분석조건
LC기울기 용리8.2.2.1.1FD-축산물-중-항균제-등-동물용의약품-동시-다성분-시험법-x1원문 표제 단서: 액체크로마토그래프
- 칼럼
- C18 · USP L1
C18계 컬럼
안지름 2.1 mm · 길이 15 cm · 입자경 3.5 μm
- 칼럼온도
- 40℃
- 이동상
- 0.1%(v/v) 포름산(formic acid) 함유한 수용액
- 0.1%(v/v) 포름산(formic acid) 함유한 아세토니트릴
- 유량
- 0.2 mL/분
- 주입량
- 5 μL
- 기타표
구분,검출한계 계열,분석성분(Compound),소,돼지,가금,알(卵),유(乳) 구충제,카벤다짐,0.0009,0.001,0.0006,0.0009,0.0003 테트라미졸,0.0006,0.0003,0.0006,0.0003,0.0006 프라지콴텔,0.0003,0.0003,0.0003,0.0003,0.0006 니트로이미다졸계,로니다졸,0.002,0.002,0.002,0.0006,0.0006 메트로니다졸,0.002,0.002,0.0009,0.003,0.0003 메트로니다졸-OH,0.003,0.0003,0.0003,0.0006,0.001 디아미노피리미딘계,오르메토프림,0.009,0.006,0.02,0.006,0.0003 트리메토프림,0.009,0.009,0.006,0.0003,0.003 린코사마이드계,린코마이신,0.009,0.03,0.02,0.002,0.02 마크로라이드계,록시스로마이신,0.001,0.0006,0.0006,0.0002,0.0006 스피라마이신,0.003,0.006,0.003,0.002,0.02 에리스로마이신,0.006,0.006,0.02,0.002,0.002 올레안도마이신,0.02,0.0009,0.002,0.003,0.003 조사마이신,0.003,0.003,0.003,0.002,0.002 타일로신 A,0.03,0.02,0.02,0.06,0.006 툴라스로마이신,0.02,0.006,0.006,0.003,0.003 틸미코신,0.006,0.002,0.002,0.003,0.0006 살충제,메토밀,0.003,0.003,0.002,0.003,0.003 에마멕틴B1a,0.0002,0.002,0.0002,0.0003,0.0009 테트라메트린,0.001,0.0006,0.002,-,0.0006 페노뷰카브,0.002,0.002,0.002,0.0006,0.002 설파제,설파구아니딘,0.01,0.02,0.01,0.006,0.003 설파독신,0.003,0.01,0.02,0.006,0.02 설파디메톡신,0.01,0.006,0.02,0.003,0.02 설파디아진,0.01,0.006,0.006,0.003,0.009 설파메라진,0.02,0.006,0.015,0.006,0.009 설파메타진,0.003,0.006,0.003,0.003,0.006 설파메톡사졸,0.006,0.003,0.009,0.006,0.03 설파메톡시피리다진,0.006,0.009,0.01,0.006,0.003 설파모노메톡신,0.006,0.006,0.002,0.002,0.01 설파퀴녹살린,0.009,0.02,0.015,0.009,0.0006 설파클로르피리다진,0.003,0.006,0.006,0.003,0.003 설파클로진,0.006,0.003,0.003,0.003,0.003 설파티아졸,0.003,0.006,0.002,0.002,0.003 설파페나졸,0.001,0.006,0.003,0.001,0.0006 설피속사졸,0.003,0.006,0.01,0.006,0.003 성장보조제,난드롤론,0.0003,0.0003,0.0006,0.0002,0.0003 락토파민,0.002,0.002,0.009,0.006,0.006 알트레노제스트,0.0003,0.00003,0.0003,0.0006,0.003 클렌부테롤,0.00003,0.00006,0.00003,0.00003,0.00003 세팔로스포린계,세파졸린,0.009,0.006,0.003,0.0006,0.003 세파피린,0.006,0.003,0.001,0.001,0.003 데스아세틸 세파피린,0.009,0.006,0.003,0.003,0.0003 세팔렉신,0.02,0.03,0.003,0.003,0.002 세팔로니움,0.002,0.009,0.009,0.02,0.003 세포페라존,0.02,0.003,0.009,0.02,0.003 세프퀴놈,0.01,0.006,0.006,0.009,0.006 세프티오퍼,0.09,0.12,0.003,0.001,0.006 데스후로일세프티오퍼,0.06,0.2,0.003,0.009,0.02 