이곳의 자료는 본/지사와 어떤 관계인가요?

Columnpia의 모든 기술 자료는 Phenomenex® 제조사의 공식 리포트를 기반으로 합니다. 이를 대한민국 공식 총판인 (주)성문시스텍 기술팀이 한국의 분석 실무 환경에 맞춰 전문적으로 해설하고 최적화하여 제공하는 '공식 실무 가이드'입니다.

분석법 개발(Method Development) 지원도 가능한가요?

물론입니다. 원하는 타겟 물질과 현재 보유 중인 장비 사양을 ChromaTalk 커뮤니티(community.columnpia.co.kr)에 남겨주시면, 전문 연구원이 24시간 이내에 최적의 컬럼과 분석 조건을 제안해 드립니다.

특수 시료(ADC, 올리고 등) 분석 가이드도 있나요?

네, 최신 바이오 의약품 트렌드에 맞춰 ADC, 올리고뉴클레오타이드, 펩타이드 맵핑 등 특수 응용 분야에 대한 전용 가이드 페이지를 운영 중이며, 지속적으로 업데이트됩니다.

Graph RAG 답변은 무엇이고, 다른 답변과 어떻게 다른가요?

한 질문에 ① 관리자가 제품·적용 경험을 바탕으로 실무 답변을 드리고, ② 한국분석과학연구소(KIAST)의 Ph.D·석사 등 전문가 그룹이 실무 관점의 전문가 답변을 직접 달아드립니다. 여기에 ③ Graph RAG 답변으로 보유 기술자료를 대조해 근거 자료와 함께 정리한 정확한 실무 정보까지 더해집니다. 세 답변은 순차 검수가 아니라 서로 독립적으로 달리며, 질문에 따라 한 가지만 달릴 수도 있습니다. 질문 내용은 외부 AI 서버로 전송되지 않습니다. AI 자동 답변 연동은 완전히 해제했고, Graph RAG 답변도 로컬 환경의 오픈소스 LLM으로 처리해 관리자 검수 후 게시합니다.

KIAST 연구진은 어떤 분들인가요?

KIAST는 한국분석과학연구소(Korea Institute of Analytical Science and Technology)이며, Ph.D·석사급 현장 분석 전문가들이 식품공전 기시법 대응·임상 대사체 분석 등 국내 실무 검증된 전문가 답변을 직접 작성합니다.

식품의 기준 및 규격 · 제8편 일반시험법분석조건 4건8.3.1

축·수산물 중 동물용의약품 동시 다성분 시험법

식품의약품안전처 고시 제2026-55호 「식품의 기준 및 규격」 제8. 일반시험법

배포 전 적대적 검증 완료 (2026-09-04, Claude Fable 5)

이 페이지는 고시 원문의 크로마토그래프 분석조건만 뽑아 정리한 것입니다. 시험 전체 절차(검체 조제, 시스템적합성 기준, 계산식 등)는 담고 있지 않으니, 실제 시험 수행과 판정은 반드시 고시 원문을 확인하십시오.

분석조건4건

분석조건 (1)

LC기울기 용리8.3.1FD-축-수산물-중-동물용의약품-동시-다성분-시험법-x1

원문 표제 단서: 액체크로마토그래프

칼럼

C18 · USP L1

C18계 컬럼

안지름 2.1 mm · 길이 15 cm · 입자경 3.5 μm

칼럼온도

40℃

이동상

0.1%(v/v) 포름산(formic acid) 함유한 수용액
0.1%(v/v) 포름산(formic acid) 함유한 아세토니트릴

유량

0.3 mL/분

주입량

5 μL

기타표

분석성분 (Compound),식육,알(卵),유(乳),어류,갑각류

나프실린 (Nafcillin),0.002,0.001,0.0007,0.01,0.01

날리딕스산 (Nalidixic acid),0.0009,0.001,0.001,0.001,0.01

노르플록사신 (Norfloxacin),0.0007,0.0007,0.0007,0.0007,0.0007

다노플록사신 (Danofloxacin),0.001,0.0005,0.0003,0.01,0.01

데하이드로콜산 (Dehydrocholic acid),-,-,-,0.002,0.01

독시싸이클린 (Doxycycline),0.003,0.0005,0.001,0.001,0.01

디아베리딘 (Diaveridine),0.001,0.0002,0.0002,0.01,0.01

디클록사실린 (Dicloxacillin),0.007,0.007,0.003,0.01,0.01

디플록사신 (Difloxacin),0.0005,0.001,0.0003,0.0003,0.001

레바미졸 (Levamisole),0.001,0.001,0.0002,0.01,0.01

록시스로마이신 (Roxithromycin),0.0003,0.0004,0.0002,0.01,0.01

리팍시민 (Rifaximin),0.0005,0.0002,0.003,0.01,0.01

린코마이신 (Lincomycin),0.003,0.0002,0.0008,0.001,0.0004

마보플록사신 (Marbofloxacin),0.002,0.0005,0.0005,0.01,0.01

메벤다졸 (Mebendazole),0.0003,0.0003,0.0003,0.01,0.01

메벤다졸아민 (Mebendazole amine),0.0007,0.0005,0.0006,0.01,0.01

5-하이드록시 메벤다졸 (5-Hydroxy mebendazole),0.0006,0.0003,0.0002,0.01,0.01

멜록시캄 (Meloxicam),0.0006,0.0005,0.0007,0.01,0.01

미노싸이클린 (Minocycline),0.002,0.001,0.005,0.01,0.01

벤질페니실린 (Benzylpenicillin, Penicillin G, Procaine benzylpenicillin),0.005,0.001,0.002,0.01,0.01

