.3298.029912917
7747
207퓨라티오카브* (Furathiocarb)Positive11.66382.5382.138319523
25217
208프로메카브 (Promecarb)Positive8.40207.3207.120815113
10923
209프로베나졸 (Probenazole)Positive5.61223.2223.022451113
63111
210프로설포카브 (Prosulfocarb)Positive11.43251.4251.12529137
12817
211프로퀴나지드 (Proquinazid)Positive13.35372.2372.037333121
28933
212프로티오코나졸 (Prothioconazole) (Prothioconazole-desthio로 분석한다)Positive9.24312.2311.13127049
12553
213프로파모카브 (Propamocarb)Positive4.10188.3188.118910223
7433
214프로파자이트* (Propargite)Positive12.69350.5350.136823121
17547
215프로파퀴자포프* (Propaquizafop)Positive11.83443.9443.144437123
29931
216프로폭서 (Propoxur)Positive6.52209.2209.121016811
15311
217플로니카미드 (Flonicamid)Positive4.96229.2229.023020327
9853
218플로릴피콕사미드 (Florylpicoxamid)Positive9.90512.5512.151323131
47119
X12485649Positive9.30470.5470.147123125
10945
219플루디옥소닐 (Fludioxonil)Positive8.20248.2248.026622921
15847
220플루리돈 (Fluridone)Positive7.76329.3329.133031041
11589
221플루벤디아마이드 (Flubendiamide)Positive9.61682.4682.068340815
27447
222플루설파마이드 (Flusulfamide)Negative10.27415.2413.941317146
17950
223플루아지남 (Fluazinam)Negative11.96465.1463.946341628
39824
224플루오메투론 (Fluometuron)Positive6.96232.2232.023316035
14047
225플루오피콜라이드 (Fluopicolide)Positive8.53383.6381.938317331
10989
226플루옥사스트로빈(E) (Fluoxastrobin E)Positive8.82458.8458.145942723
18845
플루옥사스트로빈(Z) (Fluoxastrobin Z)Positive9.48458.8458.142723
18845
227플루옥사피프롤린 (Fluoxapiprolin)Positive8.10650.1649.065061033
15771
228플루인다피르 (Fluindapyr)Positive9.30351.2351.135225639
31227
229플루톨라닐 (Flutolanil)Positive8.40323.3323.132426223
24223
230플루트리아폴 (Flutriafol)Positive7.17301.3301.13027045
12339
231플루티아셋-메틸 (Fluthiacet-methyl)Positive9.81403.9403.040427439
21553
232플루페나셋 (Flufenacet)Positive9.11363.3363.036415227
12447
233플루페녹수론 (Flufenoxuron)Negative12.58488.8488.048746712
30426
234플루폭삼 (Flupoxam)Positive9.48460.8460.046144437
12369
235플루피라디퓨론 (Flupyradifurone)Positive13.35288.7288.028927231
21647
236플루피리민 (Flupyrimin)Positive6.47315.7315.031612621
9057
237플룩사메타마이드 (Fluxametamide)Positive12.17474.3473.047440029
16051
238피디플루메토펜 (Pydiflumetofen)Positive10.63426.7425.042619351
16637
239피라족시펜 (Pyrazoxyfen)Positive10.02403.3402.04039161
10529
240피라졸레이트 (Pyrazolate)Positive10.60439.3438.043917325
14577
241피라지플루미드 (Pyraziflumid)Positive8.93379.3379.038014741
17527
242피라클로닐 (Pyraclonil)Positive6.94314.8314.131516937
27623
243피라클로스트로빈 (Pyraclostrobin)Positive10.36387.8387.038816333
19417
244피로퀼론 (Pyroquilon)Positive6.43173.2173.017413231
11743
245피리다벤 (Pyridaben)Positive13.33364.9364.136514731
30931
246피리다클로메틸 (Pyridachlometyl)Positive8.75316.7316.131724043
22047
247피리다펜티온 (Pyridaphenthion)Positive8.67340.3340.034118933
20531
248피리데이트* (Pyridate)Positive14.08378.9378.137920725
35115
249피리미디펜 (Pyrimidifen)Positive11.82377.9377.137818431
15045
250피리미설판 (Pyrimisulfan)Positive7.52419.4419.042037023
38821
251피리벤족심 (Pyribenzoxim)Positive11.84609.6609.161041317
18047
252피리벤카브 (Pyribencarb)Positive7.98361.8361.136223925
20737
KIE-9749Positive7.45361.8361.123927
20741
253피리뷰티카브 (Pyributicarb)Positive12.33330.4330.133110839
13335
254피리오페논 (Pyriofenone)Positive10.86365.8365.136618431
20933
255피리프록시펜* (Pyriproxyfen)Positive12.44321.4321.13229621
18531
256피리플루퀴나존 (Pyrifluquinazon)Positive8.68464.3464.146542327
10745
257피메트로진* (Pymetrozine)Positive4.25217.2217.021810527
7955
258피카뷰트라족스 (Picarbutrazox)Positive9.40409.4409.141031019
10735
TZ-1EPositive9.22409.4409.131019
10735
259피콜리나펜 (Picolinafen)Positive11.87376.3376.037723843
25631
260피페로포스 (Piperophos)Positive10.93353.5353.135417129
25519
261피플루뷰마이드 (Pyflubumide)Positive12.11535.5535.253615527
11175
피플루뷰마이드-NH (Pyflubumide-NH)Positive11.35465.4465.146613739
11137
262헥사지논 (Hexazinone)Positive6.57252.3252.125317123
7143
263헥사코나졸 (Hexaconazole)Positive10.20314.2313.03147039
15943
264헥사플루뮤론 (Hexaflumuron)Negative11.07461.1459.945943918
27626