소독제,아크리플라빈,0.0009,0.002,0.003,0.0009,0.0006 암페니콜계,클로람페니콜,0.00003,0.0001,0.0001,0.00009,0.0002 티암페니콜,0.002,0.002,0.003,0.003,0.003 플로르페니콜,0.03,0.02,0.009,0.002,0.003 플로프페니콜아민,0.03,0.06,0.02,0.002,0.003 지사제,로페라미드,0.0009,0.002,0.003,0.0009,0.0006 베르베린,0.0006,0.0009,0.0006,0.0003,0.0009 진정제,스코폴라민,0.0006,0.0009,0.0006,0.0003,0.0003 페노티아진,0.003,-,0.003,0.0006,0.002 진해거담제,DL-메틸에페드린,0.001,0.0003,0.0009,0.0006,0.002 퀴녹살린계,올라퀸독스,0.0006,0.0003,0.0003,0.0003,0.0003 카바독스,0.001,0.0009,0.0006,0.0003,0.006 퀴놀론계,날리딕스산,0.002,0.0006,0.001,0.002,0.001 노르플록사신,0.00006,0.0001,0.00006,0.00006,0.0001 다노플록사신,0.03,0.02,0.02,0.006,0.003 디플록사신,0.1,0.09,0.06,0.0009,0.006 마보플록사신,0.003,0.02,0.001,0.0009,0.009 사라플록사신,0.002,0.002,0.0006,0.001,0.002 시프로플록사신,0.03,0.02,0.01,0.00003,0.009 엔로플록사신,0.02,0.003,0.006,0.0002,0.009 오비플록사신,0.003,0.0003,0.002,0.002,0.003 오플록사신,0.00003,0.00003,0.00003,0.0002,0.00003 옥소린산,0.003,0.002,0.003,0.003,0.003 페플록사신,0.00003,0.00003,0.00003,0.00009,0.00006 플루메퀸,0.006,0.02,0.009,0.001,0.003 테트라싸이클린계,독시싸이클린,0.002,0.003,0.006,0.0006,0.0009 옥시테트라싸이클린,0.03,0.03,0.03,0.006,0.009 클로르테트라싸이클린,0.02,0.01,0.01,0.009,0.006 테트라싸이클린,0.01,0.03,0.01,0.01,0.003 페니실린계,나프실린,0.003,0.003,0.003,0.006,0.006 디클록사실린,0.009,0.02,0.02,0.002,0.003 벤질페니실린,0.02,0.006,0.002,0.00006,0.0003 아목시실린,0.009,0.003,0.002,0.001,0.0003 암피실린,0.003,0.003,0.002,0.0003,0.0003 옥사실린,0.0006,0.002,0.0006,0.0003,0.0003 클록사실린,0.009,0.01,0.01,0.003,0.003 폴리펩타이드계,버지니아마이신,0.002,0.003,0.006,0.003,0.01 항균제 기타,노보비오신,0.0303,0.002,0.02,0.003,0.001 답손,0.0003,0.0006,0.0006,0.0003,0.0009 모노아세틸 답손,0.0003,0.0003,0.0006,0.0006,0.0006 리팍시민,0.00009,0.002,0.002,0.002,0.01 발네물린,0.002,0.001,0.001,0.001,0.003 티아물린,0.0006,0.0009,0.002,0.003,0.002 틸디피로신,0.03,0.003,0.003,0.0006,0.0009 항염증제,아미노피린,0.003,0.003,0.003,0.001,0.002 아세트아닐라이드,0.0006,0.0009,0.001,0.0009,0.001 안티피린,0.002,0.0003,0.0006,0.0003,0.0009 페나세틴,0.0003,0.0003,0.0003,0.0003,0.0003 항히스타민제,디펜하이드라민,0.0009,0.0006,0.002,0.0009,0.0003 시프로헵타딘,0.0006,0.0003,0.0003,0.0006,0.0003 트리페레나민,0.0006,0.00009,0.0003,0.0001,0.0003 호흡촉진제,날록손,0.0009,0.0006,0.0006,0.0006,0.0006 기타 동물용 의약품,디에틸카바마진,0.0009,0.0006,0.001,0.0006,0.0006 메토크로프라미드,0.002,0.002,0.006,0.001,0.0006 