비치오놀 (Bithionol),0.0009,0.0005,0.0005,0.001,0.01

사라플록사신 (Sarafloxacin),0.0006,0.0006,0.003,0.01,0.01

설파구아니딘 (Sulfaguanidine),0.0005,0.0005,0.0005,0.0005,0.01

설파독신 (Sulfadoxine),0.0005,0.0005,0.0005,0.0005,0.01

설파디메톡신 (Sulfadimethoxine),0.0005,0.0005,0.0005,0.0005,0.01

설파디아진 (Sulfadiazine),0.0005,0.0005,0.0005,0.0005,0.01

설파메라진 (Sulfamerazine),0.0005,0.0005,0.0005,0.0005,0.01

설파메타진 (Sulfamethazine),0.0005,0.0005,0.0005,0.0005,0.01

설파메톡사졸 (Sulfamethoxazole),0.0005,0.0005,0.0005,0.0005,0.01

설파메톡시피리다진 (Sulfamethoxypyridazine),0.0005,0.0005,0.0005,0.0005,0.01

설파모노메톡신 (Sulfamonomethoxine),0.0005,0.0005,0.0005,0.0005,0.01

설파퀴녹살린 (Sulfaquinoxaline),0.0005,0.0005,0.0005,0.0005,0.01

설파클로르피라진 (Sulfachlorpyrazine),0.0005,0.0005,0.0005,0.0005,0.01

설파클로르피리다진 (Sulfacholrpyridazine),0.0005,0.0005,0.0005,0.0005,0.01

설파티아졸 (Sulfathiazole),0.0005,0.0005,0.0005,0.0005,0.01

설파페나졸 (Sulfaphenazole),0.0005,0.0005,0.0005,0.0005,0.01

설피속사졸 (Sulfisoxazole),0.0005,0.0005,0.0005,0.0005,0.01

세파드록실 (Cefadroxil),0.002,0.002,0.0009,0.005,0.01

세팔렉신 (Cefalexin),0.002,0.001,0.005,0.003,0.01

세프티오퍼 (Ceftiofur),0.002,0.002,0.002,0.002,0.002

데스후로일 세프티오퍼 (Disfuroyl ceftiofur),-,-,-,-,-

스피라마이신 (Spiramycin),0.001,0.0004,0.001,0.001,0.003

시프로플록사신 (Ciprofloxacin),0.0004,0.002,0.0007,0.002,0.001

아목시실린 (Amoxicillin),0.002,0.001,0.0004,0.005,0.002

알벤다졸 (Albendazole),0.0005,0.0004,0.0004,0.01,0.01

알벤다졸 설폭사이드 (Albendazole sulfoxide),0.0003,0.0003,0.0003,0.01,0.01

알벤다졸 설폰 (Albendazole sulfone),0.0003,0.0003,0.0003,0.01,0.01

2-아미노 알벤다졸 설폰 (2-Aminoalbendazole sulfone),0.0003,0.0002,0.0002,0.01,0.01

암피실린 (Ampicillin),0.001,0.001,0.0007,0.007,0.002

에리스로마이신 (Erythromycin),0.0003,0.0002,0.0002,0.001,0.001

에토파베이트 (Ethopabate),0.0005,0.0005,0.0006,0.01,0.01

m-페네티딘 (m-phenetidine),0.005,0.005,0.0001,0.01,0.01

엔로플록사신 (Enrofloxacin),0.0004,0.0009,0.0005,0.001,0.0004

오르메토프림 (Ormethoprim),0.0002,0.0005,0.0001,0.001,0.01

오비플록사신 (Orbifloxacin),0.004,0.002,0.003,0.01,0.01

오플록사신 (Ofloxacin),0.0002,0.0002,0.0002,0.0002,0.0002

옥사실린 (Oxacillin),0.004,0.003,0.002,0.01,0.01

옥소린산 (Oxolinic acid),0.001,0.0006,0.0009,0.01,0.001

옥스펜다졸 (Oxfendazole),0.002,0.002,0.002,0.01,0.01

옥스펜다졸 설폰 (Oxfendazole sulfone),0.0004,0.0003,0.0003,0.01,0.01

옥시벤다졸 (Oxibendazole),0.0004,0.0003,0.0003,0.01,0.01

옥시테트라싸이클린 (Oxytetracycline),0.0005,0.007,0.0005,0.0003,0.001

올레안도마이신 (Oleandomycin),0.005,0.007,0.0008,0.01,0.01

조사마이신 (Josamycin),0.0004,0.0002,0.0003,0.0003,0.01

클로람페니콜 (Chloramphenicol),0.0005,0.0005,0.0005,0.0005,0.0005

클로르테트라싸이클린 (Chlortetracycline),0.005,0.003,0.003,0.003,0.002

클록사실린 (Cloxacillin),0.001,0.0005,0.002,0.01,0.01

클린다마이신 (Clindamycin),0.005,0.0003,0.0005,0.0003,0.01

키타사마이신 (Kitasamycin),0.001,0.0009,0.0006,0.001,0.01

타일로신 (Tylosin A),0.0005,0.0005,0.0004,0.01,0.01

테트라미졸 (Tetramisole),0.0006,0.0004,0.0006,0.01,0.01

테트라싸이클린 (Tetracycline),0.003,0.003,0.0005,0.003,0.002

툴라스로마이신 (Tulathromycin),0.0006,0.0007,0.0004,0.01,0.01

트리메토프림 (Trimethoprim),0.0002,0.0005,0.0001,0.001,0.0004

트리클라벤다졸 (Triclabendazole),0.0004,0.0002,0.0003,0.01,0.01

케토 트리클라벤다졸 (Keto triclabendazole),0.0006,0.0004,0.001,0.01,-

트리클로르폰 (Trichlorfon, Metrifonate),0.006,0.001,0.001,0.001,0.01

티아물린 (Tiamulin),0.0006,0.0006,0.0004,0.0004,0.01

티아벤다졸 (Thiabendazole),0.0006,0.0003,0.0003,0.01,0.01

5-하이드록시 티아벤다졸 (5-Hydroxy thiabendazole),0.0002,0.0002,0.0003,0.01,0.01

티암페니콜 (Thiamphenicol),0.0007,0.0007,0.001,0.001,0.01

틸디피로신 (Tildipirosin),0.002,0.001,0.003,0.01,0.01

틸미코신 (Tilmicosin),0.0005,0.0005,0.0005,0.01,0.01

페노뷰카브 (Fenobucarb),0.001,0.001,0.001,0.001,0.01

페니실린 V (Penicillin V),0.001,0.001,0.0007,0.01,0.01

페반텔 (Febantel),0.0003,0.0005,0.0002,0.01,0.01

페플록사신 (Pefloxacin),0.0007,0.0007,0.0007,0.0007,0.0007

펜벤다졸 (Fenbendazole),0.0005,0.0003,0.0003,0.01,0.01

푸마길린 (Fumagillin),-,-,-,0.007,0.01

프라지콴텔 (Praziquantel),0.001,0.0009,0.0009,0.0009,0.01

플로르페니콜 (Florfenicol),0.0004,0.0005,0.0005,0.0005,0.001

플로르페니콜 아민 (Florfenicol amine),-,-,-,-,-

플루닉신 (Flunixin),0.0004,0.0004,0.0009,0.01,0.01

5-하이드록시 플루닉신 (5-Hydroxy flunixin),-,-,0.005,-,-

플루메퀸 (Flumequin),0.0008,0.0005,0.0007,0.0004,0.0004

플루벤다졸 (Flubendazole),0.0004,0.0002,0.0004,0.01,0.01

2-아미노 플루벤다졸 (2-Amino flubendazole),0.0009,0.001,0.0007,0.01,0.01

분석성분 (Compound),식육,알(卵),유(乳),어류,갑각류

난드롤론 (Nandrolone),0.001,0.008,0.001,0.01,0.01

날록손 (Naloxone),0.0006,0.0009,0.0004,0.01,0.01

노보비오신 (Novobiocin),0.0013,0.0001,0.0005,0.01,0.01

나이카바진 (Nicarbazin, N,N‘-bis-(4-nitrophenyl)urea),0.0006,0.005,0.0003,0.01,0.01

답손 (Dapsone),0.005,0.005,0.005,0.005,0.005

모노아세틸답손 (Monoacetyl dapsone),0.005,0.005,0.005,0.005,0.005

더콴텔 (Derquantel),0.005,0.0003,0.005,-,0.01

디메트리다졸 (Dimetridazole),0.0005,0.0005,0.0005,0.0005,0.0005

2-하이드록시메틸-1-메틸-5-니트로이미다졸 (2-hydroxymethyl-1-methyl-5-nitroimidazole(HMMNI)),0.002,0.002,0.002,0.002,0.002

디미나진 (Diminazene),0.004,0.004,0.0009,-,-

디에틸카바마진 (Diethylcarbamazine),0.0004,0.003,0.0004,0.01,0.01

디클라주릴 (Diclazuril),0.0008,0.0001,0.0002,0.01,0.01

디펜하이드라민 (Diphenhydramine),0.0002,0.0001,0.0004,0.01,0.01

락토파민 (Ractopamine),0.0005,0.0002,0.0001,0.01,0.01

로니다졸 (Ronidazole),0.0005,0.0005,0.0005,0.0005,0.0005

2-하이드록시메틸-1-메틸-5-니트로이미다졸 (2-hydroxymethyl-1-methyl-5-nitroimidazole(HMMNI)),0.002,0.002,0.002,0.002,0.002

로베니딘 (Robenidine),0.005,0.0005,0.001,0.01,0.01

로페라미드 (Loperamide),0.0001,0.0002,0.005,0.01,0.01

록사손 (Roxarsone),0.004,0.004,0.004,0.002,0.002

메토밀 (Methomyl),0.003,0.0008,0.0002,-,-

메토크로프라미드 (Metoclopramide),0.0001,0.0004,0.0002,0.01,0.01

메트로니다졸 (Metronidazole),0.0005,0.0005,0.0005,0.0005,0.0005

메트로니다졸-OH (Metronidazole-OH),0.0005,0.0005,0.0005,0.0005,0.0005

모란텔 (Morantel),0.002,0.0008,0.002,0.01,0.01

바시트라신 (Bacitracin),0.005,0.003,0.001,0.01,0.01

발네물린 (Valnemulin),0.0003,0.0006,0.0002,0.01,0.01

버지니아마이신 (Virginiamycin M1),0.0007,0.0002,0.0001,0.01,0.01

베르베린 (Berberine),0.0002,0.0005,0.002,0.01,0.01

석시닐-설파티아졸 (Succinyl-sulfathiazole),0.005,0.001,0.001,0.001,0.01

설파모졸 (Sulfamoxol),0.0009,0.0005,0.005,0.0005,0.01

설파미터 (Sulfameter),0.0009,0.0003,0.0002,0.001,0.01

설파벤자미드 (Sulfabenzamide),0.0005,0.0005,0.0005,0.0005,0.01

설파세타미드 (Sulfacetamide),0.0005,0.0005,0.0005,0.0005,0.01

설파피리딘 (Sulfapyridine),0.0005,0.0005,0.0005,0.0005,0.01

설피소미딘 (Sulfisomidine),0.0005,0.0005,0.0005,0.0005,0.01

설피린 (Sulpyrine, Dipyrone, Metamizole, 4-methylamino antipyrine),0.005,0.0003,0.005,0.01,0.01

세파졸린 (Cefazolin),0.003,0.001,0.002,0.01,0.01

세포페라존 (Cefoperazone),0.005,0.0004,0.003,0.01,0.01

스코폴라민 (Scopolamine),0.0007,0.0006,0.0004,0.01,0.01

시프로헵타딘 (Cyproheptadine),0.0003,0.0001,0.0006,0.01,0.01

아세트아닐라이드 (Acetanilide),0.001,0.001,0.002,0.01,0.01

아자페론 (Azaperone),0.0003,0.0001,0.0002,0.01,0.01

아자페롤 (Azaperol),0.0003,0.0001,0.0002,0.01,0.01

아크리플라빈 (Acriflavine, Euflavine),0.001,0.002,0.0005,0.01,0.01

안티피린 (Antipyrine, Phenazone),0.0005,0.0007,0.0004,0.01,0.01

알트레노제스트 (Altrenogest),0.0003,0.0003,0.0006,0.01,0.01

에마멕틴 (Emamectin benzoate),0.0001,0.0003,0.0002,0.01,0.01

에프로토마이신 (Efrotomycin),0.004,0.005,0.0006,0.01,0.01

염산메틸에페드린 (DL-methylephedrine HCl),0.0004,0.0002,0.0007,0.01,0.01

옥시클로자니드 (Oxyclozanide),0.0003,0.0002,0.0004,0.01,0.01

올라퀸독스 (Olaquindox),0.004,0.004,0.004,0.004,0.004

요힘빈 (Yohimbine),0.0005,0.0004,0.0004,0.01,0.01

이미도캅 (Imidocarb),0.0003,0.0002,0.0001,0.01,0.01

이소메타미디움 (Isometamidium),0.004,0.0005,0.005,0.01,0.01

이프로니다졸 (Ipronidazole),0.0005,0.0005,0.0005,0.0005,0.0005

이프로니다졸-OH (Ipronidazole-OH),0.0005,0.0005,0.0005,0.0005,0.0005

질파테롤 (Zilpaterol),-,-,-,0.01,0.01

카라졸롤 (Carazolol),0.0008,0.0004,0.0004,0.01,0.01

카바독스 (Carbadox),0.004,0.004,0.004,0.004,0.004

카벤다짐 (Carbendazim),0.0002,0.0004,0.0001,0.01,0.01

케토프로펜 (Ketoprofen),0.003,0.0005,0.003,0.01,0.01

쿠마포스 (Coumaphos),0.001,0.0003,0.0009,0.01,0.01

쿠마포스 옥손 (Coumaphos oxon),-,-,-,-,-

콜치신 (Colchicine),0.0005,0.0005,0.0005,0.0005,0.0005

클렌부테롤 (Clebuterol),0.0002,0.0002,0.0002,0.0002,0.0002

클로르프로마진 (Chlorpromazine),0.001,0.001,0.001,0.001,0.001

클로산텔 (Closantel),0.005,0.005,0.0005,0.01,0.01

클로술론 (Clorsulon),0.003,0.001,0.0003,0.01,0.01

클로피돌 (Clopidol),0.005,0.004,0.001,0.01,0.01

테트라메트린 (Tetramethrin),0.005,0.003,0.005,-,-

테트라크로르빈포스 (Tetrachlorvinphos),0.003,0.002,0.003,0.01,0.01

톨트라주릴 설폰 (Toltrazuril sulfone),0.02,0.002,0.01,0.01,0.01

트리페레나민 (Tripelennamine),0.001,0.0003,0.004,0.01,0.01

티니다졸 (Tinidazole),0.0008,0.001,0.002,0.01,0.01

펄리마이신 (Pirlimycin),0.0004,0.0004,0.0001,0.01,0.01

페나세틴 (Phenacetin),0.0004,0.0005,0.001,0.01,0.01

프로폭서 (Propoxur),0.0002,0.0003,0.0002,0.01,0.01

플루아주론 (Fluazuron),0.0004,0.0001,0.0001,0.01,0.01

피리메타민 (Pyrimethamine),0.0001,0.0001,0.0001,0.0001,0.0001

할로푸지논 (Halofuginone),0.001,0.0002,0.0005,0.01,0.01

질량분석(MS) 조건 보기 (6항목)