기울기 조건표

시간(분)A(%)B(%)
0.0955
1.0955
3.04060
13.00100
18.00100
18.1955
25.0955
이 조건으로 Core-Shell 전환 계산하기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.

고시 원문 보기 (축자)
가) 컬럼: C18계 컬럼(2.1 mm × 100 mm, 2.7 μm) 또는 이와 등등한 것
나) 이동상
(1) 이동상 A: 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 수용액
(2) 이동상 B: 0.1%(v/v) 포름산(formic acid)과 5 mM 아세트산암모늄(ammonium acetate) 함유한 메탄올
[표 1]
다) 이동상 유량: 0.2 mL/분
라) 컬럼온도: 40℃
마) 주입량: 2 μL
바) 분석대상(264종) 물질의 조건
[표 2]
3) 정량한계

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 C18USP L1 상당

약전 일반명 '액체크로마토그래프용옥타데실실릴실리카겔'(USP 분류로는 L1 상당)에 해당. 약전은 브랜드를 지정하지 않으므로 각조가 기재한 물리 사양(치수·입자경 등)과 KP 통칙·일반시험법의 조정 허용범위 안에서 해당 상을 충족하는 C18을 선택할 수 있다 — 선택 기준은 시스템적합성(분리도·테일링·RSD) 통과 용이성과 재현성이다.

함께 보기

Core-Shell 전환 솔루션 (동등성 검증·계산기)타사 컬럼 대체 솔루션컬럼 추천 도구저분자 API 분석 솔루션컬럼 보호·수명 관리

같은 고정상을 쓰는 다른 품목

한 컬럼으로 몇 개 시험을 함께 받을 수 있는지 볼 때 씁니다.

GC-5 품목 보기C18 품목 보기

공전이 개정되면

고시가 개정되면 이 페이지의 분석조건도 함께 갱신됩니다. 어떤 항목이 어떻게 바뀌었는지는 크로마톡 규제·약전 브리핑에 정리해 올립니다.

최신 규제·공전 개정 브리핑 보기 →

출처: 식품의약품안전처 고시 제2026-55호 「식품의 기준 및 규격」 제8. 일반시험법. 국내 고시는 저작권법 제7조에 따른 비보호 저작물이며, 이 페이지는 원문의 분석조건을 기계적으로 정리하고 원문을 축자 병기한 것입니다. 원문의 오탈자·조판 잔재는 고치지 않고 보존했습니다.

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