요힘빈,0.002,0.0006,0.0003,0.0003,0.0003 구분,정량한계 계열,분석성분(Compound),소,돼지,가금,알(卵),유(乳) 구충제,카벤다짐,0.003,-,0.002,0.003,0.001 테트라미졸,-,-,0.002,0.001,0.002 프라지콴텔,0.001,0.001,0.001,0.001,0.002 니트로이미다졸계,로니다졸,-,-,-,-,- 메트로니다졸,-,-,-,-,- 메트로니다졸-OH,-,-,-,-,- 디아미노피리미딘계,오르메토프림,-,-,-,-,0.001 트리메토프림,0.03,0.03,0.02,0.001,0.01 린코사마이드계,린코마이신,0.03,-,0.06,0.005,- 마크로라이드계,록시스로마이신,0.003,0.002,0.002,0.0006,0.002 스피라마이신,-,-,-,-,0.05 에리스로마이신,-,0.02,0.05,0.004,- 올레안도마이신,-,0.003,0.006,0.009,0.009 조사마이신,-,-,-,-,0.006 타일로신 A,-,-,-,-,- 툴라스로마이신,-,-,-,-,0.01 틸미코신,0.02,0.005,0.006,0.01,0.002 살충제,메토밀,-,-,-,-,0.01 에마멕틴B1a,-,-,0.0005,0.001,- 테트라메트린,-,-,-,-,- 페노뷰카브,-,-,-,-,- 설파제,설파구아니딘,-,-,-,-,- 설파독신,-,0.04,0.05,0.02,- 설파디메톡신,-,0.02,0.06,0.01,- 설파디아진,-,-,-,-,- 설파메라진,-,0.02,0.05,0.02,- 설파메타진,0.01,0.02,0.01,0.01,0.02 설파메톡사졸,-,0.01,0.03,0.02,- 설파메톡시피리다진,0.02,-,0.04,0.02,- 설파모노메톡신,0.02,-,-,0.006,- 설파퀴녹살린,-,-,0.05,0.03,- 설파클로르피리다진,-,-,0.02,-,- 설파클로진,-,-,-,-,- 설파티아졸,-,-,-,-,- 설파페나졸,-,0.02,0.01,0.003,- 설피속사졸,-,0.02,-,0.02,- 성장보조제,난드롤론,0.001,0.001,0.002,0.0005,0.001 락토파민,-,0.007,-,-,- 알트레노제스트,0.001,0.0001,0.001,0.002,- 클렌부테롤,-,0.0002,0.0001,0.0001,0.0001 세팔로스포린계,세파졸린,-,0.02,0.01,0.002,0.01 세파피린,-,-,-,-,- 데스아세틸 세파피린,-,-,-,-,- 세팔렉신,-,-,-,-,- 세팔로니움,0.006,0.03,-,-,0.008 세포페라존,-,0.01,-,-,0.02 세프퀴놈,-,0.02,-,-,- 세프티오퍼,-,-,0.01,0.004,- 데스후로일세프티오퍼,-,-,-,-,- 소독제,아크리플라빈,0.003,-,-,0.003,0.002 암페니콜계,클로람페니콜,-,-,-,-,0.0005 티암페니콜,-,-,-,-,- 플로르페니콜,-,-,-,-,- 플로프페니콜아민,-,-,-,-,- 지사제,로페라미드,0.002,0.006,0.002,0.002,0.003 베르베린,0.002,-,-,-,- 진정제,스코폴라민,0.002,-,0.002,0.001,0.001 페노티아진,-,-,-,-,- 진해거담제,DL-메틸에페드린,0.004,-,-,-,- 퀴녹살린계,올라퀸독스,0.002,0.001,0.001,0.001,0.001 카바독스,0.004,-,-,-,- 퀴놀론계,날리딕스산,0.006,0.002,0.004,0.006,- 노르플록사신,0.0002,0.0004,-,-,0.0004 다노플록사신,-,-,0.05,-,0.01 디플록사신,0.3,-,0.2,0.003,- 마보플록사신,0.009,-,-,-,0.03 사라플록사신,0.006,0.006,0.002,0.004,0.007 시프로플록사신,-,-,-,-,- 엔로플록사신,-,0.008,0.02,0.0005,- 오비플록사신,0.01,0.001,0.007,0.005,- 오플록사신,0.0001,0.0001,0.0001,-,0.0001 옥소린산,0.01,-,-,0.01,0.01 페플록사신,0.0001,0.0001,0.0001,0.0003,- 플루메퀸,0.02,-,-,0.004,0.01 테트라싸이클린계,독시싸이클린,-,0.009,-,-,- 옥시테트라싸이클린,-,-,-,-,- 클로르테트라싸이클린,-,-,-,-,- 테트라싸이클린,-,-,-,-,- 페니실린계,나프실린,-,-,-,-,- 디클록사실린,-,-,-,-,- 벤질페니실린,-,-,-,-,0.001 아목시실린,-,-,-,-,- 