이온화 방법: 가) 이온화 방법: ESI(Positive ion mode, Negative ion mode)
Capillary temperature: 나) Capillary temperature: 500℃
Capillary voltage: 다) Capillary voltage: 3.6 kV(Positive), 2.8 kV(Negative)
Collision gas: 라) Collision gas: 아르곤(Ar) 또는 이와 동등한 것
전이표: null
전이표_다중: 연번,분석성분 (Compound),머무름 시간 (분),이온화 (Ionization mode),분자량 (MW),관측질량 (Exact Mass),선구이온 (Precusor ion, m/z),생성이온 (Product ion, m/z),충돌 에너지 (Collision Energy, eV) 1,나프실린 (Nafcillin),6.86,Positive,414.5,414.1,415.1,115.1,55 171.2,36 199.21),16 2,날리딕스산 (Nalidixic acid),6.22,Positive,232.2,232.1,233.0,104.01),42 131.0,36 159.0,32 3,노르플록사신 (Norfloxacin),3.88,Positive,319.3,319.1,320.0,205.0,32 256.1,22 233.11),24 4,다노플록사신 (Danofloxacin),4.02,Positive,357.4,357.1,357.9,96.0,25 314.0,19 340.01),24 5,데하이드로콜산 (Dehydrocholic acid),6.35,Negative,402.5,402.2,401.1,214.9,35 249.0,33 331.31),25 6,독시싸이클린 (Doxycycline),4.86,Positive,444.4,444.2,445.1,154.3,31 321.2,30 428.21),19 7,디아베리딘 (Diaveridine),3.74,Positive,260.2,260.1,261.0,81.1,43 123.1,23 245.11),27 8,디클록사실린 (Dicloxacillin),7.04,Positive,470.3,469.0,469.7,114.01),40 160.0,16 311.0,15 9,디플록사신 (Difloxacin),4.45,Positive,399.4,399.1,400.0,279.1,38 284.9,32 299.01),29 10,레바미졸 (Levamisole),3.76,Positive,204.2,204.1,205.1,91.1,40 123.1,35 178.11),25 11,록시스로마이신 (Roxithromycin),5.96,Positive,837.0,836.5,837.4,116.3,47 158.31),34 679.5,22 12,리팍시민 (Rifaximin),7.20,Positive,785.9,785.4,786.2,123.2,44 151.2,34 754.41),23 13,린코마이신 (Lincomycin),3.62,Positive,406.5,406.2,407.2,126.31),26 359.3,18 389.3,18 14,마보플록사신 (Marbofloxacin),3.83,Positive,362.4,362.1,363.0,72.11),24 319.9,16 345.0,22 15,메벤다졸 (Mebendazole),5.78,Positive,295.2,295.1,296.1,77.1,50 105.0,35 264.01),25 메벤다졸 아민 (Mebendazole amine),4.60,Positive,237.2,237.1,238.1,77.3,42 105.21),36 133.0,25 5-하이드록시 메벤다졸 (5-Hydroxy mebendazole),4.60,Positive,297.3,297.1,298.1,79.3,40 160.2,33 266.21),21 16,멜록시캄 (Meloxicam),7.05,Positive,351.4,351.0,351.9,72.9,51 114.91),22 140.9,21 17,미노싸이클린 (Minocycline),3.75,Positive,457.4,457.2,458.1,283.2,45 352.2,31 441.31),20 18,벤질페니실린 (Benzylpenicillin, Penicillin G, Procaine benzylpenicillin),5.86,Positive,334.4,334.1,335.4,114.0,30 160.11),15 176.1,15 19,비치오놀 (Bithionol),8.04,Negative,356.0,355.9,354.9,160.71),23 162.7,23 191.7,25 20,사라플록사신 (Sarafloxacin),4.40,Positive,385.4,385.1,386.0,299.01),27 322.1,25 348.1,34 21,설파구아니딘 (Sulfaguanidine),1.85,Positive,214.2,214.1,215.0,60.1,14 95.11),26 156.0,14 22,설파독신 (Sulfadoxine),5.18,Positive,310.3,310.1,311.0,92.0,30 108.0,25 156.01),19 23,설파디메톡신 (Sulfadimethoxine),5.75,Positive,310.3,310.1,311.0,92.0,34 108.01),31 156.0,21 24,설파디아진 (Sulfadiazine),3.82,Positive,250.2,250.1,251.0,92.0,27 108.01),23 155.9,15 25,설파메라진 (Sulfamerazine),4.25,Positive,264.3,264.1,265.0,92.0,28 108.0,26 156.01),16 26,설파메타진 (Sulfamethazine),4.54,Positive,278.3,278.1,279.0,92.01),32 124.0,24 186.0,18 27,설파메톡사졸 (Sulfamethoxazole),5.25,Positive,253.2,253.1,254.0,92.01),28 108.0,23 155.9,15 28,설파메톡시피리다진 (Sulfamethoxypyridazine),4.56,Positive,280.3,280.1,281.0,92.0,30 108.0,27 156.01),17 29,설파모노메톡신 (Sulfamonomethoxine),4.85,Positive,280.3,280.1,281.0,92.0,28 108.0,27 156.01),17 30,설파퀴녹살린 (Sulfaquinoxaline),5.66,Positive,300.3,300.1,301.0,108.0,27 156.01),19 208.0,17 31,설파클로르피라진 (Sulfachlorpyrazine, Sulfaclozine),5.66,Positive,284.7,284.0,285.0,92.1,27 108.1,25 130.11),20 32,설파클로르피리다진 (Sulfachlorpyridazine),5.04,Positive,284.7,284.0,285.0,92.1,27 108.1,23 156.11),14 33,설파티아졸 (Sulfathiazole),3.94,Positive,255.3,255.0,256.0,92.0,27 108.0,24 156.01),14 34,설파페나졸 (Sulfaphenazole),5.77,Positive,314.4,314.1,315.1,92.1,34 131.1,28 158.11),22 35,설피속사졸 (Sulfisoxazole),5.39,Positive,267.3,267.1,268.0,92.0,27 113.0,16 155.91),15 36,세파드록실 (Cefadroxil),3.25,Positive,363.4,363.1,364.1,86.2,47 114.21),20 208.2,10 37,세팔렉신 (Cefalexin),3.84,Positive,347.4,347.1,348.0,106.1,30 158.01),13 174.0,15 38,세프티오퍼 (Ceftiofur),5.23,Positive,523.6,523.0,524.0,125.0,53 241.01),20 285.0,18 데스후로일 세프티오퍼 (Desfuroylceftiofur),4.35,Positive,429.5,429.0,430.0,126.01),29 227.0,24 241.1,16 39,스피라마이신 (Spiramycin),4.38,Positive,843.1,842.5,843.5,101.1,46 174.11),38 142.1,36 40,시프로플록사신 (Ciprofloxacin),3.95,Positive,331.3,331.1,332.1,231.2,36 245.2,24 314.21),20 41,아목시실린 (Amoxicillin),3.11,Positive,365.4,365.1,365.8,114.0,27 134.0,30 349.11),10 42,알벤다졸 (Albendazole),5.77,Positive,265.3,265.1,266.1,131.1,48 159.1,37 191.11),31 알벤다졸 설폭사이드 (Albendazole sulfoxide),4.29,Positive,281.3,281.1,282.0,159.1,40 208.11),23 240.1,13 알벤다졸 설폰 (Albendazole sulfone),5.07,Positive,297.3,297.1,297.6,159.1,37 224.1,26 266.11),20 2-아미노 알벤다졸 설폰 (2-Aminoalbendazole sulfone),3.74,Positive,239.3,239.1,240.0,105.1,51 133.1,18 198.11),28 43,암피실린 (Ampicillin),3.81,Positive,349.4,349.1,350.0,79.1,52 106.01),22 114.0,33 44,에리스로마이신 (Erythromycin),5.33,Positive,733.9,733.5,734.1,116.0,43 158.11),30 576.2,20 45,에토파베이트 (Ethopabate),5.59,Positive,237.2,237.1,238.0,136.11),28 164.1,19 206.1,11 m-페네티딘 (m-phenetidine),3.99,Positive,137.1,137.1,138.3,65.2,25 93.2,21 110.21),16 46,엔로플록사신 (Enrofloxacin),4.14,Positive,359.4,359.2,360.1,203.0,37 245.01),28 285.9,34 47,오르메토프림 (Ormethoprim),4.07,Positive,274.3,274.1,275.1,81.0,46 123.0,28 258.91),24 48,오비플록사신 (Orbifloxacin),4.24,Positive,395.4,395.1,396.0,253.91),31 295.0,25 352.1,19 49,오플록사신 (Ofloxacin),3.90,Positive,361.4,361.1,362.0,205.0,42 218.9,39 261.01),27 50,옥사실린 (Oxacillin),6.47,Positive,401.4,401.1,401.8,114.01),36 160.0,15 243.1,15 51,옥소린산 (Oxolinic acid),5.45,Positive,261.2,261.1,262.0,160.0,37 216.0,29 244.01),18 52,옥스펜다졸 (Oxfendazole),4.95,Positive,315.3,315.1,316.0,159.11),30 191.1,21 283.1,19 옥스펜다졸 설폰 (Oxfendazole sulfone),5.74,Positive,331.3,331.1,332.0,131.1,50 159.1,39 300.01),22 53,옥시벤다졸 (Oxibendazole),5.00,Positive,249.2,249.1,250.0,148.1,35 176.1,30 218.11),20 54,옥시테트라싸이클린 (Oxytetracycline),4.01,Positive,460.4,460.1,461.2,201.2,37 426.21),20 443.2,12 55,올레안도마이신 (Oleandomycin),5.16,Positive,687.9,687.4,688.4,116.1,45 158.11),28 544.3,18 56,조사마이신 (Josamycin),6.19,Positive,828.0,827.5,828.1,83.1,51 109.11),42 174.1,34 57,클로람페니콜 (Chloramphenicol),5.45,Negative,323.1,322.0,321.0,120.9,30 152.21),16 257.9,11 58,클로르테트라 싸이클린 (Chlortetracycline),4.74,Positive,478.9,478.1,479.1,98.0,43 154.01),30 443.9,22 59,클록사실린 (Cloxacillin),6.77,Positive,435.9,435.3,436.1,114.2,38 160.21),33 178.1,18 60,클린다마이신 (Clindamycin),4.73,Positive,425.0,424.2,424.9,82.8,55 126.11),29 377.1,21 61,키타사마이신 (Kitasamycin),5.76,Positive,828.0,771.4,772.4,83.2,50 109.11),45 174.1,35 62,타일로신 (Tylosin A),5.44,Positive,916.1,915.5,916.4,101.2,49 174.31),38 772.5,31 63,테트라미졸 (Tetramisole),3.76,Positive,204.2,204.1,205.1,91.2,27 123.2,37 178.21),20 64,테트라싸이클린 (Tetracycline),4.21,Positive,444.4,444.2,445.1,154.2,27 410.21),20 427.2,14 65,툴라스로마이신 (Tulathromycin),3.83,Positive,806.1,805.6,403.7,72.31),26 116.3,24 158.3,21 66,트리메토프림 (Trimethoprim),3.91,Positive,290.3,290.1,291.1,123.0,26 230.01),24 261.0,26 67,트리클라벤다졸 (Triclabendazole),7.58,Positive,359.7,358.0,359.0,171.1,53 274.0,37 346.01),26 케토 트리클라벤다졸 (Keto triclabendazole),7.19,Negative,329.6,328.0,327.0,118.0,40 146.1,33 182.21),25 68,트리클로르폰 (Trichlorfon, Metrifonate),4.70,Positive,257.4,255.9,256.9,79.1,30 109.21),20 223.0,10 69,티아물린 (Tiamulin),5.96,Positive,493.7,493.3,494.0,73.0,55 119.01),39 191.9,25 70,티아벤다졸 (Thiabendazole),3.72,Positive,201.2,201.0,201.9,65.1,45 131.1,35 175.01),25 5-하이드록시 티아벤다졸 (5-Hydroxy thiabendazole),3.38,Positive,217.2,217.0,217.9,81.1,45 147.0,35 191.01),25 71,티암페니콜 (Thiamphenicol),4.38,Negative,356.2,355.0,353.9,185.11),21 240.1,16 290.0,13 72,틸디피로신 (Tildipirosin),5.33,Positive,734.0,733.5,734.5,88.1,55 98.01),41 174.1,39 73,틸미코신 (Tilmicosin),4.79,Positive,869.1,868.6,869.7,88.2,60 174.31),55 696.5,45 74,페노뷰카브 (Fenobucarb),7.28,Positive,207.2,207.1,208.1,77.1,36 95.21),16 152.2,10 75,페니실린 V (Penicillin V),6.27,Negative,350.4,350.1,349.1,93.1,30 114.0,20 208.11),10 76,페반텔 (Febantel),7.41,Positive,446.5,446.1,447.0,281.2,32 384.21),20 416.2,14 77,페플록사신 (Pefloxacin),3.93,Positive,333.3,333.1,334.1,233.2,26 290.3,17 316.31),21 78,펜벤다졸 (Fenbendazole),6.49,Positive,299.3,299.1,300.0,104.1,55 131.1,48 268.11),21 79,푸마길린 (Fumagillin),7.43,Positive,458.5,458.2,459.2,103.2,50 131.11),28 177.1,17 80,프라지콴텔 (Praziquantel),6.97,Positive,312.4,312.2,313.1,83.1,28 174.0,25 203.11),17 81,플로르페니콜 (Florfenicol),5.29,Negative,358.2,357.0,355.9,151.8,19 185.1,16 336.01),10 플로르페니콜 아민 (Florfenicol amine),1.18,Positive,247.2,247.1,248.0,91.1,49 130.1,23 230.11),12 82,플루닉신 (Flunixin),7.19,Positive,296.2,296.1,297.1,109.1,48 236.1,42 264.11),32 5-하이드록시 플루닉신 (5-Hydroxy flunixin),6.78,Positive,312.2,312.2,312.9,279.91),34 295.0,23 266.9,13 83,플루메퀸 (Flumequin),6.31,Positive,261.2,261.1,262.0,126.0,50 202.0,33 244.01),18 84,플루벤다졸 (Flubendazole),6.02,Positive,313.2,313.1,314.0,95.1,50 123.1,35 282.11),24 2-아미노 플루벤다졸 (2-Amino flubendazole),4.78,Positive,255.2,255.1,256.0,75.1,55 95.11),39 133.1,37