암피실린,-,-,-,-,0.001 옥사실린,-,-,-,0.001,- 클록사실린,-,-,-,-,- 폴리펩타이드계,버지니아마이신,-,-,-,-,0.04 항균제 기타,노보비오신,-,-,-,-,- 답손,-,-,-,-,- 모노아세틸 답손,-,-,-,-,0.002 리팍시민,-,0.005,-,-,- 발네물린,-,-,0.004,0.004,0.01 티아물린,0.002,0.003,-,-,0.008 틸디피로신,0.08,-,-,-,- 항염증제,아미노피린,-,-,-,-,- 아세트아닐라이드,0.002,-,-,-,- 안티피린,0.005,0.001,0.002,0.001,0.003 페나세틴,-,0.001,0.001,0.001,0.001 항히스타민제,디펜하이드라민,0.003,0.002,0.005,0.003,0.001 시프로헵타딘,-,-,-,-,- 트리페레나민,0.002,-,-,-,0.001 호흡촉진제,날록손,0.003,-,0.002,0.002,- 기타 동물용의약품,디에틸카바마진,-,-,-,-,0.002 메토클로프라미드,0.005,0.007,-,0.004,0.002 요힘빈,-,0.002,0.001,-,0.001
질량분석(MS) 조건 보기 (5항목)
- 이온화 방법
- 가) 이온화 방법: ESI(Positive ion mode, Negative ion mode)
- Capillary temperature
- 나) Capillary temperature: 350℃
- Capillary voltage
- 다) Capillary voltage: 3.4 kV
- Collision gas
- 라) Collision gas: 아르곤(Ar) 또는 이와 동등한 것
- 전이표
연번 분석성분 (Compound) 머무름 시간 (분) 이온화 (Ionization mode) 분자량 (MW) 관측질량 (Exact Mass) 선구이온 (Precursor ion, m/z) 생성이온 (Product ion, m/z) 충돌에너지 (Collision energy, eV) 1 나프실린 (Nafcillin) 9.4 Positive 414.4 414.1 437.2 261.11) 14 278.1 16 319.1 14 2 난드롤론 (Nandrolone) 9.4 Positive 274.4 274.2 275.0 81.0 26 109.01) 26 239.0 14 3 날록손 (Naloxone) 3.7 Positive 327.3 327.1 328.1 212.01) 36 253.1 24 268.3 24 4 날리딕스산 (Nalidixic acid) 8.5 Positive 232.2 232.1 233.0 104.0 38 131.0 32 159.01) 30 5 노르플록사신 (Norfloxacin) 4.7 Positive 319.3 319.1 320.1 204.8 32 233.01) 22 256.1 20 6 노보비오신 (Novobiocin) 10.5 Positive 612.6 612.2 613.3 133.0 62 189.11) 28 218.1 12 7 다노플록사신 (Danofloxacin) 5.0 Positive 357.3 357.1 358.0 95.9 27 314.2 19 340.11) 26 8 답손 (Dapsone) 6.1 Positive 248.3 248.1 248.7 92.0 24 107.9 22 155.91) 14 모노아세틸 답손 (Monoacetyl dapson) 6.7 Positive 290.3 290.1 290.9 92.3 24 108.0 20 156.01) 12 9 독시싸이클린 (Doxycycline) 6.5 Positive 444.4 444.2 445.1 267.0 34 321.11) 29 428.2 16 10 디에틸카바마진 (Diethylcarbamazine) 3.1 Positive 199.2 199.2 200.1 72.0 20 100.0 14 127.01) 12 11 디클록사실린 (Dicloxacillin) 9.6 Positive 470.3 469.0 470.1 114.4 36 160.01) 11 310.8 14 12 디펜하이드라민 (Diphenhydramine) 7.8 Positive 255.3 255.2 256.1 115.0 50 152.0 32 167.11) 10 13 디플록사신 (Difloxacin) 5.8 Positive 399.3 399.1 400.0 279.0 38 285.0 30 299.11) 26 14 락토파민 (Ractopamine) 5.1 Positive 301.3 301.2 302.1 