연번,분석성분 (Compound),머무름 시간 (분),이온화 (Ionization mode),분자량 (MW),관측질량 (Exact Mass),선구이온 (Precusor ion, m/z),생성이온 (Product ion, m/z),충돌 에너지 (Collision Energy, eV) 1,난드롤론 (Nandrolone),6.80,Positive,274.4,274.2,275.1,109.11),26 257.2,16 239.2,17 2,날록손 (Naloxone),3.53,Positive,327.4,327.1,328.0,212.01),40 253.1,27 268.0,27 3,노보비오신 (Novobiocin),7.57,Positive,612.6,612.2,612.9,133.01),53 189.0,28 218.0,15 4,나이카바진 (Nicarbazin, N,N‘-bis-(4-nitrophenyl)urea),7.25,Negative,426.4,302.1,301.1,46.1,55 107.1,35 137.21),14 5,답손 (Dapsone),4.91,Positive,248.3,248.1,249.0,92.01),25 108.1,22 156.0,14 모노아세틸답손 (Monoacetyl dapsone),5.06,Positive,290.3,290.1,291.0,92.01),30 108.1,23 156.1,17 6,더콴텔 (Derquantel),5.42,Positive,479.6,479.3,480.0,148.3,42 405.3,31 462.21),26 7,디메트리다졸 (Dimetridazole),3.88,Positive,141.1,141.1,142.1,81.1,26 95.1,23 96.11),15 2-하이드록시메틸-1-메틸-5- 니트로이미다졸 (2-hydroxymethyl-1-methyl-5-nitroimidazole (HMMNI)),3.51,Positive,157.1,157.0,158.0,42.1,34 55.1,19 140.11),15 8,디미나진 (Diminazene),3.05,Positive,281.3,281.1,282.0,102.1,37 119.11),17 254.2,9 9,디에틸카바마진 (Diethylcarbamazine),3.34,Positive,199.2,199.2,200.1,72.01),24 100.1,16 127.0,15 10,디클라주릴 (Diclazuril),7.46,Negative,407.6,406.0,405.0,299.0,28 334.01),19 335.1,19 11,디펜하이드라민 (Diphenhydramine),5.48,Positive,255.3,255.2,256.1,115.0,55 152.0,35 167.11),13 12,락토파민 (Ractopamine),4.10,Positive,301.4,301.2,302.1,107.01),34 121.0,23 284.1,13 13,로니다졸 (Ronidazole),3.84,Positive,200.1,200.1,201.0,55.01),23 110.0,18 140.0,12 2-하이드록시메틸-1-메틸-5- 니트로이미다졸 (2-hydroxymethyl-1-methyl-5-nitroimidazole (HMMNI)),3.51,Positive,157.1,157.0,158.0,42.1,34 55.1,19 140.11),15 14,로베니딘 (Robenidine),6.50,Positive,334.2,333.1,333.9,111.0,50 138.0,25 155.11),20 15,로페라미드 (Loperamide),6.50,Positive,477.0,476.2,477.0,72.0,51 210.0,51 266.01),25 16,록사손 (Roxarsone),3.33,Negative,263.0,262.9,262.0,123.1,25 153.1,20 244.01),11 17,메토밀 (Methomyl),4.30,Positive,162.2,162.0,163.2,73.1,27 88.21),9 106.1,11 18,메토크로프라미드 (Metoclopramide),4.27,Positive,299.7,299.1,299.8,140.91),49 184.0,31 226.9,20 19,메트로니다졸 (Metronidazole),3.47,Positive,171.1,171.1,171.8,82.01),25 98.0,22 111.0,23 메트로니다졸-OH (Metronidazole-OH),3.14,Positive,187.1,187.1,188.0,68.1,22 123.11),13 126.0,17 20,모란텔 (Morantel),4.64,Positive,220.3,220.1,221.2,111.11),25 123.0,35 164.0,25 21,바시트라신 (Bacitracin),4.74,Positive,1422.7,1421.7,475.2,86.11),22 110.1,49 199.1,28 22,발네물린 (Valnemulin),6.11,Positive,564.8,564.4,565.0,147.01),39 164.0,32 263.1,19 23,버지니아마이신 (VirginiamycinM1),6.55,Positive,525.5,525.2,525.9,109.1,34 133.0,28 355.11),19 24,베르베린 (Berberine),5.32,Positive,336.4,336.1,336.0,263.01),53 278.0,43 304.0,33 25,석시닐-설파티아졸 (Succinyl-sulfathiazole),4.18,Positive,355.4,355.0,356.0,108.1,27 192.1,24 256.1),17 26,설파모졸 (Sulfamoxol),4.37,Positive,267.3,267.1,268.1,92.1,25 108.1,25 156.01),15 27,설파미터 (Sulfameter),4.62,Positive,280.3,280.1,281.1,92.1,30 108.1,25 156.11),19 28,설파벤자미드 (Sulfabenzamide),5.66,Positive,276.3,276.1,277.1,92.1,25 108.1,21 156.01),15 29,설파세타미드 (Sulfacetamide),3.65,Positive,214.2,214.0,215.1,92.1,23 108.1,21 156.01),11 30,설파피리딘 (Sulfapyridine),4.11,Positive,249.2,249.1,250.1,92.1,26 108.1,25 156.01),16 31,설피소미딘 (Sulfisomidine),3.56,Positive,278.3,278.1,279.1,92.1,30 124.11),20 186.1,20 32,설피린 (Sulpyrine, Dipyrone, Metamizole, 4-methylamino antipyrine),3.43,Positive,351.3,217.1,218.1,56.11),25 97.1,13 187.1,11 33,세파졸린 (Cefazolin),4.39,Positive,454.5,454.0,454.7,155.91),18 294.9,17 323.0,13 34,세포페라존 (Cefoperazone),4.78,Positive,645.7,645.1,645.8,143.01),36 148.0,52 530.0,12 35,스코폴라민 (Scopolamine),3.85,Positive,303.3,303.1,303.8,103.01),38 138.0,22 156.0,17 36,시프로헵타딘 (Cyproheptadine),5.86,Positive,287.4,287.2,288.2,96.11),25 191.1,30 215.1,48 37,아세트아닐라이드 (Acetanilide),4.92,Positive,135.1,135.1,135.9,43.0,31 51.0,50 77.01),30 38,아자페론 (Azaperone),4.35,Positive,327.4,327.2,328.2,95.1,64 121.1,19 123.11),44 아자페롤 (Azaperol),4.05,Positive,329.4,329.2,330.2,109.1,57 121.11),20 149.1,30 39,아크리플라빈 (Acriflavine, Euflavine),4.24,Positive,469.0,224.1,223.9,154.01),54 164.9,48 209.0,27 40,안티피린 (Antipyrine, Phenazone),4.58,Positive,188.2,188.1,188.9,56.01),34 58.5,34 104.0,25 41,알트레노제스트 (Altrenogest),7.40,Positive,310.4,310.2,311.0,227.11),24 269.1,15 293.4,18 42,에마멕틴 (Emamectin benzoate),7.38,Positive,1008.2,885.5,886.2,82.1,55 126.2,43 158.01),35 43,에프로토마이신 (Efrotomycin),7.10,Negative,1145.3,1144.6,1143.6,274.2,49 773.4,34 791.31),27 44,염산메틸에페드린 (DL-methylephedrine HCl),3.70,Positive,179.2,179.1,179.9,57.0,19 117.01),21 147.1,22 45,옥시클로자니드 (Oxyclozanide),7.60,Negative,401.4,400.9,399.9,202.1,22 363.91),17 381.9,22 46,올라퀸독스 (Olaquindox),4.63,Positive,263.2,188.1,189.0,102.0,32 143.0,16 145.01),16 47,요힘빈 (Yohimbine),4.69,Positive,354.4,354.2,355.1,117.01),52 144.0,31 212.1,24 48,이미도캅 (Imidocarb),3.26,Positive,348.4,348.2,349.0,145.1,55 162.2,25 188.11),29 49,이소메타미디움 (Isometamidium),4.45,Positive,460.6,460.2,460.2,269.1,50 298.11),25 313.1,20 50,이프로니다졸 (Ipronidazole),5.59,Positive,169.1,169.1,170.1,109.11),26 123.1,25 124.1,19 이프로니다졸-OH (Ipronidazole-OH),4.71,Positive,185.1,185.1,186.1,121.1,29 122.2,20 168.21),15 51,질파테롤 (Zilpaterol),3.12,Positive,261.3,261.1,262.2,185.11),25 202.1,19 244.2,14 52,카라졸롤 (Carazolol),4.91,Positive,298.4,298.2,299.2,116.11),21 194.1,30 222.1,20 53,카바독스 (Carbadox),4.42,Positive,262.2,174.0,174.8,102.01),32 129.0,18 131.0,16 54,카벤다짐 (Carbendazim),3.67,Positive,191.1,191.1,192.0,105.1,35 132.2,29 160.11),18 55,케토프로펜 (Ketoprofen),6.99,Positive,254.2,254.1,255.1,77.1,45 105.0,22 209.11),15 56,쿠마포스 (Coumaphos),7.71,Positive,362.8,362.0,363.0,227.01),25 307.0,18 335.0,17 쿠마포스 옥손 (Coumaphos oxon),7.08,Positive,346.7,346.0,347.0,291.01),24 221.0,33 57,콜치신 (Colchicine),5.29,Positive,399.4,399.2,400.1,310.2,27 326.2,24 358.21),23 58,클렌부테롤 (Clenbuterol),4.53,Positive,277.1,276.1,277.0,140.01),46 168.0,31 203.0,17 59,클로르프로마진 (Chlorpromazine),6.18,Positive,318.9,318.1,319.1,58.1,30 86.11),20 246.0,24 60,클로산텔 (Closantel),8.55,Negative,663.1,661.9,660.8,127.01),50 315.1,34 345.0,36 61,클로술론 (Clorsulon),5.60,Negative,380.7,378.9,378.0,277.1,22 242.2,22 342.11),12 62,클로피돌 (Clopidol),3.73,Positive,192.0,191.0,192.0,51.1,44 87.1,30 101.11),26 63,테트라메트린 (Tetramethrin),8.02,Positive,331.4,331.2,332.0,135.1,17 164.11),24 314.2,10 64,테트라크로르빈포스 (Tetrachlorvinphos),7.57,Positive,366.0,365.9,367.0,127.11),21 205.9,37 65,톨트라주릴 설폰 (Toltrazuril sulfone),7.31,Negative,457.4,457.1,456.0,42.21),22 399.1,12 66,트리페레나민 (Tripelennamine),4.83,Positive,255.3,255.2,256.1,72.11),32 91.0,36 119.0,34 67,티니다졸 (Tinidazole),4.40,Positive,247.2,247.1,248.0,82.1,34 121.11),16 128.0,21 68,펄리마이신 (Pirlimycin),4.62,Positive,411.0,410.2,411.1,56.1,52 112.11),30 363.1,19 69,페나세틴 (Phenacetin),5.54,Positive,179.2,179.1,179.9,65.11),37 93.0,28 110.0,22 70,프로폭서 (Propoxur),6.53,Positive,209.2,209.1,210.1,93.0,24 111.01),15 168.1,9 71,플루아주론 (Fluazuron),7.85,Positive,506.2,505.0,506.0,158.01),20 141.0,48 349.0,19 72,피리메타민 (Pyrimethamine),4.95,Positive,248.7,248.1,249.1,177.0,30 198.1,45 233.11),28 73,할로푸지논 (Halofuginone),4.90,Positive,414.7,413.0,414.0,100.1,24 120.11),21 138.1,20

기울기 조건표

시간(분)	A(%)	B(%)
0.0	95	5
0.5	95	5
5.5	40	60
6.0	0	100
10.0	0	100
10.2	95	5
12.0	95	5

이 조건으로 Core-Shell 전환 계산하기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.

고시 원문 보기 (축자)

가) 컬럼: C18계 컬럼(2.1 mm × 150 mm, 3.5 μm) 또는 이와 동등한 것
나) 이동상
(1) 이동상 A: 0.1%(v/v) 포름산(formic acid) 함유한 수용액
(2) 이동상 B: 0.1%(v/v) 포름산(formic acid) 함유한 아세토니트릴
[표 1]
다) 이동상 유량: 0.3 mL/분
라) 컬럼 온도: 40℃
마) 주입량: 5 μL
2) 질량분석기 분석조건
가) 이온화 방법: ESI(Positive ion mode, Negative ion mode)
나) Capillary temperature: 500℃
다) Capillary voltage: 3.6 kV(Positive), 2.8 kV(Negative)
라) Collision gas: 아르곤(Ar) 또는 이와 동등한 것
마) 분석대상물질 조건
(1) 제 1그룹
[표 2]
1) 정량이온
(2) 제 2그룹
[표 3]
3) 검량선 작성
표준용액을 농도별로 일정량 취하여 액체크로마토그래프-질량분석기에 각각 주입하여 얻은 크로마토그램상의 각 피크 높이 또는 면적 값으로 검량선을 작성한다.
4) 정량한계
가) 제 1그룹
(단위: mg/kg)
[표 4]
나) 제 2그룹
(단위: mg/kg)
[표 5]

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 C18USP L1 상당

약전 일반명 '액체크로마토그래프용옥타데실실릴실리카겔'(USP 분류로는 L1 상당)에 해당. 약전은 브랜드를 지정하지 않으므로 각조가 기재한 물리 사양(치수·입자경 등)과 KP 통칙·일반시험법의 조정 허용범위 안에서 해당 상을 충족하는 C18을 선택할 수 있다 — 선택 기준은 시스템적합성(분리도·테일링·RSD) 통과 용이성과 재현성이다.

분석조건 (2)

LC기울기 용리8.3.1FD-축-수산물-중-동물용의약품-동시-다성분-시험법-x2

원문 표제 단서: 액체크로마토그래프

칼럼

C18 · USP L1

C18계 컬럼

안지름 2.1 mm · 길이 10 cm · 입자경 1.7 μm

칼럼온도

40℃

이동상

20 mM HFBA 함유한 5%(v/v) 아세토니트릴
20 mM HFBA 함유한 50%(v/v) 아세토니트릴

유량

0.3 mL/분

주입량

10 μL

기타표

겐타마이신 C1(6.77분),겐타마이신 C1a(6.59분)

겐타마이신 C2(6.65분),겐타마이신 C2a(6.79분)

네오마이신(6.93분),디히드로스트렙토마이신(4.10분)

스트렙토마이신(4.02분),스펙티노마이신(2.97분)

아미카신(4.95분),아프라마이신(6.14분)

카나마이신(5.19분),파로모마이신(6.93분)

하이그로마이신 B(3.78분),토브라마이신(6.32분)

(단위: mg/kg)

분석성분 (Compounds),소고기,돼지고기,닭고기,알(卵),유(乳),넙치,장어,새우

겐타마이신 C1 (Gentamicin C1),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

겐타마이신 C1a (Gentamicin C1a),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

겐타마이신 C2 (Gentamicin C2),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

겐타마이신 C2a (Gentamicin C2a),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

네오마이신 (Neomycin),0.01,0.05,0.01,0.01,0.01,0.01,0.01,0.01

디히드로 스트렙토마이신 (Dihydrostreptomycin),0.005,0.005,0.005,0.005,0.005,0.008,0.005,0.005

스트렙토마이신 (Streptomycin),0.005,0.005,0.005,0.005,0.005,0.008,0.005,0.005

스펙티노마이신 (Spectinomycin),0.01,0.005,0.005,0.005,0.005,0.005,0.005,0.005

아미카신 (Amikacin),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

아프라마이신 (Apramycin),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

카나마이신 (Kanamycin),0.005,0.005,0.005,0.01,0.005,0.005,0.005,0.005

파로모마이신 (Paromomycin),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

하이그로마이신 (Hygromycin B),0.005,0.005,0.005,0.005,0.005,0.005,0.005,0.005

질량분석(MS) 조건 보기 (5항목)

이온화 방법: 가) 이온화 방법: ESI(Positive ion mode)
Capillary temperature: 나) Capillary temperature: 400℃
Capillary voltage: 다) Capillary voltage: 1.2 kV
Collision gas: 라) Collision gas: 아르곤(Ar) 또는 이와 동등한 것
전이표: 분석성분 (Compound) 머무름 분자량 (MW) 관측질량 (Exact mass) 선구이온 (Precursor ion, m/z) 생성이온 ion, m/z) 충돌에너지 (Collision energy, eV)
겐타마이신 C1 (Gentamicin C1) 6.77 477.6 477.3 478.3 157.1 20
160.0 22
322.21) 14
겐타마이신 C1a (Gentamicin C1a) 6.59 449.5 449.3 450.3 112.0 26
160.0 22
322.21) 12
겐타마이신 C2 (Gentamicin C2) 6.65 463.6 463.3 464.3 112.0 42
160.0 20
322.21) 10
겐타마이신 C2a (Gentamicin C2a) 6.79 463.6 463.3 464.3 112.0 34
160.0 20
322.21) 12
네오마이신 (Neomycin) 6.93 614.6 614.3 615.2 160.61) 32
163.5 32
293.1 20
디히드로 스트렙토마이신 (Dihydrostreptomycin) 4.10 583.6 583.3 584.2 221.1 36
246.1 34
263.11) 28
스트렙토마이신 (Streptomycin) 4.02 581.6 581.3 582.3 221.1 38
246.1 36
263.11) 30
스펙티노마이신 (Spectinomycin) 2.97 332.3 332.2 350.9 189.1 25
207.1 16
333.21) 22
아미카신 (Amikacin) 4.95 585.6 585.3 586.4 163.11) 34
264.2 24
425.2 12
아프라마이신 (Apramycin) 6.14 539.6 539.3 540.3 217.11) 26
344.1 18
378.2 16
카나마이신 (Kanamycin) 5.19 484.5 484.2 485.2 163.01) 26
205.1 32
324.1 14
파로모마이신 (Paromomycin) 6.93 615.6 615.3 616.3 163.11) 36
293.1 22
324.2 20
하이그로마이신 B (Hygromycin B) 3.78 527.5 527.2 528.2 117.11) 28
257.0 28
352.1 12
토브라마이신(내부표준물질) (Tobramycin, IS) 6.32 467.5 467.3 468.2 163.01) 24

기울기 조건표

시간(분)	A(%)	B(%)
0.0	80	20
0.5	80	20
9.0	5	95
10.0	5	95
10.1	80	20
15.0	80	20

이 조건으로 Core-Shell 전환 계산하기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.

고시 원문 보기 (축자)

가) 컬럼: C18계 컬럼(2.1 mm × 100 mm, 1.7 μm) 또는 이와 동등한 것
나) 이동상
(1) 이동상 A: 20 mM HFBA 함유한 5%(v/v) 아세토니트릴
(2) 이동상 B: 20 mM HFBA 함유한 50%(v/v) 아세토니트릴
[표 1]
다) 이동상 유량: 0.3 mL/분
라) 컬럼온도: 40℃
마) 주입량: 10 μL
2) 질량분석기 분석조건
가) 이온화 방법: ESI(Positive ion mode)
나) Capillary temperature: 400℃
다) Capillary voltage: 1.2 kV
라) Collision gas: 아르곤(Ar) 또는 이와 동등한 것
마) 분석대상물질 조건
[표 2]
1) 정량이온
3) 검량선 작성표준용액을 농도별로 일정량 취하여 액체크로마토그래프-질량분석기에 각각 주입하여 얻은 크로마토그램상의 각 피크 높이 또는 면적 값으로 검량선을 작성한다.
4) 표준품 크로마토그램
[표 3]
그림 1. 표준품의 크로마토그램 예시.
5) 정량한계
[표 4]

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 C18USP L1 상당

분석조건 (3)

LC기울기 용리8.3.1FD-축-수산물-중-동물용의약품-동시-다성분-시험법-x3

원문 표제 단서: 액체크로마토그래프

칼럼

C8 · USP L7

C8계 컬럼

안지름 2.1 mm · 길이 10 cm · 입자경 3.5 μm

칼럼온도

35℃

이동상

0.3%(v/v) 포름산(formic acid) 함유한 수용액
0.3%(v/v) 포름산(formic acid) 함유한 아세토니트릴

유량

0.25 mL/분

주입량

10 μL

기타표

나라신(14.11분),라살로시드(11.7분)	마두라마이신(15.0분),모넨신(13.1분)	살리노마이신(12.9분),샘두라마이신(10.7분)
분석성분 (Compounds),정량한계(mg/kg)	식육,유(乳),알(卵),수산물	나라신(Narasin),0.01,0.002,0.003,0.002	라살로시드(Lasalocid A-Na),0.005,0.001,0.01,0.001	마두라마이신(Maduramycin),0.004,0.002,0.002,0.002	모넨신(Monensin-Na),0.009,0.002,0.004,0.002	살리노마이신(Salinomycin-Na),0.008,0.001,0.005,0.002	샘두라마이신(Semduramicin),0.005,0.002,0.003,0.002

질량분석(MS) 조건 보기 (5항목)

이온화 방법: 가) 이온화 방법: ESI(Positive ion mode)
Source temperature: 나) Source temperature: 350℃
Capillary voltage: 다) Capillary voltage: 4.0 kV
Collision gas: 라) Collision gas: 질소(N2) 또는 이와 동등한 것
전이표: 분석성분 (Compound) 머무름 시간 (분) 분자량 (MW) 관측질량 (Exact mass) 선구이온 (Precursor ion, m/z) 생성이온 (Product ion, m/z) 충돌에너지 (Collision energy, eV)
나라신 (Narasin) 14.11 765.0 764.5 787.5 431.31) 60
531.3 50
413.1 60
라살로시드 (Lasalocid A-Na) 11.71 612.8 612.4 613.2 377.11) 40
577.1 30
595.3 30
마두라마이신 (Maduramycin) 15.02 934.2 916.5 939.4 877.41) 30
895.2 50
859.0 50
모넨신 (Monensin-Na) 13.15 692.9 692.4 693.3 461.21) 60
479.2 60
501.2 60
살리노마이신 (Salinomycin-Na) 12.92 791.0 772.5 773.3 431.21) 60
531.2 50
265.2 60
샘두라마이신 (Semduramicin) 10.75 873.1 872.5 895.3 833.41) 30
851.2 30
815.1 30

기울기 조건표

시간(분)	A(%)	B(%)
0.0	50	50
10.0	10	90
14.0	10	90
15.0	0	100
25.0	0	100
25.5	50	50
30.0	50	50

이 조건으로 Core-Shell 전환 계산하기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.