107.0 28 121.01) 20 284.1 14 15 로니다졸 (Ronidazole) 4.2 Positive 200.1 200.1 201.1 55.0 18 110.0 14 140.01) 8 16 로페라미드 (Loperamide) 9.1 Positive 477.0 476.2 477.0 115.0 33 210.0 71 266.01) 45 17 록시스로마이신 (Roxithromycin) 8.7 Positive 837.0 836.5 837.4 116.0 46 158.11) 34 679.4 20 18 리팍시민 (Rifaximin) 9.9 Positive 785.8 785.4 786.3 95.0 50 151.0 34 754.21) 20 19 린코마이신 (Lincomycin) 4.2 Positive 406.5 406.2 407.2 82.3 64 126.0 28 359.21) 18 20 마보플록사신 (Marbofloxacin) 4.6 Positive 362.3 362.1 363.2 72.0 19 320.11) 15 345.0 22 21 메토밀 (Methomyl) 5.0 Positive 162.2 162.0 163.0 65.0 4 88.01) 6 106.0 8 22 메토크로프라미드 (Metoclopramide) 5.4 Positive 299.8 299.1 300.1 140.9 44 183.91) 26 227.1 16 23 메트로니다졸 (Metronidazole) 3.4 Positive 171.1 171.1 172.0 82.01) 22 98.2 16 111.0 20 메트로니다졸-OH (Metronidazole-OH) 5.7 Positive 187.1 187.1 188.2 68.0 22 80.0 28 123.11) 8 24 DL-메틸에페드린 (DL-methylephedrine) 4.2 Positive 179.2 179.1 180.1 57.0 16 117.11) 18 146.9 18 25 발네물린 (Valnemulin) 8.7 Positive 564.8 564.4 565.4 147.0 36 164.0 28 263.21) 16 26 버지니아마이신 (Virginiamycin M1) 9.0 Positive 525.5 525.2 526.2 109.0 32 133.0 24 355.01) 16 27 베르베린 (Berberine) 7.4 Positive 336.3 336.1 336.0 262.8 46 278.01) 40 303.7 28 28 벤질페니실린 (Benzylpenicillin) 8.3 Positive 334.3 334.1 335.0 91.0 38 128.01) 22 159.9 20 29 사라플록사신 (Sarafloxacin) 5.7 Positive 385.3 385.1 386.2 299.11) 24 322.1 22 348.1 32 30 설파구아니딘 (Sulfaguanidine) 2.2 Positive 214.2 214.1 215.1 60.0 10 92.0 20 156.01) 12 31 설파독신 (Sulfadoxine) 6.7 Positive 310.3 310.1 311.0 92.0 28 108.1 24 156.01) 16 32 설파디메톡신 (Sulfadimethoxine) 7.7 Positive 310.3 310.1 311.1 92.1 28 108.11) 26 156.1 18 33 설파디아진 (Sulfadiazine) 4.2 Positive 250.2 250.1 251.0 92.1 26 108.1 22 156.01) 14 34 설파메라진 (Sulfamerazine) 4.9 Positive 264.3 264.1 265.3 92.1 24 108.0 22 156.01) 16 35 설파메타진 (Sulfamethazine) 5.5 Positive 278.3 278.1 279.1 92.1 28 124.1 22 186.11) 16 36 설파메톡사졸 (Sulfamethoxazole) 6.8 Positive 253.2 253.1 254.0 92.1 26 108.0 20 156.01) 14 37 설파메톡시피리다진 (Sulfamethoxy pyridazine) 6.1 Positive 280.3 280.1 281.0 92.0 30 108.0 24 156.01) 14 38 설파모노메톡신 (Sulfamonomethoxine) 5.6 Positive 280.3 280.1 281.0 92.0 28 108.0 24 156.01) 16 39 설파퀴녹살린 (Sulfaquinoxaline) 