고시 원문 보기 (축자)

가) 컬럼: C8계 컬럼(2.1 mm × 100 mm, 3.5 μm) 또는 이와 동등한 것
나) 이동상
(1) 이동상 A: 0.3%(v/v) 포름산(formic acid) 함유한 수용액
(2) 이동상 B: 0.3%(v/v) 포름산(formic acid) 함유한 아세토니트릴
[표 1]
다) 이동상 유량: 0.25 mL/분
라) 컬럼 온도: 35℃
마) 주입량: 10 μL
2) 질량분석기 분석조건
가) 이온화 방법: ESI(Positive ion mode)
나) Source temperature: 350℃
다) Capillary voltage: 4.0 kV
라) Collision gas: 질소(N2) 또는 이와 동등한 것
마) 분석대상물질 조건
[표 2]
1) 정량이온
3) 검량선 작성
4) 표준품 크로마토그램
[표 3]
그림 1. 표준품의 크로마토그램 예시.
5) 정량한계
[표 4]

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 C8USP L7 상당

약전 일반명 '옥틸실릴실리카겔'(USP L7)에 해당.

분석조건 (4)

LC기울기 용리8.3.1FD-축-수산물-중-동물용의약품-동시-다성분-시험법-x4

원문 표제 단서: 액체크로마토그래프

칼럼

C18 · USP L1

C18계 컬럼

안지름 2.1 mm · 길이 10 cm · 입자경 3 μm

칼럼온도

40℃

이동상

0.1%(v/v) 포름산(formic acid) 함유한 수용액
0.1%(v/v) 포름산(formic acid) 함유한 아세토니트릴

유량

0.35 mL/분

주입량

5 μL

기타표

데코퀴네이트(9.02분),디사이클라닐(2.10분)	암프롤리움(0.88분),죠렌(4.98분)	ANOT(3.46분)
분석성분 (Compound),정량한계(mg/kg)	식육,유(乳),알(卵),어류	데코퀴네이트(Decoquinate),0.1,0.004,0.004,0.004	디사이클라닐(Dicyclanil),0.003,0.003,0.002,0.003	암프롤리움(Amprolium),0.09,0.002,0.002,0.001	죠렌(Zoalene),0.2,0.001,0.002,0.004	*3-Amino-5-nitro-o-toluamide,0.003,0.001,0.002,0.004

질량분석(MS) 조건 보기 (4항목)

이온화 방법: 가) 이온화 방법: ESI(Positive ion mode, Negative ion mode)
Capillary temperature: 나) Capillary temperature: 350℃
Collision gas: 다) Collision gas: 질소(N2) 또는 이와 동등한 것
전이표: 연번 분석성분 (Compound) 머무름 시간 (분) 이온화 (Ionization mode) 분자량 (MW) 관측질량 (Exact mass) 선구이온 (Precursor ion, m/z) 생성이온 (Product ion, m/z) 충돌에너지 (Collision energy, eV)
1 데코퀴네이트 (Decoquinate) 9.02 Positive 417.5 417.3 418.2 372.11) 33.0
203.9 55.0
231.9 47.0
2 디사이클라닐 (Dicyclanil) 2.10 Positive 190.2 190.1 191.0 150.01) 27.0
149.8 29.0
163.1 23.0
3 암프롤리움 (Amprolium) 0.88 Positive 278.7 278.1 243.1 150.01) 17.0
93.8 19.0
122.0 31.0
4 죠렌 (Zoalene) 4.98 Negative 225.1 225.0 223.9 181.01) 14.0
42.0 36.0
151.0 22.0
*3-Amino-5-nitro-toluamide(ANOT) 3.46 Positive 195.1 195.1 196.0 107.01) 23.0
153.1 23.0
179.0 11.0

기울기 조건표

시간(분)	A(%)	B(%)
0.0	95	5
1.0	95	5
9.0	5	95
11.0	5	95
11.1	95	5
13.5	95	5

이 조건으로 Core-Shell 전환 계산하기

이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.

고시 원문 보기 (축자)

가) 컬럼: C18계 컬럼(2.1 mm × 100 mm, 3 μm) 또는 이와 동등한 것
나) 이동상
(1) 이동상 A: 0.1%(v/v) 포름산(formic acid) 함유한 수용액
(2) 이동상 B: 0.1%(v/v) 포름산(formic acid) 함유한 아세토니트릴
[표 1]
다) 이동상 유량: 0.35 mL/분
라) 컬럼 온도: 40℃
마) 주입량: 5 μL
2) 질량분석기 분석조건
가) 이온화 방법: ESI(Positive ion mode, Negative ion mode)
나) Capillary temperature: 350℃
다) Collision gas: 질소(N2) 또는 이와 동등한 것
라) 분석대상물질 조건
1) 정량이온
[표 2]
3) 검량선 작성
4) 표준품 크로마토그램
[표 3]
그림 1. 표준품의 크로마토그램 예시.
5) 정량한계
[표 4]

고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.

상 분류 C18USP L1 상당

같은 고정상을 쓰는 다른 품목

한 컬럼으로 몇 개 시험을 함께 받을 수 있는지 볼 때 씁니다.

C18 품목 보기 C8 품목 보기

공전이 개정되면

고시가 개정되면 이 페이지의 분석조건도 함께 갱신됩니다. 어떤 항목이 어떻게 바뀌었는지는 크로마톡 규제·약전 브리핑에 정리해 올립니다.