7.7 Positive 300.3 300.1 300.9 108.0 25 155.91) 15 207.7 18 40 설파클로르피리다진 (Sulfachlorpyridazine) 7.6 Positive 284.7 284.0 285.0 92.0 24 108.0 22 156.01) 14 41 설파클로진 (Sulfaclozine, Sulfachlorpyrazine) 6.4 Positive 284.7 284.0 285.0 92.0 26 108.0 24 155.91) 16 42 설파티아졸 (Sulfathiazole) 4.4 Positive 255.3 255.0 256.0 92.1 24 108.1 22 156.01) 14 43 설파페나졸 (Sulfaphenazole) 7.8 Positive 314.3 314.1 315.1 92.0 34 158.21) 28 158.8 22 44 설피속사졸 (Sulfisoxazole) 7.0 Positive 267.3 267.1 268.1 92.0 30 113.0 16 156.01) 14 45 세파졸린 (Cefazolin) 5.4 Positive 454.5 454.0 455.0 156.01) 12 295.0 14 323.0 8 46 세파피린 (Cephapirin) 3.4 Positive 423.4 423.1 424.1 152.0 22 181.0 23 292.01) 13 데스아세틸 세파피린 (Desacetyl cephapirin) 2.2 Positive 381.4 381.1 382.1 111.8 22 124.1 40 152.01) 24 47 세팔렉신 (Cephalexin) 4.7 Positive 347.3 347.1 348.0 106.0 26 158.01) 6 174.0 14 48 세팔로니움 (Cefalonium) 4.7 Positive 458.5 458.1 459.1 152.0 16 158.0 14 337.01) 6 49 세포페라존 (Cefoperazone) 6.2 Positive 645.6 645.1 646.1 143.01) 28 148.0 44 530.1 8 50 세프퀴놈 (Cefquinome) 1.8 Positive 528.6 528.1 529.1 134.01) 12 166.9 22 396.0 10 51 세프티오퍼 (Ceftiofur) 7.1 Positive 523.5 523.1 524.1 95.0 42 125.21) 58 241.0 16 데스후로일 세프티오퍼 (Desfuroylceftiofur) 5.4 Positive 429.5 429.1 430.1 125.9 32 227.01) 22 241.1 14 52 스코폴라민 (Scopolamine) 4.4 Positive 303.3 303.1 304.1 103.0 38 138.11) 18 156.1 14 53 스피라마이신 (Spiramycin) 6.0 Positive 843.0 842.5 843.4 101.0 42 142.0 34 174.11) 34 54 시프로플록사신 (Ciprofloxacin) 4.9 Positive 331.3 331.1 332.0 203.1 36 231.0 34 245.01) 24 55 시프로헵타딘 (Cyproheptadine) 8.5 Positive 287.4 287.2 288.0 58.0 20 70.0 22 96.01) 22 56 아목시실린 (Amoxicillin) 2.6 Positive 365.4 365.1 366.1 113.91) 19 134.0 31 349.1 5 57 아미노피린 (Aminopyrine) 3.6 Positive 231.2 231.1 232.0 98.0 16 113.01) 12 113.0 14 58 아세트아닐라이드 (Acetanilide) 6.1 Positive 135.1 135.1 136.0 43.0 16 51.0 74 77.01) 22 59 아크리플라빈 (Acriflavine) 5.3 Positive 259.7 224.1 224.1 154.1 46 164.9 40 209.01) 26 60 안티피린 (Antipyrine) 5.6 Positive 188.2 188.1 189.0 55.6 22 58.5 22 104.11) 20 61 알트레노제스트 (Altrenogest) 10.3 Positive 310.4 310.2 311.0 159.0 24 227.01) 22 251.0 12 62 암피실린 (Ampicillin) 4.6 Positive 349.4 349.1 350.1 79.0 44 106.01) 17 114.0 30 63 에리스로마이신 (Erythromycin) 7.7 Positive 733.9 733.5 734.2 116.1 46 158.11) 30 576.3 18 64 에마멕틴 B1a (Emamectin B1a) 10.1 Positive 886.1 885.5 886.0 82.0 72 126.0 44 158.01) 34 65 엔로플록사신 (Enrofloxacin) 5.2 Positive 359.4 359.2 360.1 203.2 36 245.11) 24 286.0 32 66 오르메토프림 (Ormetoprim) 5.1 Positive 274.3 274.1 274.9 80.9 43 122.91) 25 258.9 27 67 오비플록사신 (Orbifloxacin) 5.4 Positive 395.3 395.1 396.1 254.1 28 295.0 22 352.11) 16 68 오플록사신 (Ofloxacin) 4.8 Positive 361.3 361.1 362.0 205.0 38 218.4 36 261.11) 26 69 옥사실린 (Oxacillin) 8.9 Positive 401.4 401.1 402.2 114.1 36 159.91) 13 243.0 12 70 옥소린산 (Oxolinic acid) 8.6 Positive 261.2 261.1 262.0 160.1 35 216.1 28 244.11) 17 71 옥시테트라싸이클린 (Oxytetracycline) 4.9 Positive 460.4 460.1 461.1 201.0 40 337.0 28 426.11) 18 72 올라퀸독스 (Olaquindox: 3-methyl quinoxaline-2-carboxylic acid, MQCA) 5.7 Positive 263.2 188.1 189.2 102.1 27 143.0 15 145.01) 12 73 올레안도마이신 (Oleandomycin) 7.4 Positive 687.8 687.4 688.5 116.1 40 158.11) 24 544.3 14 74 요힘빈 (Yohimbine) 6.2 Positive 354.4 354.2 355.2 117.0 44 144.01) 30 212.1 20 75 조사마이신 (Josamycin) 8.9 Positive 828.0 827.5 828.3 83.0 46 109.0 44 174.11) 30 76 카바독스 (Carbadox: Quinoxaline-2-carboxylic acid, QCA) 5.3 Positive 262.2 174.0 175.1 102.1 29 129.11) 16 131.1 13 77 카벤다짐 (Carbendazim) 4.1 Positive 191.1 191.1 192.0 105.0 32 132.0 30 160.01) 14 78 클렌부테롤 (Clenbuterol) 5.9 Positive 277.1 276.1 277.1 140.1 44 167.9 28 203.11) 16 79 클로람페니콜 (Chloramphenicol) 7.3 Negative 323.1 322.0 321.1 175.9 14 194.0 10 257.01) 10 80 클로르테트라싸이클린 (Chlortetracycline) 6.4 Positive 478.8 478.1 479.1 98.0 36 154.01) 24 444.0 18 81 클록사실린 (Cloxacillin) 9.2 Positive 435.8 435.3 436.1 114.1 38 160.01) 11 277.0 11 82 타일로신 A (Tylosin A) 7.9 Positive 916.1 915.5 916.4 88.0 74 101.0 44 174.11) 40 83 테트라메트린 (Tetramethrin) 12.0 Positive 331.4 331.4 332.0 107.0 40 135.01) 14 164.0 20 84 테트라미졸 (Tetramisole) 4.5 Positive 204.2 204.1 205.0 91.0 30 123.0 24 178.01) 20 85 테트라싸이클린 (Tetracycline) 5.3 Positive 444.4 444.2 445.1 98.0 34 154.01) 22 410.1 16 86 툴라스로마이신 (Tulathromycin) 5.0 Positive 806.0 805.6 806.5 116.1 38 158.1 38 577.31) 24 87 트리메토프림 (Trimethoprim) 4.7 Positive 290.3 290.1 291.2 123.0 24 230.11) 