최신 규제·공전 개정 브리핑 보기 →

연번,분석성분 (Compound),머무름 시간 (분),이온화 (Ionization mode),분자량 (MW),관측질량 (Exact Mass),선구이온 (Precusor ion, m/z),생성이온 (Product ion, m/z),충돌 에너지 (Collision Energy, eV)	1,나프실린 (Nafcillin),6.86,Positive,414.5,414.1,415.1,115.1,55	171.2,36	199.21),16	2,날리딕스산 (Nalidixic acid),6.22,Positive,232.2,232.1,233.0,104.01),42	131.0,36	159.0,32	3,노르플록사신 (Norfloxacin),3.88,Positive,319.3,319.1,320.0,205.0,32	256.1,22	233.11),24	4,다노플록사신 (Danofloxacin),4.02,Positive,357.4,357.1,357.9,96.0,25	314.0,19	340.01),24	5,데하이드로콜산 (Dehydrocholic acid),6.35,Negative,402.5,402.2,401.1,214.9,35	249.0,33	331.31),25	6,독시싸이클린 (Doxycycline),4.86,Positive,444.4,444.2,445.1,154.3,31	321.2,30	428.21),19	7,디아베리딘 (Diaveridine),3.74,Positive,260.2,260.1,261.0,81.1,43	123.1,23	245.11),27	8,디클록사실린 (Dicloxacillin),7.04,Positive,470.3,469.0,469.7,114.01),40	160.0,16	311.0,15	9,디플록사신 (Difloxacin),4.45,Positive,399.4,399.1,400.0,279.1,38	284.9,32	299.01),29	10,레바미졸 (Levamisole),3.76,Positive,204.2,204.1,205.1,91.1,40	123.1,35	178.11),25	11,록시스로마이신 (Roxithromycin),5.96,Positive,837.0,836.5,837.4,116.3,47	158.31),34	679.5,22	12,리팍시민 (Rifaximin),7.20,Positive,785.9,785.4,786.2,123.2,44	151.2,34	754.41),23	13,린코마이신 (Lincomycin),3.62,Positive,406.5,406.2,407.2,126.31),26	359.3,18	389.3,18	14,마보플록사신 (Marbofloxacin),3.83,Positive,362.4,362.1,363.0,72.11),24	319.9,16	345.0,22	15,메벤다졸 (Mebendazole),5.78,Positive,295.2,295.1,296.1,77.1,50	105.0,35	264.01),25	메벤다졸 아민 (Mebendazole amine),4.60,Positive,237.2,237.1,238.1,77.3,42	105.21),36	133.0,25	5-하이드록시 메벤다졸 (5-Hydroxy mebendazole),4.60,Positive,297.3,297.1,298.1,79.3,40	160.2,33	266.21),21	16,멜록시캄 (Meloxicam),7.05,Positive,351.4,351.0,351.9,72.9,51	114.91),22	140.9,21	17,미노싸이클린 (Minocycline),3.75,Positive,457.4,457.2,458.1,283.2,45	352.2,31	441.31),20	18,벤질페니실린 (Benzylpenicillin, Penicillin G, Procaine benzylpenicillin),5.86,Positive,334.4,334.1,335.4,114.0,30	160.11),15	176.1,15	19,비치오놀 (Bithionol),8.04,Negative,356.0,355.9,354.9,160.71),23	162.7,23	191.7,25	20,사라플록사신 (Sarafloxacin),4.40,Positive,385.4,385.1,386.0,299.01),27	322.1,25	348.1,34	21,설파구아니딘 (Sulfaguanidine),1.85,Positive,214.2,214.1,215.0,60.1,14	95.11),26	156.0,14	22,설파독신 (Sulfadoxine),5.18,Positive,310.3,310.1,311.0,92.0,30	108.0,25	156.01),19	23,설파디메톡신 (Sulfadimethoxine),5.75,Positive,310.3,310.1,311.0,92.0,34	108.01),31	156.0,21	24,설파디아진 (Sulfadiazine),3.82,Positive,250.2,250.1,251.0,92.0,27	108.01),23	155.9,15	25,설파메라진 (Sulfamerazine),4.25,Positive,264.3,264.1,265.0,92.0,28	108.0,26	156.01),16	26,설파메타진 (Sulfamethazine),4.54,Positive,278.3,278.1,279.0,92.01),32	124.0,24	186.0,18	27,설파메톡사졸 (Sulfamethoxazole),5.25,Positive,253.2,253.1,254.0,92.01),28	108.0,23	155.9,15	28,설파메톡시피리다진 (Sulfamethoxypyridazine),4.56,Positive,280.3,280.1,281.0,92.0,30	108.0,27	156.01),17	29,설파모노메톡신 (Sulfamonomethoxine),4.85,Positive,280.3,280.1,281.0,92.0,28	108.0,27	156.01),17	30,설파퀴녹살린 (Sulfaquinoxaline),5.66,Positive,300.3,300.1,301.0,108.0,27	156.01),19	208.0,17	31,설파클로르피라진 (Sulfachlorpyrazine, Sulfaclozine),5.66,Positive,284.7,284.0,285.0,92.1,27	108.1,25	130.11),20	32,설파클로르피리다진 (Sulfachlorpyridazine),5.04,Positive,284.7,284.0,285.0,92.1,27	108.1,23	156.11),14	33,설파티아졸 (Sulfathiazole),3.94,Positive,255.3,255.0,256.0,92.0,27	108.0,24	156.01),14	34,설파페나졸 (Sulfaphenazole),5.77,Positive,314.4,314.1,315.1,92.1,34	131.1,28	158.11),22	35,설피속사졸 (Sulfisoxazole),5.39,Positive,267.3,267.1,268.0,92.0,27	113.0,16	155.91),15	36,세파드록실 (Cefadroxil),3.25,Positive,363.4,363.1,364.1,86.2,47	114.21),20	208.2,10	37,세팔렉신 (Cefalexin),3.84,Positive,347.4,347.1,348.0,106.1,30	158.01),13	174.0,15	38,세프티오퍼 (Ceftiofur),5.23,Positive,523.6,523.0,524.0,125.0,53	241.01),20	285.0,18	데스후로일 세프티오퍼 (Desfuroylceftiofur),4.35,Positive,429.5,429.0,430.0,126.01),29	227.0,24	241.1,16	39,스피라마이신 (Spiramycin),4.38,Positive,843.1,842.5,843.5,101.1,46	174.11),38	142.1,36	40,시프로플록사신 (Ciprofloxacin),3.95,Positive,331.3,331.1,332.1,231.2,36	245.2,24	314.21),20	41,아목시실린 (Amoxicillin),3.11,Positive,365.4,365.1,365.8,114.0,27	134.0,30	349.11),10	42,알벤다졸 (Albendazole),5.77,Positive,265.3,265.1,266.1,131.1,48	159.1,37	191.11),31	알벤다졸 설폭사이드 (Albendazole sulfoxide),4.29,Positive,281.3,281.1,282.0,159.1,40	208.11),23	240.1,13	알벤다졸 설폰 (Albendazole sulfone),5.07,Positive,297.3,297.1,297.6,159.1,37	224.1,26	266.11),20	2-아미노 알벤다졸 설폰 (2-Aminoalbendazole sulfone),3.74,Positive,239.3,239.1,240.0,105.1,51	133.1,18	198.11),28	43,암피실린 (Ampicillin),3.81,Positive,349.4,349.1,350.0,79.1,52	106.01),22	114.0,33	44,에리스로마이신 (Erythromycin),5.33,Positive,733.9,733.5,734.1,116.0,43	158.11),30	576.2,20	45,에토파베이트 (Ethopabate),5.59,Positive,237.2,237.1,238.0,136.11),28	164.1,19	206.1,11	m-페네티딘 (m-phenetidine),3.99,Positive,137.1,137.1,138.3,65.2,25	93.2,21	110.21),16	46,엔로플록사신 (Enrofloxacin),4.14,Positive,359.4,359.2,360.1,203.0,37	245.01),28	285.9,34	47,오르메토프림 (Ormethoprim),4.07,Positive,274.3,274.1,275.1,81.0,46	123.0,28	258.91),24	48,오비플록사신 (Orbifloxacin),4.24,Positive,395.4,395.1,396.0,253.91),31	295.0,25	352.1,19	49,오플록사신 (Ofloxacin),3.90,Positive,361.4,361.1,362.0,205.0,42	218.9,39	261.01),27	50,옥사실린 (Oxacillin),6.47,Positive,401.4,401.1,401.8,114.01),36	160.0,15	243.1,15	51,옥소린산 (Oxolinic acid),5.45,Positive,261.2,261.1,262.0,160.0,37	216.0,29	244.01),18	52,옥스펜다졸 (Oxfendazole),4.95,Positive,315.3,315.1,316.0,159.11),30	191.1,21	283.1,19	옥스펜다졸 설폰 (Oxfendazole sulfone),5.74,Positive,331.3,331.1,332.0,131.1,50	159.1,39	300.01),22	53,옥시벤다졸 (Oxibendazole),5.00,Positive,249.2,249.1,250.0,148.1,35	176.1,30	218.11),20	54,옥시테트라싸이클린 (Oxytetracycline),4.01,Positive,460.4,460.1,461.2,201.2,37	426.21),20	443.2,12	55,올레안도마이신 (Oleandomycin),5.16,Positive,687.9,687.4,688.4,116.1,45	158.11),28	544.3,18	56,조사마이신 (Josamycin),6.19,Positive,828.0,827.5,828.1,83.1,51	109.11),42	174.1,34	57,클로람페니콜 (Chloramphenicol),5.45,Negative,323.1,322.0,321.0,120.9,30	152.21),16	257.9,11	58,클로르테트라 싸이클린 (Chlortetracycline),4.74,Positive,478.9,478.1,479.1,98.0,43	154.01),30	443.9,22	59,클록사실린 (Cloxacillin),6.77,Positive,435.9,435.3,436.1,114.2,38	160.21),33	178.1,18	60,클린다마이신 (Clindamycin),4.73,Positive,425.0,424.2,424.9,82.8,55	126.11),29	377.1,21	61,키타사마이신 (Kitasamycin),5.76,Positive,828.0,771.4,772.4,83.2,50	109.11),45	174.1,35	62,타일로신 (Tylosin A),5.44,Positive,916.1,915.5,916.4,101.2,49	174.31),38	772.5,31	63,테트라미졸 (Tetramisole),3.76,Positive,204.2,204.1,205.1,91.2,27	123.2,37	178.21),20	64,테트라싸이클린 (Tetracycline),4.21,Positive,444.4,444.2,445.1,154.2,27	410.21),20	427.2,14	65,툴라스로마이신 (Tulathromycin),3.83,Positive,806.1,805.6,403.7,72.31),26	116.3,24	158.3,21	66,트리메토프림 (Trimethoprim),3.91,Positive,290.3,290.1,291.1,123.0,26	230.01),24	261.0,26	67,트리클라벤다졸 (Triclabendazole),7.58,Positive,359.7,358.0,359.0,171.1,53	274.0,37	346.01),26	케토 트리클라벤다졸 (Keto triclabendazole),7.19,Negative,329.6,328.0,327.0,118.0,40	146.1,33	182.21),25	68,트리클로르폰 (Trichlorfon, Metrifonate),4.70,Positive,257.4,255.9,256.9,79.1,30	109.21),20	223.0,10	69,티아물린 (Tiamulin),5.96,Positive,493.7,493.3,494.0,73.0,55	119.01),39	191.9,25	70,티아벤다졸 (Thiabendazole),3.72,Positive,201.2,201.0,201.9,65.1,45	131.1,35	175.01),25	5-하이드록시 티아벤다졸 (5-Hydroxy thiabendazole),3.38,Positive,217.2,217.0,217.9,81.1,45	147.0,35	191.01),25	71,티암페니콜 (Thiamphenicol),4.38,Negative,356.2,355.0,353.9,185.11),21	240.1,16	290.0,13	72,틸디피로신 (Tildipirosin),5.33,Positive,734.0,733.5,734.5,88.1,55	98.01),41	174.1,39	73,틸미코신 (Tilmicosin),4.79,Positive,869.1,868.6,869.7,88.2,60	174.31),55	696.5,45	74,페노뷰카브 (Fenobucarb),7.28,Positive,207.2,207.1,208.1,77.1,36	95.21),16	152.2,10	75,페니실린 V (Penicillin V),6.27,Negative,350.4,350.1,349.1,93.1,30	114.0,20	208.11),10	76,페반텔 (Febantel),7.41,Positive,446.5,446.1,447.0,281.2,32	384.21),20	416.2,14	77,페플록사신 (Pefloxacin),3.93,Positive,333.3,333.1,334.1,233.2,26	290.3,17	316.31),21	78,펜벤다졸 (Fenbendazole),6.49,Positive,299.3,299.1,300.0,104.1,55	131.1,48	268.11),21	79,푸마길린 (Fumagillin),7.43,Positive,458.5,458.2,459.2,103.2,50	131.11),28	177.1,17	80,프라지콴텔 (Praziquantel),6.97,Positive,312.4,312.2,313.1,83.1,28	174.0,25	203.11),17	81,플로르페니콜 (Florfenicol),5.29,Negative,358.2,357.0,355.9,151.8,19	185.1,16	336.01),10	플로르페니콜 아민 (Florfenicol amine),1.18,Positive,247.2,247.1,248.0,91.1,49	130.1,23	230.11),12	82,플루닉신 (Flunixin),7.19,Positive,296.2,296.1,297.1,109.1,48	236.1,42	264.11),32	5-하이드록시 플루닉신 (5-Hydroxy flunixin),6.78,Positive,312.2,312.2,312.9,279.91),34	295.0,23	266.9,13	83,플루메퀸 (Flumequin),6.31,Positive,261.2,261.1,262.0,126.0,50	202.0,33	244.01),18	84,플루벤다졸 (Flubendazole),6.02,Positive,313.2,313.1,314.0,95.1,50	123.1,35	282.11),24	2-아미노 플루벤다졸 (2-Amino flubendazole),4.78,Positive,255.2,255.1,256.0,75.1,55	95.11),39	133.1,37
연번,분석성분 (Compound),머무름 시간 (분),이온화 (Ionization mode),분자량 (MW),관측질량 (Exact Mass),선구이온 (Precusor ion, m/z),생성이온 (Product ion, m/z),충돌 에너지 (Collision Energy, eV)	1,난드롤론 (Nandrolone),6.80,Positive,274.4,274.2,275.1,109.11),26	257.2,16	239.2,17	2,날록손 (Naloxone),3.53,Positive,327.4,327.1,328.0,212.01),40	253.1,27	268.0,27	3,노보비오신 (Novobiocin),7.57,Positive,612.6,612.2,612.9,133.01),53	189.0,28	218.0,15	4,나이카바진 (Nicarbazin, N,N‘-bis-(4-nitrophenyl)urea),7.25,Negative,426.4,302.1,301.1,46.1,55	107.1,35	137.21),14	5,답손 (Dapsone),4.91,Positive,248.3,248.1,249.0,92.01),25	108.1,22	156.0,14	모노아세틸답손 (Monoacetyl dapsone),5.06,Positive,290.3,290.1,291.0,92.01),30	108.1,23	156.1,17	6,더콴텔 (Derquantel),5.42,Positive,479.6,479.3,480.0,148.3,42	405.3,31	462.21),26	7,디메트리다졸 (Dimetridazole),3.88,Positive,141.1,141.1,142.1,81.1,26	95.1,23	96.11),15	2-하이드록시메틸-1-메틸-5- 니트로이미다졸 (2-hydroxymethyl-1-methyl-5-nitroimidazole (HMMNI)),3.51,Positive,157.1,157.0,158.0,42.1,34	55.1,19	140.11),15	8,디미나진 (Diminazene),3.05,Positive,281.3,281.1,282.0,102.1,37	119.11),17	254.2,9	9,디에틸카바마진 (Diethylcarbamazine),3.34,Positive,199.2,199.2,200.1,72.01),24	100.1,16	127.0,15	10,디클라주릴 (Diclazuril),7.46,Negative,407.6,406.0,405.0,299.0,28	334.01),19	335.1,19	11,디펜하이드라민 (Diphenhydramine),5.48,Positive,255.3,255.2,256.1,115.0,55	152.0,35	167.11),13	12,락토파민 (Ractopamine),4.10,Positive,301.4,301.2,302.1,107.01),34	121.0,23	284.1,13	13,로니다졸 (Ronidazole),3.84,Positive,200.1,200.1,201.0,55.01),23	110.0,18	140.0,12	2-하이드록시메틸-1-메틸-5- 니트로이미다졸 (2-hydroxymethyl-1-methyl-5-nitroimidazole (HMMNI)),3.51,Positive,157.1,157.0,158.0,42.1,34	55.1,19	140.11),15	14,로베니딘 (Robenidine),6.50,Positive,334.2,333.1,333.9,111.0,50	138.0,25	155.11),20	15,로페라미드 (Loperamide),6.50,Positive,477.0,476.2,477.0,72.0,51	210.0,51	266.01),25	16,록사손 (Roxarsone),3.33,Negative,263.0,262.9,262.0,123.1,25	153.1,20	244.01),11	17,메토밀 (Methomyl),4.30,Positive,162.2,162.0,163.2,73.1,27	88.21),9	106.1,11	18,메토크로프라미드 (Metoclopramide),4.27,Positive,299.7,299.1,299.8,140.91),49	184.0,31	226.9,20	19,메트로니다졸 (Metronidazole),3.47,Positive,171.1,171.1,171.8,82.01),25	98.0,22	111.0,23	메트로니다졸-OH (Metronidazole-OH),3.14,Positive,187.1,187.1,188.0,68.1,22	123.11),13	126.0,17	20,모란텔 (Morantel),4.64,Positive,220.3,220.1,221.2,111.11),25	123.0,35	164.0,25	21,바시트라신 (Bacitracin),4.74,Positive,1422.7,1421.7,475.2,86.11),22	110.1,49	199.1,28	22,발네물린 (Valnemulin),6.11,Positive,564.8,564.4,565.0,147.01),39	164.0,32	263.1,19	23,버지니아마이신 (VirginiamycinM1),6.55,Positive,525.5,525.2,525.9,109.1,34	133.0,28	355.11),19	24,베르베린 (Berberine),5.32,Positive,336.4,336.1,336.0,263.01),53	278.0,43	304.0,33	25,석시닐-설파티아졸 (Succinyl-sulfathiazole),4.18,Positive,355.4,355.0,356.0,108.1,27	192.1,24	256.1),17	26,설파모졸 (Sulfamoxol),4.37,Positive,267.3,267.1,268.1,92.1,25	108.1,25	156.01),15	27,설파미터 (Sulfameter),4.62,Positive,280.3,280.1,281.1,92.1,30	108.1,25	156.11),19	28,설파벤자미드 (Sulfabenzamide),5.66,Positive,276.3,276.1,277.1,92.1,25	108.1,21	156.01),15	29,설파세타미드 (Sulfacetamide),3.65,Positive,214.2,214.0,215.1,92.1,23	108.1,21	156.01),11	30,설파피리딘 (Sulfapyridine),4.11,Positive,249.2,249.1,250.1,92.1,26	108.1,25	156.01),16	31,설피소미딘 (Sulfisomidine),3.56,Positive,278.3,278.1,279.1,92.1,30	124.11),20	186.1,20	32,설피린 (Sulpyrine, Dipyrone, Metamizole, 4-methylamino antipyrine),3.43,Positive,351.3,217.1,218.1,56.11),25	97.1,13	187.1,11	33,세파졸린 (Cefazolin),4.39,Positive,454.5,454.0,454.7,155.91),18	294.9,17	323.0,13	34,세포페라존 (Cefoperazone),4.78,Positive,645.7,645.1,645.8,143.01),36	148.0,52	530.0,12	35,스코폴라민 (Scopolamine),3.85,Positive,303.3,303.1,303.8,103.01),38	138.0,22	156.0,17	36,시프로헵타딘 (Cyproheptadine),5.86,Positive,287.4,287.2,288.2,96.11),25	191.1,30	215.1,48	37,아세트아닐라이드 (Acetanilide),4.92,Positive,135.1,135.1,135.9,43.0,31	51.0,50	77.01),30	38,아자페론 (Azaperone),4.35,Positive,327.4,327.2,328.2,95.1,64	121.1,19	123.11),44	아자페롤 (Azaperol),4.05,Positive,329.4,329.2,330.2,109.1,57	121.11),20	149.1,30	39,아크리플라빈 (Acriflavine, Euflavine),4.24,Positive,469.0,224.1,223.9,154.01),54	164.9,48	209.0,27	40,안티피린 (Antipyrine, Phenazone),4.58,Positive,188.2,188.1,188.9,56.01),34	58.5,34	104.0,25	41,알트레노제스트 (Altrenogest),7.40,Positive,310.4,310.2,311.0,227.11),24	269.1,15	293.4,18	42,에마멕틴 (Emamectin benzoate),7.38,Positive,1008.2,885.5,886.2,82.1,55	126.2,43	158.01),35	43,에프로토마이신 (Efrotomycin),7.10,Negative,1145.3,1144.6,1143.6,274.2,49	773.4,34	791.31),27	44,염산메틸에페드린 (DL-methylephedrine HCl),3.70,Positive,179.2,179.1,179.9,57.0,19	117.01),21	147.1,22	45,옥시클로자니드 (Oxyclozanide),7.60,Negative,401.4,400.9,399.9,202.1,22	363.91),17	381.9,22	46,올라퀸독스 (Olaquindox),4.63,Positive,263.2,188.1,189.0,102.0,32	143.0,16	145.01),16	47,요힘빈 (Yohimbine),4.69,Positive,354.4,354.2,355.1,117.01),52	144.0,31	212.1,24	48,이미도캅 (Imidocarb),3.26,Positive,348.4,348.2,349.0,145.1,55	162.2,25	188.11),29	49,이소메타미디움 (Isometamidium),4.45,Positive,460.6,460.2,460.2,269.1,50	298.11),25	313.1,20	50,이프로니다졸 (Ipronidazole),5.59,Positive,169.1,169.1,170.1,109.11),26	123.1,25	124.1,19	이프로니다졸-OH (Ipronidazole-OH),4.71,Positive,185.1,185.1,186.1,121.1,29	122.2,20	168.21),15	51,질파테롤 (Zilpaterol),3.12,Positive,261.3,261.1,262.2,185.11),25	202.1,19	244.2,14	52,카라졸롤 (Carazolol),4.91,Positive,298.4,298.2,299.2,116.11),21	194.1,30	222.1,20	53,카바독스 (Carbadox),4.42,Positive,262.2,174.0,174.8,102.01),32	129.0,18	131.0,16	54,카벤다짐 (Carbendazim),3.67,Positive,191.1,191.1,192.0,105.1,35	132.2,29	160.11),18	55,케토프로펜 (Ketoprofen),6.99,Positive,254.2,254.1,255.1,77.1,45	105.0,22	209.11),15	56,쿠마포스 (Coumaphos),7.71,Positive,362.8,362.0,363.0,227.01),25	307.0,18	335.0,17	쿠마포스 옥손 (Coumaphos oxon),7.08,Positive,346.7,346.0,347.0,291.01),24	221.0,33	57,콜치신 (Colchicine),5.29,Positive,399.4,399.2,400.1,310.2,27	326.2,24	358.21),23	58,클렌부테롤 (Clenbuterol),4.53,Positive,277.1,276.1,277.0,140.01),46	168.0,31	203.0,17	59,클로르프로마진 (Chlorpromazine),6.18,Positive,318.9,318.1,319.1,58.1,30	86.11),20	246.0,24	60,클로산텔 (Closantel),8.55,Negative,663.1,661.9,660.8,127.01),50	315.1,34	345.0,36	61,클로술론 (Clorsulon),5.60,Negative,380.7,378.9,378.0,277.1,22	242.2,22	342.11),12	62,클로피돌 (Clopidol),3.73,Positive,192.0,191.0,192.0,51.1,44	87.1,30	101.11),26	63,테트라메트린 (Tetramethrin),8.02,Positive,331.4,331.2,332.0,135.1,17	164.11),24	314.2,10	64,테트라크로르빈포스 (Tetrachlorvinphos),7.57,Positive,366.0,365.9,367.0,127.11),21	205.9,37	65,톨트라주릴 설폰 (Toltrazuril sulfone),7.31,Negative,457.4,457.1,456.0,42.21),22	399.1,12	66,트리페레나민 (Tripelennamine),4.83,Positive,255.3,255.2,256.1,72.11),32	91.0,36	119.0,34	67,티니다졸 (Tinidazole),4.40,Positive,247.2,247.1,248.0,82.1,34	121.11),16	128.0,21	68,펄리마이신 (Pirlimycin),4.62,Positive,411.0,410.2,411.1,56.1,52	112.11),30	363.1,19	69,페나세틴 (Phenacetin),5.54,Positive,179.2,179.1,179.9,65.11),37	93.0,28	110.0,22	70,프로폭서 (Propoxur),6.53,Positive,209.2,209.1,210.1,93.0,24	111.01),15	168.1,9	71,플루아주론 (Fluazuron),7.85,Positive,506.2,505.0,506.0,158.01),20	141.0,48	349.0,19	72,피리메타민 (Pyrimethamine),4.95,Positive,248.7,248.1,249.1,177.0,30	198.1,45	233.11),28	73,할로푸지논 (Halofuginone),4.90,Positive,414.7,413.0,414.0,100.1,24	120.11),21	138.1,20