22 261.1 24 88 트리페레나민 (Tripelennamine) 6.3 Positive 255.3 255.4 256.1 72.0 28 91.0 28 119.21) 28 89 티아물린 (Tiamulin) 8.4 Positive 493.7 493.3 494.3 73.1 50 119.0 40 192.11) 20 90 티암페니콜 (Thiamphenicol) 5.3 Negative 356.2 355.0 354.1 185.0 22 240.0 16 290.01) 12 91 틸디피로신 (Tildipirosin) 4.0 Positive 734.0 733.5 734.5 88.0 60 98.01) 34 174.1 36 92 틸미코신 (Tilmicosin) 6.9 Positive 869.1 868.6 869.5 88.0 72 174.01) 40 696.4 40 93 페나세틴 (Phenacetin) 7.3 Positive 179.2 179.1 180.0 65.0 30 92.8 22 110.01) 18 94 페노뷰카브 (Fenobucarb) 10.3 Positive 207.2 207.1 208.0 77.0 51 95.01) 17 152.0 11 95 페노티아진 (Phenothiazine) 7.1 Positive 199.2 199.0 199.0 139.6 36 166.91) 24 139.0 36 96 페플록사신 (Pefloxacin) 4.8 Positive 333.3 333.1 334.1 70.0 34 204.9 32 233.01) 24 97 프라지콴텔 (Praziquantel) 9.5 Positive 312.4 312.2 313.1 83.1 22 174.1 28 203.11) 14 98 플로르페니콜 (Florfenicol) 6.8 Negative 358.2 357.0 356.1 151.9 16 185.0 20 335.91) 10 플로르페니콜아민 (Florfenicol amine) 2.2 Positive 247.2 247.1 248.0 91.0 42 130.0 25 230.11) 10 99 플루메퀸 (Flumequine) 8.6 Positive 261.2 261.1 262.1 126.1 47 202.1 31 244.11) 17
기울기 조건표
| 시간(분) | A(%) | B(%) |
|---|---|---|
| 0.0 | 90 | 10 |
| 1.0 | 90 | 10 |
| 6.0 | 60 | 40 |
| 10.0 | 5 | 95 |
| 15.0 | 5 | 95 |
| 15.1 | 90 | 10 |
| 20.0 | 90 | 10 |
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이 조건의 칼럼 사양·유량이 크로마톡 계산기에 채워진 채로 열립니다.
고시 원문 보기 (축자)
가) 컬럼: C18계 컬럼(2.1 mm × 150 mm, 3.5 μm) 또는 이와 동등한 것 나) 이동상 (1) 이동상 A: 0.1%(v/v) 포름산(formic acid) 함유한 수용액 (2) 이동상 B: 0.1%(v/v) 포름산(formic acid) 함유한 아세토니트릴 [표 1] 다) 이동상 유량: 0.2 mL/분 라) 컬럼 온도: 40℃ 마) 주입량: 5 μL 2) 질량분석기 분석조건 가) 이온화 방법: ESI(Positive ion mode, Negative ion mode) 나) Capillary temperature: 350℃ 다) Capillary voltage: 3.4 kV 라) Collision gas: 아르곤(Ar) 또는 이와 동등한 것 마) 분석대상물질 조건 [표 2] 1) 정량이온 3) 검량선 작성표준용액을 농도별로 일정량 취하여 액체크로마토그래프-질량분석기에 각각 주입하여 얻은 크로마토그램상의 각 피크 높이 또는 면적 값으로 검량선을 작성한다. 4) 검출한계 (단위: mg/kg) [표 3] 5) 정량한계 (단위: mg/kg) [표 4] ※ 정성만 가능한 물질은 ‘-’로 표시
고시 원문의 표기·오탈자·조판 잔재를 고치지 않고 그대로 옮겼습니다.
상 분류 C18USP L1 상당
약전 일반명 '액체크로마토그래프용옥타데실실릴실리카겔'(USP 분류로는 L1 상당)에 해당. 약전은 브랜드를 지정하지 않으므로 각조가 기재한 물리 사양(치수·입자경 등)과 KP 통칙·일반시험법의 조정 허용범위 안에서 해당 상을 충족하는 C18을 선택할 수 있다 — 선택 기준은 시스템적합성(분리도·테일링·RSD) 통과 용이성과 재현성이다.