분석성분 (Compound)	머무름	분자량 (MW)	관측질량 (Exact mass)	선구이온 (Precursor ion, m/z)	생성이온 ion, m/z)	충돌에너지 (Collision energy, eV)
겐타마이신 C1 (Gentamicin C1)	6.77	477.6	477.3	478.3	157.1	20
160.0	22
322.21)	14
겐타마이신 C1a (Gentamicin C1a)	6.59	449.5	449.3	450.3	112.0	26
160.0	22
322.21)	12
겐타마이신 C2 (Gentamicin C2)	6.65	463.6	463.3	464.3	112.0	42
160.0	20
322.21)	10
겐타마이신 C2a (Gentamicin C2a)	6.79	463.6	463.3	464.3	112.0	34
160.0	20
322.21)	12
네오마이신 (Neomycin)	6.93	614.6	614.3	615.2	160.61)	32
163.5	32
293.1	20
디히드로 스트렙토마이신 (Dihydrostreptomycin)	4.10	583.6	583.3	584.2	221.1	36
246.1	34
263.11)	28
스트렙토마이신 (Streptomycin)	4.02	581.6	581.3	582.3	221.1	38
246.1	36
263.11)	30
스펙티노마이신 (Spectinomycin)	2.97	332.3	332.2	350.9	189.1	25
207.1	16
333.21)	22
아미카신 (Amikacin)	4.95	585.6	585.3	586.4	163.11)	34
264.2	24
425.2	12
아프라마이신 (Apramycin)	6.14	539.6	539.3	540.3	217.11)	26
344.1	18
378.2	16
카나마이신 (Kanamycin)	5.19	484.5	484.2	485.2	163.01)	26
205.1	32
324.1	14
파로모마이신 (Paromomycin)	6.93	615.6	615.3	616.3	163.11)	36
293.1	22
324.2	20
하이그로마이신 B (Hygromycin B)	3.78	527.5	527.2	528.2	117.11)	28
257.0	28
352.1	12
토브라마이신(내부표준물질) (Tobramycin, IS)	6.32	467.5	467.3	468.2	163.01)	24

분석성분 (Compound)	머무름 시간 (분)	분자량 (MW)	관측질량 (Exact mass)	선구이온 (Precursor ion, m/z)	생성이온 (Product ion, m/z)	충돌에너지 (Collision energy, eV)
나라신 (Narasin)	14.11	765.0	764.5	787.5	431.31)	60
531.3	50
413.1	60
라살로시드 (Lasalocid A-Na)	11.71	612.8	612.4	613.2	377.11)	40
577.1	30
595.3	30
마두라마이신 (Maduramycin)	15.02	934.2	916.5	939.4	877.41)	30
895.2	50
859.0	50
모넨신 (Monensin-Na)	13.15	692.9	692.4	693.3	461.21)	60
479.2	60
501.2	60
살리노마이신 (Salinomycin-Na)	12.92	791.0	772.5	773.3	431.21)	60
531.2	50
265.2	60
샘두라마이신 (Semduramicin)	10.75	873.1	872.5	895.3	833.41)	30
851.2	30
815.1	30

연번	분석성분 (Compound)	머무름 시간 (분)	이온화 (Ionization mode)	분자량 (MW)	관측질량 (Exact mass)	선구이온 (Precursor ion, m/z)	생성이온 (Product ion, m/z)	충돌에너지 (Collision energy, eV)
1	데코퀴네이트 (Decoquinate)	9.02	Positive	417.5	417.3	418.2	372.11)	33.0
203.9	55.0
231.9	47.0
2	디사이클라닐 (Dicyclanil)	2.10	Positive	190.2	190.1	191.0	150.01)	27.0
149.8	29.0
163.1	23.0
3	암프롤리움 (Amprolium)	0.88	Positive	278.7	278.1	243.1	150.01)	17.0
93.8	19.0
122.0	31.0
4	죠렌 (Zoalene)	4.98	Negative	225.1	225.0	223.9	181.01)	14.0
42.0	36.0
151.0	22.0
*3-Amino-5-nitro-toluamide(ANOT)	3.46	Positive	195.1	195.1	196.0	107.01)	23.0
153.1	23.0
179.0	11.0